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92.
93.
Multipole expansions offer a natural path to coarse-graining the electrostatic potential. However, the validity of the expansion is restricted to regions outside a spherical enclosure of the distribution of charge and, therefore, not suitable for most applications that demand accurate representation at arbitrary positions around the molecule. We propose and demonstrate a distributed multipole expansion approach that resolves this limitation. We also provide a practical algorithm for the computational implementation of this approach. The method allows the partitioning of the charge distribution into subsystems so that the multipole expansion of each component of the partition, and therefore of their superposition, is valid outside an enclosing surface of the molecule of arbitrary shape. The complexity of the resulting coarse-grained model of electrostatic potential is dictated by the area of the molecular surface and therefore, for a typical three-dimensional molecule, it scale as N2/3 with N, the number of charges in the system. This makes the method especially useful for coarse-grained studies of biological systems consisting of many large macromolecules provided that the configuration of the individual molecules can be approximated as fixed. 相似文献
94.
Atomic-resolution transmission electron microscopy has largely benefited from the implementation of aberration correctors in the imaging part of the microscope. Though the dominant geometrical axial aberrations can in principle be corrected or suitably adjusted, the impact of higher-order aberrations, which are mainly due to the implementation of non-round electron optical elements, on the imaging process remains unclear. Based on a semi-empirical criterion, we analyze the impact of residual aperture aberrations on the quality of exit-plane waves that are retrieved from through-focal series recorded using an aberration-corrected and monochromated instrument which was operated at 300 kV and enabled for an information transfer of ∼0.05 nm. We show that the impact of some of the higher-order aberrations in retrieved exit-plane waves can be balanced by a suitable adjustment of symmetry equivalent lower-order aberrations. We find that proper compensation and correction of 1st and 2nd order aberrations is critical, and that the required accuracy is difficult to achieve. This results in an apparent insensitivity towards residual higher-order aberrations. We also investigate the influence of the detector characteristics on the image contrast. We find that correction for the modulation transfer function results in a contrast gain of up to 40%. 相似文献
95.
Philip Dobie Julie Dendy Christine Sherman Jenny Padgham Anna Wood Angharad M. R. Gatehouse 《Journal of Stored Products Research》1990,26(4):177-186
The importance of carefully applied bioassay techniques is highlighted for identifying resistance of Phaseolus spp to the bruchids Acanthoscelides obtectus (Say) and Zabrotes subfasciatus Boheman. Two potential sources of resistance are identified amongst the varieties of P. vulgaris screened. In one the presence of a lectin-like protein (LLP) was identified, which has previously been associated with resistance, while in the other, resistance may be linked to the presence of a novel protein, similar to but not the same as LLP. The use of anti-LLP antibodies are suggested as a useful tool for distinguishing between resistant and susceptible varieties. Five varieties of P. lunatus and six of P. acutifolius are shown to be resistant to A. obtectus, and the potential is recognized for transferring resistant genes to P. vulgaris via interspecific crosses. 相似文献
96.
Philip O Owuor John E Orchard Janet M Robinson Sarah J Taylor 《Journal of the science of food and agriculture》1990,52(1):55-61
The chemical composition of black teas (Camellia sinensis L) varies when the green leaf from which they are manufactured is withered physically to the same degree but for different periods. Caffeine contents progressively increase with prolonged withering time whereas theaflavins decrease due to prolonged withering. Although the sums of group I and group II volatile flavour compounds (VFC) decrease with prolonged withering time, the flavour index (expressed as group II VFC/group I VFC) increases due to prolonged withering. No significant changes were noted in the thearubigin levels with variation in withering time, but the tasters' evaluations were at a maximum for teas withered for 14 h. Subsequently the evaluation decreased with longer withering times. 相似文献
97.
