由乙腈一步法制备乙酸丁酯的研究

以丁醇和制备丙烯腈的副产物乙腈为原料 ,采用一步法合成了乙酸丁酯。通过正交实验得到了影响反应的 4种因素。确定了最佳的工艺条件为 :催化剂的量为样品质量的 40 % ;n(CH3CN)∶ n(C4 H9OH) =1∶ 1 .0 5 ;反应温度为 1 0 5℃ ;反应时间为 8h。在此反应条件下 ,乙酸丁酯的收率为 88.8% ,纯度可达 99.5 %。并用气相色谱及红外光谱对产品的纯度进行了表征     

ANALYSIS OF THE SCATTERING OF RIVET ON AIRCRAFT

This letter investigates the scattering characteristic of the rivets on aircraft.The electric Field Integral Equation (EFIE)is used with the moment to calculate the current distribution on the surface of the rivet.With the application of Gaussian integral corresponding triangular cell,the time to fill the Z matrix is greatly reduced.Finally,the RCS of a type of rivet on aircraft is analyzed.     

低品位硼矿的富集加工技术

报道了青海大柴旦地区低品位硼矿富集加工的新工艺，该工艺使硼矿品位30％－35％，B2O3收率大于80％，该工艺路线已工业化。     

西曲矿选煤厂降低介质损失的方法探讨

简述了西曲矿选煤厂三产品重介系统的脱介现状和存在的问题,提出了具体的改进措施,改造后的效果良好.     

浅析嵌入式电脑及其发展趋势

主要介绍嵌入式电脑的构成特点、应用与发展前景。     

综合孔径微波辐射计二阶量化数字相关器研究

微波辐射计作为一种无源遥感器,在遥感技术领域有着巨大的应用前景.传统的微波辐射计的空间分辨率受到天线孔径的限制.综合孔径微波辐射计利用了干涉测量原理和复相关技术,是一种可以有效地提高空间分辨率的新型辐射计.本文针对综合孔径微波辐射计的数字相关器进行了深入研究,分析论证了二阶量化数字相关器的工作机理,并对采用该种相关器的系统的信噪比进行了分析.初步的试验验证结果证明了该方案的有效性.     

Improvement of RCA transistor using RTA annealing after theformation of interfacial oxide

A polysilicon emitter RCA transistor (an ultra-thin interfacial oxide layer exists between polysilicon and silicon emitter) is presented which can operate at 77 K for the first time. An ultra-thin (1.5 nm) interfacial oxide layer is grown deliberately between polysilicon and silicon emitter using RCA oxidation and excellent device stability is obtained after rapid thermal annealing (RTA) treatment in nitrogen atmosphere. The RCA transistor exhibits good electrical performance at very low temperature for an emitter area of 3 × 8 μm². The maximum toggle frequency of a 1:2 static divider is 1.2 GHz and 732 MHz at 300 K and 77 K, respectively     

The influence of viewing distance on subjective impairment assessment

In this paper, the influence of viewing distance on subjective assessment of the impairment in video sequences is investigated. Subjective tests using the double-stimulus impairment scale variant II (DSIS II) method have been conducted at viewing distances of 5H (where H stands for the screen height) and 3H, respectively. Several statistical measures have been used to analyze the influence, including correlations and ANOVA (analysis of variance) tests. The results reveal that there is a very high correlation between the subjective scores, the variances are similar under the two viewing distances, the means of subjective data at these two viewing distances are the same, and there is no interaction between the viewing distance and the other two factors, i.e., the codec system and the source sequence. Throughout the tests, there is no evidence that a closer viewing distance such as 3H will vary the subjective test result statistically significantly.     

An EM‐based adaptive multiple target tracking filter

Tracking targets of interest is one of the major research areas in radar surveillance systems. We formulate the problem as incomplete data estimation and apply EM to the MAP estimate. The resulting filter has a recursive structure analogous to the Kalman filter. The advantage is that the measurement‐update deals with multiple measurements in parallel and the parameter‐update estimates the system parameters on the fly. Experiments tracking separate targets in parallel show that tracking maintenance ratio of the proposed system is better than that of NNF and RMS position error is smaller than that of PDAF. Also, the system parameters are correctly obtained even from incorrect initial values. Copyright © 2001 John Wiley & Sons, Ltd.     

固井声幅-变密度测井的影响因素分析

利用声幅－变密度测井进行固井质量的评价受到诸多因素的影响，各种影响因素对声幅－变密度测井资料的影响作用有较大的差异，根据大量测井资料分析和实验研究，对仪器偏心、测井时间，套管尺寸与重量，地层岩性，气侵、水泥环微间隔等因素的影响作用进行了较为深入的分析，为各种影响因素的识别与校正提出了相应的方法和依据。