绍兴市城区河道整治工程若干问题初探

通过对绍兴城区环城河、大环河、古运河、古城河等河道整治工程内容和整治成效的分析，总结了绍兴城区河道整治的5大特点，针对河道建设中存在的有关问题，提出了今后城市河道整治的4条具体措施。     

SU-8 3D microoptic components fabricated by inclined UV lithography in water

Out-of-plane microlenses and microoptical fiber holder are two of the most important components for building an integrated microoptic system with a precise alignment accuracy. In this paper, a simple and convenient method to fabricate these components from SU-8 by using inclined UV lithography in water is proposed. It consists of two perpendicular exposures in SU-8 at ±45°. DI water possesses a low absorption coefficient and a moderate and stable value of refractive index in near UV. Using water, the exposure angle in SU-8 can be increased to 50° from 35° in air necessary to pattern the desired 45° slope of the sidewalls. The principle of the proposed technique and the detailed fabrication process of the microoptic components will be presented. The integratability of the fabricated components was demonstrated by the fabrication of the microoptical fiber holder with a pre-aligned out-of-plane microlens.     

多孔薄膜荫罩热变形的有限元仿真设计

荫罩的热变形使电子束产生着屏偏移 ,进而导致了色纯变坏。本文采用大型软件ANSYS对 1 5英寸荫罩进行了热变形的有限元仿真 ,从而得到了电子束的着屏偏移。建立了包括阴极射线管 (CRT)里所有部件的完整的有限元模型。荫罩被建为无孔连续薄壳的模型 ,对它的表面导热系数和表面弹性模量作了等效的计算。考虑了弹簧片的预应力以及弹簧片和销钉的连接。这样可使我们的分析模型更接近真实情况。本文给出了 50 0、1 0 0 0、1 0 0 0 0s时的热变形和电子束着屏偏移。分析表明 :电子束着屏偏移的最大值发生在 50 0s左右。利用这种分析方法及研究结果可指导新型荫罩的设计和研制。     

基体温度对磁控溅射沉积ZAO薄膜性能的影响

利用中频交流磁控溅射方法 ,采用氧化锌铝陶瓷靶材 [w(ZnO) =98%、w(Al2 O3 ) =2 % ]制备了ZAO(ZnO∶Al)薄膜 ,观察了基体温度对ZAO薄膜的晶体结构、电学和光学性能的影响 ,采用X射线衍射仪对薄膜的结构进行了分析 ,采用光学分度计和电阻测试仪测量了薄膜的光学、电学特性 ,采用霍尔测试仪测量了薄膜的载流子浓度和霍尔迁移率。结果表明 :沉积薄膜时的基体温度对薄膜的结构、结晶状况、可见光透射率以及导电性有较大的影响。当基体温度为 2 5 0℃ ,Ar分压为 0 8Pa时 ,薄膜的最低电阻率为 4 6× 10 -4Ω·cm ,方块电阻为 35Ω时 ,可见光 (λ =5 5 0nm)透射率高达 92 0 %。     

为国家重点建设项目服务打造有公信力的名牌监理公司

中咨工程建设监理公司是中国国际工程咨询公司的全资子公司。而其母公司早在80年代即承担起多个工程项目的施工监理。进入90年代，中咨监理业务得到迅速发展，成为中国监理行业的一支重要力量。2001年起经过整合重组而成中咨工程建设监理公司后，以集中和优化资源配置，努力打造有公信力的名牌监理公司。经过多年的探索和积累，该公司形成了一套既符合国家规范，又具有自身特色的管理模式。本文介绍该公司在承担国家重点建设项目工程监理方面的一些经验和做法。     

