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101.
Full analysis of triglycerides of natural fats and oils has been investigated by the combination of argentation high performance
liquid chromatography (HPLC) with nonaqueous reversed phase (NARP) HPLC. An infrared detector was used in argentation HPLC,
because it indicated molar responsibility to all triglycerides. After peak trapping with argentation HPLC, each triglyceride
fraction was analyzed with NARP chromatography using the glyceride-selective post-column reactor detector. The results of
the analyses of triglycerides of palm oil and cocoa butter by the proposed method agreed well with those reported earlier. 相似文献
102.
The potential protection of Picea glehnii seedlings from damping-off by seed-epiphytic Penicillium species was investigated. We studied the chemical response of seed-epiphytic Penicillium species (Pen. cyaneum, Pen. damascenum, and Pen. implicatum) to Pythium vexans, a damping-off fungus, in vitro. Penicillium species were cultured singly or cocultured with Pyt. vexans for 14 or 18 d, and mycelial growth, pH of culture filtrate, antifungal activity of the culture filtrate against Pyt. vexans, and the amount of antifungal compound produced by each Penicillium species, were examined. The filtrate of both the single culture of Penicillium and the coculture of Penicillium and Pyt. vexans showed antifungal activity against Pyt. vexans. In a coculture with Pyt. vexans, Pen. cyaneum produced an antifungal compound (patulin) as in the single culture. Pen. damascenum cocultured with Pyt. vexans produced an antifungal compound (citrinin), as it did in the single culture and in larger amounts on day 10. Pen. implicatum produced two antifungal compounds, frequentin and palitantin, and the ratio of frequentin (with higher antifungal activity than palitantin) to palitantin was higher in the coculture with Pyt. vexans than in the single culture. Our results indicate that these Penicillium species have the ability to produce antifungal compounds and to keep antifungal activity under competitive condition with Pyt. vexans. The chemical response of these Penicillium species to Pyt. vexans may contribute to protect P. glehnii seedlings from damage by Pyt. vexans. 相似文献
103.
Thin SiO2 layers were deposited by atomic layer deposition (ALD) using either Bis-dimethylamino-silane (BDMAS: SiH2(N(CH3)2)2) or Tris-dimethylamino-silane (TDMAS: SiH(N(CH3)2)3) precursors. The purpose of this study is to evaluate these precursors for their suitability for ALD of hafnium (Hf)-silicate gate dielectrics. The advantages of these precursors are that the melting points and vapor pressures are moderate. The thickness of SiO2 deposited using ALD process is controlled by the number of growth cycles and the growth rate was different for each precursor, that for BDMAS being 1.5 times that for TDMAS at the same reactor pressure. The carbon impurity in the SiO2 film deposited using BDMAS was about half an order of magnitude less than that using for TDMAS. Furthermore, the carbon impurity was reduced to about the detection limit of secondary ion mass spectrometry after high temperature annealing at 1000 °C during 5 s. 相似文献
104.
Theory of Three-Dimensional Discontinuous Deformation Analysis and Its Application to a Slope Toppling at Amatoribashi, Japan 总被引:1,自引:0,他引:1
Jian-Hong Wu Yuzo Ohnishi Gen-Hua Shi Satoshi Nishiyama 《Canadian Metallurgical Quarterly》2005,5(3):179-195
A three-dimensional (3D) rock slope toppling occurred in a discontinuous rock mass. To simulate the failure process and study the mechanism of this rock failure with contact and large displacement in 3D, a new discrete numerical method has been developed called the 3D discontinuous deformation analysis (DDA). This article first introduces the basic principles and then derives the formulas in detail. Finally, the slope failure simulation is applied as an example to investigate the applicability of this new method to rock slope failure research. The simulation results indicate the advantages of using this new method to study the mechanism of a rock slope failure with 3D behavior. 相似文献
105.
Atsushi Ikeda Tatsuya Suzuki Masao Aida Yasuhiko Fujii Toshiaki Mitsugashira Mitsuo Hara Masaki Ozawa 《Progress in Nuclear Energy》2005,47(1-4):454-461
A novel chromatographic separation technique using a tertiary pyridine type resin has been applied to the partitioning of the trivalent actinides (An) and lanthanides (Ln) and several successful results have been shown. In an alcoholic hydrochloric acid system, the trivalent An were clearly separated from the Ln, while no such group separation was achieved in an alcoholic nitric acid system. On the other hand, the nitric acid system was more effective for the intragroup (i.e. individual) separation of the trivalent An and the Ln than the hydrochloric acid system. On the basis of these results, a novel concept for the partitioning of the trivalent An and Ln using the present separation technique and its flowchart have been proposed with its advantages and disadvantages. 相似文献
106.
