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61.
The Alternaria toxins alternariol (AOH; 3,7,9-trihydroxy-1-methyl-6H-benzo[c]chromen-6-one) and alternariol methyl ether (AME, 3,7-dihydroxy-9-methoxy-1-methyl-6H-benzo[c]chromen-6-one) are common contaminants of food and feed, but their oxidative metabolism in mammals is as yet unknown. We have therefore incubated AME and AOH with microsomes from rat, human, and porcine liver and analyzed the microsomal metabolites with HPLC and GC-MS/MS. Seven oxidative metabolites of AME and five of AOH were detected. Their chemical structures were derived from their mass spectra using deuterated trimethylsilyl (TMS) derivatives, and from the information obtained from enzymatic methylation. Several of the metabolites were identified by comparison with synthetic reference compounds. AME as well as AOH were monohydroxylated at each of the four possible aromatic carbon atoms and also at the methyl group. In addition, AME was demethylated to AOH and dihydroxylated to a small extent. As the four metabolites arising through aromatic hydroxylation of AME and AOH are either catechols or hydroquinones, the oxidative metabolism of these mycotoxins may be of toxicological significance. 相似文献
62.
Manfred Schulz Gerd West Sakum Ourk Ingo Strunz 《Advanced Synthesis \u0026amp; Catalysis》1980,322(2):295-304
Azoperoxides. VI. Selective Decomposition of β-Azoacylperoxides The selective decomposition of the O O-Groups in the azoperoxides 1 and 2 is possible by reaction with dimethylaniline at 35°C. Rate constants were measured and the decomposition products were analyzed. Intermediates are azoalkyl radicals. The radical yield of the amine induced decomposition of 2 in ethylbenzene is 8.2% at 35°C. UV irradiation of the azoperoxides 1 and 2 at 20°C in ethylbenzene results in a quantitative and selective decomposition of the azo groups. Intermediates are C-radicals with intact peroxide groups. The reaction of 1 and 2 with triethylstannane yields reduction products of the O O-groups and the NN-groups, respectively. 相似文献
63.
Scientometrics - The primary goal of this article is to identify the research fronts on the application of data-driven methods in business and economics. For this purpose, the research literature... 相似文献
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Manfred Jeitler 《控制论与系统》2013,44(3-4):315-333
This article gives an introduction into the current understanding of time invariance and evidence of its violation in experimental particle physics. The connection between time invariance and other discrete symmetries, particularly, CP-invariance, is explained. The first experimental determination of CP-violation is explained, and recent experiments on CP-violation and on T-violation are discussed. 相似文献
69.
Andreas Menrad Thomas Goedecke Klaus‐Peter Gruender Manfred H. Wagner 《Packaging Technology and Science》2013,26(6):311-326
The effect of the wall thickness variation of blow‐moulded bodies made of high‐density polyethylene on an internal pressure test after prestoring the packaging with standard liquids was evaluated in experiments and simulations. The objects of the investigation were jerrycans used for the transportation and storage of dangerous goods. The wall thickness was determined using two alternative methods to the magnetostatic measurement. These alternative methods are used for research purpose to get a volumetric model of the jerrycan wall as a geometric model for the simulation. The comparison of the experiments and the simulations of the internal pressure test were performed using the digital image correlation method. The integral strain and deformation of the whole jerrycan was detected by measuring the total mass of the jerrycan being filled with water during the internal pressure test. This is a suitable alternative to the optical measurements of local deformation by the digital image correlation method. Prestorage at 40 °C without the influence of chemicals strengthens the jerrycan, whereas the swelling effect of butyl acetate and hydrocarbon mixture softens the jerrycan. The comparison with the experiment is necessary to verify the accuracy of the simulation. It shows that the deformation can be simulated more precisely by using the actual measured geometry. The weakening of the high‐density polyethylene caused by a hydrocarbon mixture can be simulated using the Arrhenius equation. The aim of the simulation was to discover whether it is possible to use specimens to predict the behaviour of a packaging both after the influence of standard liquids. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
70.
Marco Deluca Raúl Bermejo Martin Pletz Manfred Wießner Peter Supancic Robert Danzer 《Journal of the European Ceramic Society》2012,32(16):4371-4380
Miniaturised silicon-based multilayer chips are nowadays widespread as semiconductor components for the mobile device technology. The use of special processing and integration procedures requires such materials to possess a definite mechanical strength to ensure the functionality of the entire device. The strength and mechanical reliability of such components can be described by the Weibull theory, and is highly influenced by the geometry of the metallisation and other near-surface functional layers. In this work, we attempt to clarify the mechanisms leading to the failure of the metallised side of Si-chip components. The combined use of Finite Elements (FE) and Focused Ion Beam (FIB) analyses allowed recognising that cracks are induced in the metal-oxide-silicon interfacial area well before complete failure of the component. Such cracks have a crucial role in the lower strength and higher Weibull modulus observed on the metallised side. 相似文献