茯苓皮三萜类物质抗氧化活性研究

以茯苓皮三萜甲醇提取物为材料,熊果酸为对照,通过化学发光法和比色法评价其体外抗氧化活性。结果表明：茯苓皮三萜能有效清除超氧阴离子自由基(O2－)、羟自由基( ·OH)和过氧化氢(H2O2),半数抑制率(IC50)分别为1.01、0.91、0.87mg/mL,且清除率与质量浓度存在剂量依赖关系;进一步体外抗氧化实验表明,茯苓皮三萜具有抑制家鸡红细胞溶血作用,对小鼠肝脂质过氧化产生的丙二醛(MDA)有较好的清除效果。     

北京黑猪的肉质特性研究

通过对北京黑猪肉的食用品质、营养品质和加工品质等肉质特性的检测分析,考察黑猪肉品质与普通猪肉品质的差异。结果表明：黑猪的肉色a值为5.85±1.63,熟肉率为(75.79±1.85)%,剪切力为(5638±64.20)N;每千克黑猪五花肉中矿物质元素Ca、Mg、Zn、Cu的含量为16.9、85.9、11、0.35mg/kg。饱和脂肪酸(C14:0、C16:0、C18:0和C20:0)总量约占全部脂肪总量的42.24%、油酸占46.64%;背最长肌中必需氨基酸总量(EAA)为9.42g/100g,非必需氨基酸总量(NEAA)为12.82g/100g,氨基酸总量(TAA)为22.23g/100g,EAA/TAA为42.35%,EAA/NEAA为73.46%。黑猪肉色较普通猪肉稍红,具有较高熟肉率,剪切力大小适中,含有多种矿物质元素和维生素,氨基酸和脂肪酸含量丰富,营养较为均衡,是具有重要开发价值的肉类品种。     

集中式多跳调度系统性能建模与协议参数优化

现有集中式多跳网络研究对其性能的建模分析较少考虑协议参数的影响,使实际场景中的协议设计缺乏理论依据.针对这一问题,充分考虑网络参数、业务参数、协议参数的影响,建立了集中式多跳网络调度时延模型和有效吞吐量模型.该模型和数值仿真结果揭示了网络节点个数、网络总带宽、业务流数目、平均跳数、控制时隙比例、最大可预约时隙个数等参数对系统性能的影响.最后给出了特定网络场景和业务需求条件下的控制时隙比例和最大可预约时隙个数等协议参数的优化策略.     

方形塔的有限元分析

应用 AN S Y S有限元分析软件, 考虑设备承受的内压、 液柱静压力、 风载荷以及地震载荷等多种工况 载荷, 对原料储斗方形塔进行了有限元参数化建模与分析, 并对平盖结构进行了优化设计, 确定了底部支撑基础环 板上地脚螺栓的尺寸和数量, 完成了对整台设备的强度计算, 为进一步进行详细设计及制造奠定了基础。研究结果 对方形塔的工程设计具有一定的指导意义。     

Chemical Profiling Using Uplc Q‐Tof/Ms and Antioxidant Activities of Fortunella Fruits

The fruits of Fortunella Swingle are widely consumed as fresh fruits and traditional medicine in China. China is the origin center and has the largest cultivated area of the genus Fortunella. In this study, the chemical compositions of ethanol extracts of the major Fortunella cultivated types including Fortunella japonica Swingle, Fortunella margarita Swingle, Fortunella crassifolia Swingle 1 (Lanshang) and Fortunella crassifolia Swingle 2 (Liuyang) were determined using ultra performance liquid chromatography coupled with quadrupole time‐of‐flight mass spectrometry (UPLC Q‐TOF/MS) method, and their antioxidant activities were evaluated. 12 compounds were identified and 5 compounds were tentatively characterized. The results showed that the chemical compositions of the ethanol extracts of 4 Fortunella cultivated types were largely the same. 3′, 5′‐di‐C‐glucopyranosylphloretin was the predominant flavonoid in Fortunella fruits, and Fortunella margarita Swingle had higher contents of flavonoids than other species. In addition, the data demonstrated high antioxidant activities of Fortunella fruits. The developed method could be available to rapidly analyze the chemical compounds in Fortunella fruits and its products. This study will provide information for further quality assessment and utilization of Fortunella resources.     

