搅拌摩擦对接焊6061铝合金的高周疲劳行为

对6061铝合金进行搅拌摩擦对接焊,其焊接工艺参数为：旋转速度600、800、1000、1200 r/min,前进速度80、100 mm/min,探针插入深度1.85 mm。基于搅拌摩擦焊参数计算得到的能量输入结果表明,在输入能量为196～405 kJ的情况下,接头在297～354 kJ的输入能量范围内有最大的抗拉强度。在不同的应力比（R=0.5,0.3,0.1,-0.3,-0.5）下,将高强度、低强度2种焊接头进行疲劳测试。结果表明,对于这2种焊接头,显微组织特征明显影响其疲劳性能,比如搅拌区、热力影响区（TMAZ）和热影响区。从接头的显微组织、裂纹扩展路径和断裂表面观察等方面对其疲劳强度进行讨论。     

An integrated production-inventory model with reprocessing and inspection

Competitive pressures continually force management to examine cost and quality levels of production systems. In this paper these issues are addressed via a model that synthesizes several potential features of production systems: production processes, quality control procedures, in-process inventory and reprocessing. For any specified inspection configuration the model can be used, for serial production systems, to obtain closed-form expressions for two important decision variables: optimal lot size and reprocessing batch size, which minimize the total system costs. A numerical example highlights the interdependencies and the role of various system features in determining the values of the decision variables and hence in reducing the total costs. The paper also discusses the managerial implications of the model.     

Effect of power variation on wettability and optical properties of co-sputtered titanium and zirconium oxynitride films

The present paper deals with deposition of titanium and zirconium oxynitride films prepared from co-sputtering titanium and zirconium targets by reactive RF magnetron sputtering. The effect of power variation on various properties of the deposited films is analysed. The film gets transformed from amorphous to well crystalline oxynitride films with gradual increase of target powers as observed from XRD graphs. The films exhibit hydrophilic and hydrophobic behaviours depending upon the presence of various phases. Surface energy decreases as the film properties change from hydrophilic to hydrophobic due to greater contact angle values. The optical properties were measured by UV–Vis–NIR spectrophotometer, transmission spectra and bandgap values show variation with respect to change in elemental composition as determined from EDS analysis.     

Impact of interfacial interactions on optical and ammonia sensing in zinc oxide/polyaniline structures

Zinc oxide/polyaniline (ZnO/PANI) hybrid structures have been investigated for their optical and gas sensing properties. ZnO nanoparticles, prepared by the sol–gel method, pressed in the form of pellets were used for gas sensing. The hybrid ZnO/PANI structure was obtained by the addition of PANI on the surface of ZnO. The UV–Vis absorption of the modified pellets show band edge at 363 nm corresponding to ZnO, while a change in the absorption peaks for PANI was observed. The possible interaction between Zn^2?+? of ZnO and NH-group of PANI was confirmed using Raman spectroscopy studies. The results reveal that the hybrid structures exhibit much higher sensitivity to NH $_{{3}}$ gas at room temperature than blank ZnO, which is sensitive to NH₃ gas at higher temperature. This enhancement has been attributed to the creation of active sites on the ZnO surface due to the presence of PANI.     

Biological synthesis and characterization of intracellular gold nanoparticles using biomass of Aspergillus fumigatus

Nanotechnology is emerging as one of the most important and revolutionizing area in research field. Nanoparticles are produced by various methods like physical, chemical, mechanical and biological. Biological methods of reduction of metal ions using plants or microorganisms are often preferred because they are clean, non-toxic, safe, biocompatible and environmentally acceptable. In the present study, Aspergillus fumigatus was used for the intracellular synthesis of gold nanoparticles. Stable nanoparticles were produced when an aqueous solution of chloroauric acid (HAuCl₄) was reduced by A. fumigatus biomass as the reducing agent. Production of nanoparticles was confirmed by the colour change from yellow to pinkish violet after ～ 72 h of reaction. The produced nanoparticles were then characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction spectroscopy (XRD). SEM images of sample revealed that the nanoparticles were spherical, irregularly shaped with indefinite morphology. Biosynthesized gold nanoparticles were in the range of 85·1–210 nm in size. The presence of gold nanoparticle was confirmed by EDS analysis. Crystalline nature and face-centred cubic structure of synthesized gold nanoparticle was confirmed by XRD pattern.     

