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Summary Novel hyperbranched copolymers were successfully synthesized by the controlled charge transfer complex inimer and living radical copolymerization of p-(chloromethyl)styrene (PCMS) and acrylonitrile (AN). The resulting copolymers were characterized by SEC, NMR, FTIR, DSC and elemental analysis etc.. The influences of reaction conditions, such as the polymerization temperature, the catalyst (CuBr) concentration and the monomer ratio, on the resulting copolymers were investigated in detail. The monomer reactivity ratios were evaluated to be rPCMS=0.937 and rAN=0.088 respectively by the Fineman-Ross method. The higher are the polymerization temperature and the ratio of catalyst to monomer, the higher is the branching degree of the resulting copolymer. When the amount of monomer AN was used in excess than that of the monomer PCMS in the raw feed, the hyperbranched predominantly alternating copolymers HP[PCMS-co-AN] could be obtained. These hyperbranched copolymers were successfully used as functional macroinitiators to synthesize the star-shaped poly(PCMS-co-AN)/poly(MMA) block copolymers. 相似文献
54.
Electromigration reliability of interconnect under bidirectional current stress has been studied in a wide frequency range (mHz to 200 MHz). Experimental results show that the AC lifetime rises with the stress current frequency. The current density exponent and the activation energy of AC lifetime are found to be twice that of DC lifetime. Pure AC current stress failure at extremely high current density is believed to result from thermal migration of metal at hot/cold transition points 相似文献
55.
When melting processes are associated with an exothermic heat of mixing, unique coupled transport phenomena take place. In
this article, a mathematical model has been developed to simulate these unique coupled heat and mass transfer events. The
model was based on the control-volume finite difference approach and on an enthalpy method. In order to verify the mathematical
model, a low-temperature physical model was established consisting of ice and sulfuric acid solutions. In this physical model,
both temperature and velocity measurements were carried out. The model predictions were compared with experimental measurements,
and they were found to be in good agreement. The model was also applied to a high-temperature system, namely, the melting
of silicon metal in liquid high carbon iron. The predictions distinguished two periods present in the entire melting process.
In the first period, the silicon was heated up. The second period, i.e., free melting period, occurred in tandem with the exothermic reaction, and consequently, the melting process was greatly
accelerated. As was the case with the low-temperature physical model, as with the high-temperature system, good agreement
was obtained between the predicted results and the experimental measurements. 相似文献
56.
Kwong-Sak Leung Han-Bing Ji Yee Leung 《IEEE transactions on systems, man, and cybernetics. Part B, Cybernetics》1997,27(3):533-543
Associative-memory neural networks with adaptive weighted outer-product learning are proposed in this paper. For the correct recall of a fundamental memory (FM), a corresponding learning weight is attached and a parameter called signal-to-noise-ratio-gain (SNRG) is devised. The sufficient conditions for the learning weights and the SNRG's are derived. It is found both empirically and theoretically that the SNRG's have their own threshold values for correct recalls of the corresponding FM's. Based on the gradient-descent approach, several algorithms are constructed to adaptively find the optimal learning weights with reference to global- or local-error measure. 相似文献
57.
中国的三种非同步轨道卫星移动通信系统星座方案 总被引:6,自引:1,他引:5
本文介绍基于我国的三种非同步轨道卫星移动通信系统星座方案:低、中轨系统各有24和18颗星,轨道高度分别为1326和8035km,两系统各以5°和30°的仰角对我国的覆盖率为99.78%和99.96%;椭圆轨道系统12颗星,近、远地点分别为427和2906km,以7°和15°仰角对我国北纬20°以上地区覆盖率分别为97.90%和89.61%,若增加4颗中轨卫星,以15°仰角对我国的覆盖率为99.99%。 相似文献
58.
59.
Cluster analysis in industrial market segmentation through artificial neural network 总被引:6,自引:0,他引:6
Market segmentation has commonly applied cluster analysis. This study intends to make the comparison of conventional two-stage method with proposed two-stage method through the simulated data. The proposed two-stage method is the combination of self-organizing feature maps and K-means method. The simulation results show that the proposed scheme is better than the conventional two-stage method based on the rate of misclassification. 相似文献
60.
介绍了一种采用改进型的CLS3700数控测井系统对微电阻率扫描仪数据采集与控制接口的设计及实现方法。基于CLS3700数控测井仪和FMS仪采用89C51单片机设计出通信接口,解决了微电阻率方法。基于CLS3700数控测井仪和FMS仪采用89C51单片机设备出通信接口电路,解决了微电阻主扫描仪现现场实时处理中的瓶颈问题。 相似文献