Allelopathic Potential and Chemical Constituents of Volatile Oil from Ageratum conyzoides

Fresh leaves and volatile oil of the important weed Ageratum conyzoides in south China were highly inhibitory to seedling growth of various cultivated crops, especially in an adverse habitat. The constituents of the volatile oil were analyzed by GC-MS. Eleven components were identified and six main components, precocene I, precocene II, 3,3-dimethyl-5-tert-butylindone, -caryophyllene, -bisabolene, and fenchyl acetate, were isolated by means of column chromatography. Precocene I, precocene II, -caryophyllene, and 3,3-dimethyl-5-tert-butylindone inhibited seedling growth of acceptor plants. Inhibitory activity of the volatile oil was more intense than that of the pure components. Fenchyl acetate and -bisabolene have no inhibitory activity, but when mixed with precocene II, they increased the inhibitory activity to growth of acceptor seedling plants. Experiments show that allelopathic synergism exists among allelochemicals of Ageratum conyzoides.     

外掺氧化镁拱坝温控仿真分析及横缝设置研究

基于现阶段条件下的混凝土热力学参数及温控措施,考虑气温、混凝土性能随龄期的变化及MgO的膨胀性等因素,采用三维有限元法对鱼粮水库拱坝的温度场进行仿真计算分析,计算结果表明,坝体混凝土在自然入仓、冬季保温的情况下,无需采取其它温控措施,通过对比不分缝方案及分缝方案,说明设置诱导缝可改善坝体应力分布情况。通过改变缝的位置更加有利于释放大坝温度应力,且各部位应力均能满足规范要求。     

强化质量意识 提高市场竞争力

介绍了企业在面临国际陶瓷市场竞争激烈的形势下，努力转变发展思路，拓宽市场，强化质量意识。根据市场变化，生产适销对路搞档优质陶瓷产品，增强产品的市场能力，提高了企业的经济效益。     

气相色谱法测定3-氯-1-丙醇

以填充柱气相色谱对 3 氯 1 丙醇进行了分析研究 ,方法变异系数 0 .5 % ,回收率99.5 0 %～ 10 0 .6 7%     

大掺量粉煤灰高性能混凝土的研究

本文从高分散性表面活性剂显著影响粉煤灰的形态效应而大幅降低混凝土用水量的角度出发,利用复合激发剂激发粉煤灰的火山灰效应,结合粉煤灰自身的微集料效应提高混凝土强度的技术手段,探讨了大掺量粉煤灰在混凝土中的应用,分析了高分散性表面活性剂与复合激发剂的组合对大掺量粉煤灰混凝土的作用机理。     

Image super-resolution based on multi-space sparse representation

Sparse representation provides a new method of generating a super-resolution image from a single low resolution input image. An over-complete base for sparse representation is an essential part of such methods. However, discovering the over-complete base with efficient representation from a large amount of image patches is a difficult problem. In this paper, we propose a super-resolution construction based on multi-space sparse representation to efficiently solve the problem. In the representation, image patches are decomposed into a structure component and a texture component represented by the over-complete bases of their own spaces so that their high-level features can be captured by the bases. In the implementation, a prior knowledge about low resolution images generation is combined to the typical base construction for high construction quality. Experiment results demonstrate that the proposed method significantly improves the PSNR, SSIM and visual quality of reconstructed high-resolution image.     

Know by a handful the whole sack: efficient sampling for top-k influential user identification in large graphs

Influence Maximization aims to find the top-K influential individuals to maximize the influence spread within a social network, which remains an important yet challenging problem. Most existing greedy algorithms mainly focus on computing the exact influence spread, leading to low computational efficiency and limiting their application to real-world social networks. While in this paper we show that through supervised sampling, we can efficiently estimate the influence spread at only negligible cost of precision, thus significantly reducing the execution time. Motivated by this, we propose ESMCE, a power-law exponent supervised Monte Carlo estimation method. In particular, ESMCE exploits the power-law exponent of the social network to guide the sampling, and employs multiple iterative steps to guarantee the estimation accuracy. Moreover, ESMCE shows excellent scalability and well suits large-scale social networks. Extensive experiments on six real-world social networks demonstrate that, compared with state-of-the-art greedy algorithms, ESMCE is able to achieve almost two orders of magnitude speedup in execution time with only negligible error (2.21 % on average) in influence spread.     

管材超声波分层缺陷检测中盲区的构成探析

管材超声波分层检测作为控制产品质量的关键步骤,必须引起相关从业人员的重视,特别是要重点分析分层缺陷检测中盲区的构成原因和分布特征。只有这样,才能切实保证检测结果的准确性,更好地控制管材质量。通过对超声波分层缺陷检测的重要性进行阐释,分析了其中盲区的构成和分布等问题。     

壳聚糖固定化脲酶生物传感器选择性测定铜离子

基于重金属对脲酶的抑制作用,研制了用于测定铜离子的生物传感器。该生物传感器的制备以壳聚糖为载体,将脲酶固定于pH电极表面。由于壳聚糖对Cu2+的富集,该生物传感器展现出高灵敏度。在样品溶液中加入5 mmol/L NaI,可以消除Hg2+和Ag+的干扰,从而实现Cu2+的选择性检测。在0.005～0.5μg/mL的浓度范围内,脲酶活性的抑制率与Cu2+浓度的对数呈良好的线性响应关系,其检出限为0.002μg/mL。将使用后的生物传感器浸泡于0.5 mmol/L的EDTA溶液再生5 min,被Cu2+抑制的脲酶的活性可以得到恢复。     

对位取代酚钾与10′10′-二烃基-9,9′-联二吖啶盐电荷转移光谱的研究

对位取代酚钾与１０′１０′－二烃基－９，９′－联二啶盐电荷转移光谱的研究宋化灿＊＊英柏宁郑祥礼（中山大学化学系，广州５１０２７５）关键词硝酸１０，１０′－二烃基－９，９′－联二啶盐，对位取代酚钾，电荷转移络合物，电子亲合能１０，１０′－二烃基－９，９...