Satoshi Izumi Chan Wee Ping Shinsuke Sakai Atsushi Suzuki 《Engineering Fracture Mechanics》2005,72(17):2672-2685
Specimens and fracture test methods for strength analysis of MEMS micromirrors were proposed. Bending and combined loading tests were performed, and torsion strength was estimated from those results. Two-parameter Weibull distribution was used to evaluate the fracture stresses estimated from the FEM model. The resulting scale and shape parameters were 787 MPa and 7.77 for the bending test and 517 MPa and 5.28 for the combined loading test. There was a difference in strength between the results of the bending and combined loading tests. From the load factor analysis, it was found that both geometry and stress distribution have to be considered to estimate the strength of MEMS since flaws are non-uniformly distributed. It was also found that torsional strength can be estimated on the safe side using the results of the combined loading test. 相似文献
107.
SCARA型机械手的鲁棒防振控制 总被引:1,自引:0,他引:1
对SCARA型机械手的防振控制进行研究,提出了两自由度鲁棒控制法,应用μ控制理论设计鲁棒反馈控制器,保证了系统的鲁棒稳定性及鲁棒性能指标;基于模型匹配法设计前馈控制器,组成两自由度控制系统,进一步改善了闭环系统的跟踪特性。仿真研究表明,与传统的PD控制相比,该控制系统能对机械手前端的残留振支进行有效的抑制,取得较好的轨迹跟踪特性。 相似文献
108.
Kobayashi H. Yamamoto T. Ekawa M. Watanabe T. Ishikawa T. Fujii T. Soda H. Ogita S. Kobayashi M. 《IEEE journal of selected topics in quantum electronics》1997,3(6):1384-1391
This paper describes the optimum design, fabrication, and performance of a 1.3-μm multiple-quantum-well (MQW) laser diode monolithically integrated with a tapered thickness spot-size transformer. The dependence of the lasing characteristics on the thickness distribution of the core layer and on the current injection profile of the device were analyzed. This integrated laser with its optimized structure performed at a low threshold current of 22.2 mA, even at 85°C. The integrated spot-size transformer effectively reduced the lateral and vertical far-field FWHM's to 8° and 9°, respectively. A very long lifetime of over 1×105 h was estimated at 85°C and 8 mW under CW operation 相似文献
109.
In order to investigate the effect of atomic oxygen exposure of an aluminum alloy on bubble formation during welding, electron beam welding was performed on the samples exposed to atomic oxygen produced by the oxygen plasma method. The change in the aluminum surface due to the exposure was analyzed by auger electron spectroscopy. Due to the exposure of atomic oxygen, the thickness of the aluminum oxide film increases on the surface, and pores are formed during welding. The pores can be formed by the formation of the Al2O gas through the reaction between the aluminum oxide and aluminum in a high vacuum. 相似文献
110.
Scott L. Huang Matthew T. Bray Satoshi Akagawa Masami Fukuda 《Canadian Metallurgical Quarterly》2004,18(1):2-34
A large scale 105-m-long, 0.9-m-diam chilled pipeline experiment was conducted to assess the response of a production pipeline that transits between unfrozen (seasonally frozen) and permafrost soils in discontinuous permafrost regions. Thermal and heave characteristics of the experiment for a three-year monitoring period are reported. In response to the chilled pipeline, the progressive cooling patterns within the permafrost and unfrozen soils were different, resulting in the development of a thermal boundary at the transition zone between the two thermally different soils. The absolute maximum movement of pipeline was 0.197 m near the thermal boundary, resulting in a differential heave of 0.148 m. Three distinct heave phases were identified within the unfrozen soil. Phase 1 of the first 200 days related to penetration and heave above the groundwater table and was characterized by heave rates between 0.211 and 0.237 mm/day. Phase 2 resulted in increased ice segregation due to interaction of the freez-ing front with the groundwater table. This phase lasted from approximately day200 to day 500 and corresponded to a heave rate from 0.206 to 0.313 mm/day. Phase 3 was characterized by a further decrease in the heave rate to about 0.081 mm/day and lasted from approximately day 500 to day 1,056. 相似文献