Philip O Owuor Herman O Odhiambo Janet M Robinson Sarah J Taylor 《Journal of the science of food and agriculture》1990,52(1):63-69
Green leaf standard, chemical composition and quality of black tea (Camellia sinensis (L) O Kuntze) change with plucking intervals. Long plucking intervals lead to poor leaf standard with a lot of mature leaves and lower theaflavins, the sum of volatile flavour compounds imparting a sweet flowery aroma (group II volatile flavour compounds), caffeine contents and tasters' evaluations of black tea. The sum of volatile flavour compounds imparting inferior, grassy, green flavour (group I volatile flavour compounds) to tea, however, increases with long plucking intervals. 相似文献
98.
Georg Arnold Robert Winkler Martin Stermitz Angelina Orthacker Joo‐Hyon Noh Jason D. Fowlkes Gerald Kothleitner Michael Huth Philip D. Rack Harald Plank 《Advanced functional materials》2018,28(19)
The detection of gas species with high sensitivity is a significant task for fundamental sciences as well as for industrial applications. Similarly, the ongoing trend for device miniaturization brings new challenges for advanced fabrication including on‐demand functionality tuning. Following this motivation, here the additive, direct‐write fabrication of freestanding 3D nanoarchitectures is introduced, which can be brought into mechanical resonance via electric AC fields. Specifically, this study focuses on the 3D nanostructure synthesis, the subsequent determination of Young's modulus, and demonstrates a postgrowth procedure, which can precisely tune the material modulus. As‐fabricated resonators reveal a Young's modulus of 9–13 GPa, which can be increased by a factor greater than 5. Next, the electric readout of the resonance behavior is demonstrated via electric current measurement as an essential element for the resonance sensor applications. Finally, the implications of gas‐physisorption and gas‐chemisorption on the resonance frequencies are studied, representing a proof‐of‐principle for sensing applications by the here presented approach. 相似文献
99.
Yi Ke Stephan Lany Joseph J. Berry John D. Perkins Philip A. Parilla Andriy Zakutayev Tim Ohno Ryan O'Hayre David S. Ginley 《Advanced functional materials》2014,24(19):2875-2882
The increase of the band gap in Zn1‐xMgxO alloys with added Mg facilitates tunable control of the conduction band alignment and the Fermi‐level position in oxide‐heterostructures. However, the maximal conductivity achievable by doping decreases considerably at higher Mg compositions, which limits practical application as a wide‐gap transparent conductive oxide. In this work, first‐principles calculations and material synthesis and characterization are combined to show that the leading cause of the conductivity decrease is the increased formation of acceptor‐like compensating intrinsic defects, such as zinc vacancies (VZn), which reduce the free electron concentration and decrease the mobility through ionized impurity scattering. Following the expectation that non‐equilibrium deposition techniques should create a more random distribution of oppositely charged dopants and defects compared to the thermodynamic limit, the paring between dopant GaZn and intrinsic defects VZn is studied as a means to reduce the ionized impurity scattering. Indeed, the post‐deposition annealing of Ga‐doped Zn0.7Mg0.3O films grown by pulsed laser deposition increases the mobility by 50% resulting in a conductivity as high as σ = 475 S cm‐1. 相似文献
100.
Liang-Yu Chen Gary W Hunter Philip G Neudeck Dak Knight 《Solid-state electronics》1998,42(12):2209-2214
The surface and interface properties of Pd0.9Cr0.1/SiC Schottky diode gas sensors both before and after annealing are investigated using Auger electron spectroscopy (AES), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). At room temperature the alloy reacted with SiC and formed PdxSi only in a very narrow interfacial region. After annealing for 250 h at 425°C, the surface of the Schottky contact area has much less silicon and carbon contamination than that found on the surface of an annealed Pd/SiC structure. Palladium silicides (PdxSi) formed at a broadened interface after annealing, but a significant layer of alloy film is still free of silicon and carbon. The chromium concentration with respect to palladium is quite uniform down to the deep interface region. A stable catalytic surface and a clean layer of Pd0.9Cr0.1 film are likely responsible for significantly improved device sensitivity. 相似文献