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11.
Quantitation of Cefaclor in Pharmaceutical Dosage Forms Using High Performance Liquid Chromatography
Mary Mathew V. Das Gupta Charlie Bethea 《Drug development and industrial pharmacy》1993,19(14):1723-1729
A stability-indicating high-performance liquid chromatography for the quantitation of cefaclor in pharmaceutical dosage forms has been developed. The method is accurate and precise with a percent relative standard deviation of 1.2 based on 5 readings. A number of inactive ingredients present in the capsules and suspensions did not interfere with the assay procedure. The extraction procedure from the dosage forms is very simple. The recovery from the synthetic mixtures was quantitative. The capsules which had expired 3 years ago lost only 3% of the potency. The drug appears to be very sensitive to strong acids or bases since a 5 minute boiling caused 100% degradation of drug in both the solutions. 相似文献
12.
Mary Cramer 《电子设计应用》2007,(3):20-20,22
目前,低成本手机数量不断增多,市场份额越来越大,比高端手机更受欢迎。研究表明,未来三年,低成本手机市场还将持续增长,这将是无线产业最主要的发展趋势之一,已经并将继续为无线手机制造商、服务供应商及芯片设计商带来金融、市场、战略和技术领域的重大变革与挑战。 相似文献
13.
Malik Mary L.; Beutler Larry E.; Alimohamed Shabia; Gallagher-Thompson Dolores; Thompson Larry 《Canadian Metallurgical Quarterly》2003,71(1):150
The definition of an empirically supported treatment (EST) arguably embodies 2 untested assumptions: (a) that different manualized renditions of the same therapy are functionally equivalent and (b) that therapies can be reliably applied independently of therapist, setting, and format. These assumptions were tested as applied to cognitive therapy (CT), using process data from a large multisite study (N=235) that included 3 cognitive and 6 alternative therapies. Although the non-CTs were more variable than the CTs on 2 of 4 dimensions studied (directiveness and emotional arousal), there was considerable variation among the 3 CTs, even when implemented in the current context of rigorous training, manualization, and adherence checks. Results are discussed as related to the assumptions underlying EST criteria. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
14.
Shuman Daniel W.; Cunningham Mark D.; Connell Mary A.; Reid William H. 《Canadian Metallurgical Quarterly》2003,34(3):233
Forensic psychology has made important gains in professional recognition and stature in the courts, resulting in increasing demands for mobility of expertise. Current regulations regarding the interjurisdictional temporary forensic practice of psychology, however, are characterized by variability of regulations, ambiguity and inaccessibility, and continuing total barriers. A uniform, well-reasoned policy is needed. A conceptual basis for such a policy is provided by a discussion of licensing rationales and the application of these to forensic practice. Uniformity, public and professional protection, and practicability are identified as fundamental regulatory criteria. A Model Rule Regarding the Temporary Forensic Practice of Psychology is proposed for adoption by state licensing boards on a nationwide basis. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
15.
Yoon Carolyn; Feinberg Fred; Hu Ping; Gutchess Angela Hall; Hedden Trey; Chen Hiu-Ying Mary; Jing Qicheng; Cui Yao; Park Denise C. 《Canadian Metallurgical Quarterly》2004,19(3):379
Understanding how aging influences cognition across different cultures has been hindered by a lack of standardized, cross-referenced verbal stimuli. This study introduces a database of such item-level stimuli for both younger and older adults, in China and the United States, and makes 3 distinct contributions. First, the authors specify which item categories generalize across age and/or cultural groups, rigorously quantifying differences among them. Second, they introduce novel, powerful methods to measure between-group differences in freely generated ranked data, the rank-ordered logit model and Hellinger Affinity. Finally, a broad archive of tested, cross-linguistic stimuli is now freely available to researchers: data, similarity measures, and all stimulus materials for 105 categories and 4 culture-by-age groups, comprising over 10,000 fully translated unique item responses. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
16.
Cuddihy P. Hinman R.T. Avestruz A. Lupton E.C. Livshin G. Rodriguez J.I. Leeb S.B. Clark C.M. Horvath K.J. Volicer L. Landfeldt B. Kay J. Kummerfeld R. Quigley A. West D. Apted T. Sinclair G. Haniff D.J. Kalawsky R. Atkins D. Lewin M. Brown S.J. Shahmehri N. Aberg J. Maciuszek D. Chisalita I. 《Pervasive Computing, IEEE》2004,3(2):48-50
This issue's Works in Progress department presents six abstracts for projects that are developing interesting solutions to the elderly's quality of life challenges. The first two abstracts discuss projects that will help provide the elderly with freedom and independence by instrumenting their environments with supportive technology. The next two abstracts discuss projects building specialized user interfaces for addressing some of the challenges associated with aging, such as vision impairment. The final two abstracts present projects that will aid independence for the elderly by providing remote monitoring and assistance. 相似文献
17.
