Mercury transformation across particulate control devices in six power plants of China: The co-effect of chlorine and ash composition

This paper presents the results of field measurements on mercury speciation in six power plants of China by applying the Ontario hydro method. During the tests, flue gas was sampled simultaneously before and after particulate control devices (electrostatic precipitator and fabric filter baghouse) along with the pulverized coal, bottom ash and fly ash sampling. The amount of oxidized mercury in gas phase before and after ESP/FF suggests that mercury oxidation after combustion is a kinetically controlled process. The comparison of mercury speciation in different power plant indicates a clear relationship with coal type, especially the chlorine concentration and the basic ash compositions in coal. Both of the factors are analyzed quantitatively in this study. A new parameter C (ratio of chlorine in coal to base/acid ratio) has been introduced to evaluate the co-effect of the two factors above on mercury speciation.     

注塑流动与传热分析的自适应隐式控制体积法

在注塑流动与传热分析中采用自适应隐式控制体积法,利用自动控制的参数识别方法来自动调节时间步长,在每个时间步长流动将向前推进大约半个单元大小的距离,厚度方向的温度采用契比雪夫配点法进行计算,压力方程的求解方法是预条件共轭梯度法。计算结果表明,自适应隐式控制体积法的时间复杂度是结点数目的平方,而且1h之内可以求解10000结点规模的问题。     

尖山铁矿破碎机硐室围岩位移反分析及稳定性评价

推导了非均匀应力场下硐室（或隧道）的位移反分析公式，并利用尖山铁矿破碎机硐室围岩位移监测结果反演了围岩的力学参数。计算了硐室周围应力并对其稳定性作了分析评价。     

Synthesis of Dimethyl Carbonate from Methanol and Carbon dioxide using Potassium Methoxide as Catalyst under Mild Conditions

Pd-supported on WO₃–ZrO₂ (W/Zr atomic ratio=0.2) calcined at 1073 K was found to be highly active and selective for gas-phase oxidation of ethylene to acetic acid in the presence of water at 423 K and 0.6 MPa. Contact time dependence demonstrated that acetic acid is formed via acetaldehyde formed by a Wacker-type reaction, not through ethanol by hydration of ethylene.     

浅谈出口巴基斯坦铁路客车新型酚醛玻璃钢风道的研制开发

本文阐述了新型酚醛玻璃钢风道的成型工艺、开发过程，并与传统玻璃钢风道作了比较，论述了新型酚醛玻璃钢风道的优点，并对其应用前景和对铁路客车的设计思路的影响进行了探讨。     

高效液相色谱法测定焦性没食子酸

在大量焦性没食子酸（９９％）存在下，采用甲醇－二甲基甲酰胺－磷酸－水为流动相和Ｍｉｃｒｏｓｏｒｂ—ＭＶＴＭＣ１８色谱柱，能很好地将没食子酸以及其它酚类杂质与其分离。该方法测定焦性没食子酸简便、准确，已应用于工业生产。     

GLGLφ2.6×2立式液压全自动开门大口径硫化罐的结构设计

通过错齿液压缸驱动使罐盖与罐口啮合错开;通过翻转液压缸驱动使罐盖与罐口关闭打开,从而实现自动开门;在整个操作过程中依靠安全联锁装置,使每一操作步骤联锁,从而保证了安全性.     

Synthesis of nano Sb-encapsulated pyrolytic polyacrylonitrile composite for anode material in lithium secondary batteries

A novel process was proposed to synthesize nano Sb-encapsulated pyrolytic polyacrylonitrile composite for anode material in lithium secondary batteries. The preparation started with the dissolution of SbCl₃ and polyacrylonitrile (PAN) in dimethylformamide (DMF) solution, followed by the addition of KBH₄ to reduce Sb³⁺ in the solution. The Sb composite was obtained by pyrolysis of the Sb/PAN mixture that precipitated out when the DMF solution was added by plentiful water. The TEM analysis showed that about 100-200 nm Sb particles were embedded by the pyrolyzed PAN, which provided a conductive matrix to relieve the morphological change of Sb during electrochemical cycling. As-prepared composite presented good cycleability for lithium storage. The proposed process paves an effective way to prepare high performance alloy based composite anode materials for high performance lithium-ion batteries.