纳米碳酸钙和三元乙丙橡胶接枝马来酸酐协同增韧聚丙烯

纳米碳酸钙和三元乙丙橡胶接枝马来酸酐对聚丙烯具有显著的协同增韧作用，可能是因为纳米碳酸钙和三元乙丙橡胶接枝马来酸酐之间发生物理化学作用，形成一种新的核壳结构（硬核软壳），与一般的核壳增韧剂（硬壳软核）完全不同。     

Properties and crystallization kinetics of poly(ether ether ketone)‐co‐poly(ether ether ketone ketone) block copolymers

A series of block copolymers composed of poly(ether ether ketone) (PEEK) and poly(ether ether ketone ketone) (PEEKK) components were prepared from their corresponding oligomers via a nucleophlilic aromatic substitution reaction. Various properties of the copolymers were investigated with differential scanning calorimetry (DSC) and a tensile testing machine. The results show that the copolymers exhibited no phase separation and that the relationship between the glass‐transition temperature (T_g) and the compositions of the copolymers approximately followed the formula T_g = T_g1X₁ + T_g2X₂, where T_g1 and T_g2 are the glass‐transition‐temperature values of PEEK and PEEKK, respectively, and X₁ and X₂ are the corresponding molar fractions of the PEEK and PEEKK segments in the copolymers, respectively. These copolymers showed good tensile properties. The crystallization kinetics of the copolymers were studied. The Avrami equation was used to describe the isothermal crystallization process. The nonisothermal crystallization was described by modified Avrami analysis by Jeziorny and by a combination of the Avrami and Ozawa equations. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 97: 1652–1658, 2005     

基于自相关算法的 TOA 估计方法研究

TOA（脉冲到达时间）估计是检测和截获非合作突发通信信号的关键,在通信对抗中至关重要。在介绍基于自相关（AC）算法 TOA 估计原理的基础上,讨论了在低信噪比情况下自相关算法的门限设置问题。采用双门限方法对门限设置进行了改进,并通过计算机进行了仿真分析和验证。     

基于LabVIEW的三传声器声速测量方法研究

提出了一种新的声速测量方法,通过测量管道壁面上3个固定位置的声压求解出声速。以LabVIEW软件为测量分析平台,建立声速测量系统,测得当前介质在不同频率处的声速。与理论的声速计算值比较,测量结果验证了测量方法的正确性。     

NiCr薄膜微加热器在低温环境下的电学特性研究

设计了一种适用于深低温环境的微型加热器。使用AC磁控溅射技术将NiCr(80/20 at.%)合金沉积到SiO2/Si基底上,并采用微加工工艺实现薄膜图形化,作为加热器的加热元件。研究了NiCr薄膜的电学性能和晶体结构与退火条件之间的关系。实验表明:在450℃氮气环境下退火30min,可以获得深低温性能优良的NiCr加热器。该加热器在20K时的电阻温度系数(TCR)为80.80×10-6/K。X射线衍射(XRD)分析显示NiCr薄膜在450℃氮气环境下退火后,薄膜的结晶度增大,因此,退火条件对薄膜的电阻率和电阻温度系数有较大的影响。     

序贯抗差估计在旋转调制陀螺寻北中的应用

基于序贯抗差估计方法针对简化了的旋转调制陀螺寻北仪输出信号进行了寻北仿真研究.介绍了该型寻北仪的基本原理,在经典充贯平差的基础上,结合抗差M估计的原理,得到了序贯抗差估计的计算流程与公式.将寻北仪输出信号划分为2个阶段,对上述方法进行了仿真应用.仿真结果表明：通过该算法所得寻北结果误差均值与标准差均优于其它算法.     

灭多威及其混合剂对棉铃虫的杀卵作用和生化机理

用灭多威及其混合剂处理不同发育阶段的棉铃虫卵和初孵幼虫，生化法测定不同发育阶段卵中的乙酰胆碱酯酶，羧酸酯酶活性和蛋白质含量。结果表明，灭多威及其混合剂对初产卵杀卵作用较小，对发育至１日龄以后卵的杀卵作用大；３种混合剂对初孵幼虫的击倒毒力均高于灭多威；该类药剂杀卵作用大小与卵内乙酰胆碱酯酶的活性呈正相关。     

低速率拒绝服务攻击研究与进展综述

低速率拒绝服务攻击是新型的拒绝服务攻击,对Internet的安全造成严重的潜在威胁,引起众多研究者的兴趣和重视,成为网络安全领域的重要研究课题之一.自2003年以来,研究者先后刻画了Shrew攻击、降质攻击、脉冲拒绝服务攻击和分布式拒绝服务攻击等多种低速率拒绝服务攻击方式,并提出了相应的检测防范方法.从不同角度对这种新型攻击的基本机理和攻击方法进行了深入的研究;对TCP拥塞控制机制进行了安全性分析,探讨了引起安全问题的原因;对现有的各种各样的LDoS攻击防范和检测方案,从多个方面进行了分类总结和分析评价;最后总结了当前研究中出现的问题,并展望了未来研究发展的趋势,希望能为该领域的研究者提供一些有益的启示.     

Preparation and self‐assembly of poly(diglycidyl maleate‐co‐stearyl methacrylate)

Poly(diglycidyl maleate‐co‐stearyl methacrylate) (P(DGMA‐co‐SMA)) with reactive epoxy groups was synthesized by reaction of poly(maleic anhydride‐co‐stearyl methacrylate) (P(MA‐co‐SMA)) and epichlorohydrin. The effect of precipitant on self‐assembly behaviors of the resultant copolymer was investigated. It was found that vesicles and nanotubule liked aggregates can be obtained through self‐assembly of P(DGMA‐co‐SMA) in THF solution using CH₃CH₂OH (EtOH) as precipitant while spheral aggregates can be obtained using H₂O as precipitant. The mechanism of the self‐assembly behavior was discussed. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007     

Communicating Is Crowdsourcing: Wi-Fi Indoor Localization with CSI-Based Speed Estimation

Numerous indoor localization techniques have been proposed recently to meet the intensive demand for location-based service (LBS). Among them, the most popular solutions are the Wi-Fi fingerprint-based approaches. The core challenge is to lower the cost of fingerprint site-survey. One of the trends is to collect the piecewise data from clients and establish the radio map in crowdsourcing manner. However the low participation rate blocks the practical use. In this work, we propose a passive crowdsourcing channel state information (CSI) based indoor localization scheme, C²IL. Despite a crowdsourcing based approach, our scheme is totally transparent to the client and the only requirement is to connect to our 802.11n access points (APs). C²IL is built upon an innovative method to accurately estimate the moving speed solely based on 802.11n CSI. Knowing the walking speed of a client and its surrounding APs, a graph matching algorithm is employed to extract the received signal strength (RSS) fingerprints and establish the fingerprint map. For localization phase, we design a trajectory clustering based localization algorithm to provide precise real-time indoor localization and tracking. We develop and deploy a practical working system of C²IL in a large office environment. Extensive evaluations indicate that the error of speed estimation is within 3%, and the localization error is within 2 m at 80% time in a very complex indoor environment.