It is proposed that when solving an arithmetic word problem, unsuccessful problem solvers base their solution plan on numbers and keywords that they select from the problem (the direct translation strategy), whereas successful problem solvers construct a model of the situation described in the problem and base their solution plan on this model (the problem-model strategy). Evidence for this hypothesis was obtained in 2 experiments. In Experiment 1, the eye fixations of successful and unsuccessful problem solvers on words and numbers in the problem statement were compared. In Experiment 2, the degree to which successful and unsuccessful problem solvers remember the meaning and exact wording of word problems was examined. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
18.
High-performance liquid chromatography of human milk triacylglycerols and gas chromatography of component fatty acids 总被引:1,自引:0,他引:1
Human milk triacylglycerols were separated by high-performance liquid chromatography. A 5-μ Supelcosil LC-18 column (Supelco,
Inc., Bellefonte, PA) was used with acetone/acetonitrile (64∶36, vol/vol) as mobile phase. Triacylglycerols were tentatively
identified based on theoretical carbon number and relative retention time. Despite changes resulting from dietary fat variation,
the major component triacylglycerols were those composed of palmitic, oleic and linoleic acids. Triacylglycerols with palmitic,
stearic and oleic acids were present as minor components. Fatty acids were quantified by gas chromatography relative to an
internal standard. Ratios of n−6/n−3 fatty acids were found to be high than previously reported.
Based on a paper presented at the Symposium on Milk Lipids held at the AOCS Annual Meeting, Baltimore, MD, April 1990. 相似文献
19.
Qiwen Wang Xiaoyun Sun Bruce L. Golden Lenore Desilets Edward A. wasil Scott Luco Adam Peck 《Computers & Operations Research》1993,20(8)
A crucial step in manufacturing microcircuits is the wire bonding process in which a very thin gold wire must be formed to connect two surfaces in the microcircuit. The quality of the wire bond can be measured by visual inspection and a pull test—both of which are high-reliability, high-cost approaches to statistical process control. Westinghouse wanted to develop a high-reliability, low-cost quality assurance system. In this paper, we report on a year-long study to construct a neural network model that is capable of predicting the quality of wire bonds. The results of our modeling efforts reveal that neural networks are useful tools for statistical process control problems. 相似文献
20.
There is now considerable evidence suggesting that alterations in the DNA methylating machinery play an important role in tumorigenesis and tumour progression. For example, focal hypermethylation and generalised genomic demethylation are features of many different types of neoplasms. It is thought that tumorigenesis and tumour progression may be caused by hypermethylation induced mutational events and silencing of genes which control cellular proliferation and/or demethylation induced reactivation of genes which may only be required during embryological development. Consequently, we have begun to investigate the role of DNA methylation and developmental genes in malignant lymphoproliferative diseases. Previously, in all cases of non-Hodgkins lymphoma and leukemia studied, we have shown that the myogenic developmental gene Myf-3 is abnormally hypermethylated. In this review we discuss the possible significance of these findings since in vitro studies suggest that Myf-3 may play an important role in control of the cell cycle and therefore lymphomagenesis. In vitro and in vivo evidence suggests that PAX genes may also have oncogenic potential. The PAX family of developmental genes are involved in cellular differentiation, proliferation and cell migration. Expression of PAX3 in particular is associated with cellular mobility. Our previous studies have indicated that alternate regional expression of PAX genes may be controlled by DNA methylation. Therefore, we have proposed that abnormal methylation profiles of PAX3 may be associated with neoplastic transformation and/or metastatic potential. Results thus far reveal that the paired box of PAX3 is abnormally hypermethylated and the homeobox abnormally hypomethylated in lymphomas and leukemias. These new findings are consistent with our postulate and support the idea that inappropriate methylation induced activation or inactivation of developmental genes such as Myf-3 and PAX3 play an important role in lymphomagenesis and disease progression and that inspection of the methylation status of other developmental genes is warranted. 相似文献