Cold Oxygen Plasma Treatments for the Improvement of the Physicochemical and Biodegradable Properties of Polylactic Acid Films for Food Packaging

The effects of cold plasma (CP) treatment on the physicochemical and biodegradable properties of polylactic acid (PLA) films were studied. The PLA films were exposed to CP for 40 min at 900 W and 667 Pa using oxygen as the plasma‐forming gas. The tensile, optical, and dynamic mechanical thermal properties, surface morphology, printability, water contact angle, chemical structure, weight change, and biodegradability properties of the films were evaluated during storage for up to 56 d. The tensile and optical properties of the PLA films were not significantly affected by CP treatment (CPT; P > 0.05). The surface roughness and water contact angle of PLA films increased by CPT and further increased during storage for 56 d. The printability of the PLA films increased following CPT and remained stable throughout the storage period. CP‐induced hydrophilicity was also sustained during the storage period. The PLA films lost 1.9% of their weight after CPT, but recovered 99.5% of this loss after 14 d in storage. Photodegradation, thermal, and microbial biodegradable properties of the films were significantly improved by CPT (P < 0.05). Accelerated biodegradation of CP‐treated PLA sachets with and without cheese was observed in compost. These results demonstrate the potential of CPT for modifying the stiffness, water contact angle, and chemical structure of PLA films and improving the printability and biodegradability of the films for food packaging.     

不同感官质量曲药在培曲过程中理化指标变化规律研究

从五粮液中温曲多批次曲药中选取感官质量差异较大的两个批次曲药作为研究对象,分别对其培曲过程中发酵力、糖化力、温度和水分等理化指标进行分析研究,为进一步优化培曲过程管理,提升曲药质量提供重要依据。结果表明：在培曲过程中,优质曲与普通曲的理化指标变化趋势大体一致,但变化过程存在差异。优质曲的糖化力整体偏低,平均值为300～400 mg/（g·h）;而普通曲糖化力整体较高,平均值为400～500 mg/（g·h）。优质曲的发酵力整体偏高,平均在400～500 mL/（g·72 h）之间;普通曲则整体偏低,平均在300 mL/（g·72 h）左右;优质曲酵母菌数量在培曲第8天左右可达到约107个/g曲药,约是普通曲的10倍。 关键词：中图分类号：TS262.3 文章编号：0254-5071（20１6）10-0116-04 doi:     

综采工作面推进速度与支架工作阻力的研究

为了使察哈素煤矿31201工作面在末采段的支架能够安全回撤,实现贯通时顶板无来压的目标,运用理论分析与现场实测,研究推进速度对支架工作阻力的影响。首先对支架工作阻力的确定方法进行介绍,其中包括3种方法;其次通过对推进速度与围岩应力的理论分析,得出随着综采面推进速度的增加,支架工作阻力减小;最后,将实测支架工作阻力与推进速度进行线性回归,得出随推进速度的增加,支架循环末阻力下降。掌握这一规律能够有效指导末采,保证支架安全回撤。     

基于模糊调整的矿井提升机速度控制方法

为了满足现场矿井提升机对不同工况的性能需求,研究了基于模糊调整的PI速度调节器,以转速和转矩作为模糊化输入。实验结果表明,系统在轻载和重载、低速和高速时均具有较好的控制性能,可以同时满足生产和检修运行需求。     

河北宣化“战国红”玛瑙的结构特征及颜色成因

宣化“战国红”玛瑙是指产于河北省张家口市宣化县塔儿村乡滴水崖、王千户一带的缟玛瑙,主要颜色为红色和黄色。以宣化“战国红”玛瑙原石为研究对象,利用偏光显微镜、环境扫描电子显微镜和拉曼光谱等测试技术对其结构特征进行测试与分析,并结合热处理实验探讨其颜色成因。宣化“战国红”玛瑙在正交偏光显微镜下主要有长纤维状结构、短纤维状结构、球粒状结构和晶质石英等。扫描电子显微镜图像显示晶粒大小约为0.5~5.0μm,晶粒呈大小不一的片状紧密堆积。能谱仪测试表明宣化“战国红”的主要成分为SiO2,并含有Fe、Al、Mg、Na、K、Ca等元素。结合拉曼光谱测试可知,红色条带可见较强的赤铁矿吸收峰,黄色条带可见较强的针铁矿特征吸收峰。对“战国红”玛瑙在200、300、400℃温度下进行热处理,热处理后玛瑙透明度下降,表面干涩,随着加热温度的升高,黄色条带中红色调越来越明显,400℃时黄色完全变成红色,这是由针铁矿失水转化为赤铁矿所致。结合拉曼光谱测试与热处理实验可知宣化“战国红”玛瑙红色主要由赤铁矿致色,黄色主要由针铁矿致色。