Ring‐opening polymerization of D,L‐lactide by rare earth 2,6‐dimethylaryloxide

Ring‐opening polymerization of D,L ‐lactide (LA) has been successfully carried out by using rare earth 2,6‐dimethylaryloxide (Ln(ODMP)₃) as single component catalyst or initiator for the first time. The effects of different rare earth elements, solvents, monomers and catalyst concentration as well as polymerization temperature and time on the polymerization were investigated. The results show that La(ODMP)₃ exhibits higher activity to prepare poly(D,L ‐lactide) (PLA) with a viscosity molecular weight of 4.5 × 10⁴ g mol^?1 and the conversion of 97 % at 100 °C in 45 min. The catalytic activity of Ln(ODMP)₃ has following sequence: La > Nd > Sm > Gd > Er > Y. A kinetic study has indicated that the polymerization is first order with respect to both monomer and catalyst concentration. The apparent activation energy of the polymerization of LA with La(ODMP)₃ is 69.6 kJ mol^?1. The analyses of polymer ends indicate that the LA polymerization proceeds according to ‘coordination–insertion’ mechanism with selective cleavage of the acyl–oxygen bond of the monomer. Copyright © 2004 Society of Chemical Industry     

MIP-CGP工艺专用催化剂CGP-1的开发与应用

阐述了生产汽油组分满足欧Ⅲ排放标准并多产丙烯的催化裂化工艺（简称MIP-CGP）专用催化剂（简称CGP-1）的研究开发与工业应用结果。CGP-1催化剂的基质具有良好的容炭性能，使活性组元受到良好保护，其优势作用在第二反应区得以充分发挥，具有更高的氢转移活性和强的汽油小分子烯烃裂化活性。中国石化九江分公司和镇海炼化公司的MIP-CGP工业试验标定结果表明，与常规FCC相比，采用CGP-1催化剂的MIP-CGP技术在生产烯烃体积分数小于18％的汽油组分的同时，丙烯产率达到8％以上。此外，汽油诱导期大幅提高，抗爆指数增加；总液体收率有所提高，干气产率下降，焦炭选择性良好。     

Novel tiO2 nanocatalysts for wastewater purification: tapping energy from the sun.

Water treatment using TiO2 semiconductor as a durable heterogeneous photocatalyst has been the focus of environmentalists in recent years. Currently, we developed an inexpensive and highly efficient approach for synthesizing nitrogen-doped TiO2 with lower band-gap energy that can respond to visible light. Doping on the molecular scale led to an enhanced nitrogen concentration of up to 21.8%. Reflectance measurements showed the synthesized N-doped TiO2 nanoparticles are catalytically active with the absorbance that extends into the visible region up to 600 nm. The water purification potential of this new class of compound was evaluated by studying the photodegradation of Acid Orange 7 (AO7) and E. coli. Experiments were conducted to compare the photocatalytic activities of N-doped TiO2 nanocatalysts and commercially available Degussa P25 power under identical solar light exposure. N-doped TiO2 demonstrated superior photocatalytic activities in both chemical compound degradation and bactericidal reactions. The result of this study shows the potential of applying new generations of catalyst for wastewater purification and disinfection.     

�����������������������������ܿ��������о�

白马庙气田蓬莱镇气藏储层致密 ,孔隙结构复杂 ,非均质性强 ,单井产能低 ,研究储层特征和受控因素 ,加强储层改造方是气藏效益开发的出路。储层精细研究揭示 ,气井产能受沉积相和构造条件控制 ;高、中产井与大而厚、物性好的河口坝、河道砂坝沉积微相有关 ,纵向上具很强的层段性 ,主产层集中在Ⅳ～③、Ⅲ～③两套砂组 ,其钻探成功率分别达 82 %和 10 0 % ;平面上多分布于主体构造和东南鼻状突起 ,二者高、中产能井分别占 30 %和 70 %。在深入的地质研究和储层压裂评层选井的基础上 ,采用多层打开、分层压裂、多层合采的方法可提高气井产能 ,并形成了一套行之有效的压裂评层选井的综合配套技术。采用该技术优选出 19口井 ,已实施 5口井全获成功 ,气产量成倍或十几倍增加 ,其中白浅 4 5井气无阻流量高达 18× 10 4m3 /d ,白浅 38井投产 16 5d净增产值 10 0余万元