Diffraction effects and inelastic electron transport in angle‐resolved microscopic imaging applications

We analyse the signal formation process for scanning electron microscopic imaging applications on crystalline specimens. In accordance with previous investigations, we find nontrivial effects of incident beam diffraction on the backscattered electron distribution in energy and momentum. Specifically, incident beam diffraction causes angular changes of the backscattered electron distribution which we identify as the dominant mechanism underlying pseudocolour orientation imaging using multiple, angle‐resolving detectors. Consequently, diffraction effects of the incident beam and their impact on the subsequent coherent and incoherent electron transport need to be taken into account for an in‐depth theoretical modelling of the energy‐ and momentum distribution of electrons backscattered from crystalline sample regions. Our findings have implications for the level of theoretical detail that can be necessary for the interpretation of complex imaging modalities such as electron channelling contrast imaging (ECCI) of defects in crystals. If the solid angle of detection is limited to specific regions of the backscattered electron momentum distribution, the image contrast that is observed in ECCI and similar applications can be strongly affected by incident beam diffraction and topographic effects from the sample surface. As an application, we demonstrate characteristic changes in the resulting images if different properties of the backscattered electron distribution are used for the analysis of a GaN thin film sample containing dislocations.     

Magnetic resonance in superparamagnetic zinc ferrite

In the present work, we have synthesized zinc ferrite nanoparticles by nitrate method. Presence of almost zero value of coercivity and remanence in the hysteresis of these samples shows the superparamagnetic nature at room temperature. Electron paramagnetic resonance spectroscopy performed on these samples in the temperature range 120–300 K indicates the systematic variation of the line-shapes of the spectra with temperature. Both g-value and peak-to-peak linewidth decrease with increase in temperature. The variation of g-values and peak-to-peak linewidth with temperature has been fitted with existing models and we observed different values of activation energies of the spins for both the samples.     

Iron nanoparticles from blood coated with collagen as a matrix for synthesis of nanohydroxyapatite

A simple wet precipitation technique was used to prepare nanobiocomposite containing iron nanoparticles coated with collagen. This nanobiocomposite was used as matrix for the synthesis of nanohydroxyapatite. The physicochemical characteristic studies of the nanohydroxyapatite thus formed were carried out using fourier transform infrared spectroscopy, transmission electron microscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction technique to confirm the formation of hydroxyapatite on iron nanoparticle–collagen complex. The results of the above studies supported the formation of iron nanoparticle–collagen–hydroxyapatite composite. The biological studies such as biocompatibility and hemocompatibility were carried out for nanohydroxyapatite using different cell lines and blood sample. The results of biocompatibility and hemolytic assay revealed that the prepared nanobiocomposite was 100 % biocompatible and hemocompatible. This nanobiocomposite may be used for biomedical application such as injectables for targeted delivery and as scaffold for tissue engineering.     

A theoretical approach for the assessment of intralaminar fracture mode and toughness of multilayered composites

Analytical evaluation of fracture toughness of a multilayered composite laminate was well-established using modified crack closure integral (MCCI) approach based on test data on the failure load. For this purpose the crack initiation direction, which is treated as a branch crack direction for the theoretical prediction, is required. The crack initiation direction in a multilayered composite laminate depends on mode of failure. In the present work, a fracture parameter n ^* is introduced to predict the mode of failure in multilayered composite having a crack and is validated. Analytical relationship for the prediction of fracture toughness of multilayered composite between a base laminate and its constituent sublaminates is also arrived at. With available test data on the toughness of a set of sub-laminates, toughness of base laminate is determined and validated. The present approach is useful in evaluating the load carrying capability of composite structures with defects in the form of cracks and this information is valuable for design.