High-Tg porous polyimide films with low dielectric constant derived from spiro-(adamantane-2,9′(2′,7′-diamino)-fluorene)

Porous polyimide (PI) films with low dielectric constants and excellent thermal properties have been a pressing demand for the next generation of high-performance, miniature, and ultrathin microelectronic devices. A series of novel porous PI films containing fluorenyl-adamantane groups were prepared successfully via thermolysis of poly(ethylene glycol) (PEG) added in the PI matrix. The cross-sectional morphologies of porous PI films showed closed pores with diameters ranging from 135 to 158 nm, which were uniform and regular in shape without interconnectivity. These porous PI films exhibited excellent thermal properties with a glass-transition temperature at 376 °C whereas the 5% weight loss temperature in air excess of 405 °C due to enhanced rigidity afforded by fluorenyl-adamantane groups. Accompanied by thermolysis content of PEG increasing from 0 to 20 wt %, the density of porous PI films decreased, and the corresponding porosity grew significantly from 0 to 11.48%. Depending on porosity, the dielectric constant and dielectric loss of porous PI films significantly declined from 2.89 to 2.37 and from 0.050 to 0.021, respectively. These excellent properties benefit the as-prepared porous PI films for application as interlayer dielectrics, integrated circuit chips, or multichip modules in microelectronic fields. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47313.     

具有底水边界的水平井压力不稳态特征分析及认识

根据水平井三维渗流特征，在底水油藏情形仍假定顶面为不渗透隔层所封闭，底部则是恒压边界，水平井渗流表现为早期径向流以及稳定流动期，由此进行常规试井分析。以TKxxDH井为例，通过水平井的静压、压恢试井资料结果的对比分析，阐述了不稳定试井资料的应用，为此类油藏油井模型的选择及效果评价提供了可借签的经验。     

大牛地气田气井无阻流量的确定方法研究

大牛地气田气井试井大多采用一点法，由于气层渗透性差，测试时间短，流压很难达到稳定，计算的无阻流量往往偏高，且无法获得正确的产能方程。通过气田多口井修正等时试井数据进行统计分析，获得了一点法试井在不同生产时间下计算无阻流量的经验公式；利用气田修正等时试井的二项式方程系数曰，计算惯性阻力系数并经过曲线回归处理获得了经验关系式，很好地解决了一点法试井计算产能方程的问题。     

分组密码算法芯片验证

介绍了分组密码算法芯片验证的流程、内容和方法,详细介绍了分组密码算法芯片的验证技术——测试基准。     

共面波导(CPW)馈电单极子天线的设计与研究

给出一种工作于900MHz的共面波导(CPW)馈电单极子天线的设计。该单极子天线以共面波导的中心导带为辐射单极子，以中心导带两边的金属导体作反射板，结构简单紧凑。但是由于天线与共面波导之间缺少有效的隔离，造成天线性能受共面波导尺寸的影响较严重。本文通过模拟计算和实验测量详细分析了共面波导尺寸的变化对天线性能的影响，给出了结合共面波导尺寸设计的工作在900MHz的单极子天线结构数据。     

西门子全集成自动化理念初探

系统阐述了全集成自动化理念的内涵，指出其特点在于统一的数据管理、统一的编程组态、统一的通讯以及无与伦比的开放性，其中采用WINCC与STEP7两个软件进行了说明，井提出全集成自动化应用将是今后自动化技术发展应用的方向。     

Optimal and self‐tuning fusion Kalman filters for discrete‐time stochastic singular systems

Based on the optimal fusion estimation algorithm weighted by scalars in the linear minimum variance sense, a distributed optimal fusion Kalman filter weighted by scalars is presented for discrete‐time stochastic singular systems with multiple sensors and correlated noises. A cross‐covariance matrix of filtering errors between any two sensors is derived. When the noise statistical information is unknown, a distributed identification approach is presented based on correlation functions and the weighted average method. Further, a distributed self‐tuning fusion filter is given, which includes two stage fusions where the first‐stage fusion is used to identify the noise covariance and the second‐stage fusion is used to obtain the fusion state filter. A simulation verifies the effectiveness of the proposed algorithm. Copyright © 2008 John Wiley & Sons, Ltd.     

防治水泥稳定碎石基层沥青路面裂缝的措施浅析

水泥稳定碎石基层沥青路面裂缝产生的原因复杂 ,但非荷载型裂缝更为主要。防治水泥稳定碎石基层沥青路面的裂缝应该从设计和施工两方面考虑 ,其中由结构、材料组成设计 ,以及施工工艺出发控制水泥稳定碎石基层本身的收缩也是一项重要措施。     

MPEG-2视频编码标准及CLM4400视频编码芯片简介

本文通过MPEG-2和MPEG-1在视频方面的比较，简略地介绍了MPEG-2视频标准，并附带介绍了C-CUBE公司的MPEG-2视频编码芯片CLM4400的功能和应用前景。     

机械合金化过程中Fe70B30粉末晶粒尺寸和微观应变的研究

用Ｘ射线和电镜研究了Ｆｅ＿（７０）Ｂ＿（３０）粉末经不同时间高能球磨后晶粒尺寸和微观应力的变化。在机械合金化过程中，粉末的Ｘ射线衍射谱的宽度随球磨时间的增加逐渐加宽，这是晶粒细化和内部微观应力共同作用的结果。Ｘ射线衍射结果表明：随着机械合金化的进行，粉末的晶粒尺寸逐渐减小，球磨初期晶粒尺寸下降较快，经１５ｈ球磨，晶粒尺寸为２５ｎｍ，机械合金化进行到一定时间后晶粒尺寸下降缓慢，８０ｈ球磨后晶粒尺寸可达５ｎｍ。在机械合金化过程中球磨所造成的微观应变不大，球磨初期粉末的内应力随球磨时间增加而增加，当粉末粒子尺寸很小时，随球磨的进行粉末中的微观应变显著下降。