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81.
Several methods for the determination of TBA-value were compared with a new direct modification (omitting the previous distillation), using 1-butanol as the sole solvent. The absorbance is measured at 530 nm after heating to 95 degrees C for 120 min, and cooling. The effect of variables was tested by the Youdens ruggedness test (reaction time, temperature, cooling, concentration of sample, thiobarbituric acid, water, heavy metals, antioxidants, chelating agents, bubbling with oxygen or nitrogen). The Lambert-Beers law is valid in the absorbance range between 0.05 and 0.8. The repeatability is better than that of the Dzikowskis procedure and comparable with those of more complicated distillation methods. The standard deviation is in a linear relation with the absorbance (range 0.1-1.0). The method was found satisfactory for evaluating lard, cooking fat, soybean, sunflower, and rapeseed oils in the stage of beginning rancidity. 相似文献
82.
83.
J. R. Díaz-Estrada E. Camps L. Escobar-Alarcón J. A. Ascencio 《Journal of Materials Science》2007,42(4):1360-1368
Deposition of Ti was carried out by laser ablation onto hydroxyapatite porous discs in an Ar atmosphere. Ti nanoparticles
were deposited onto HAp surface in order to modify its roughness and morphology as it is observed by scanning electron microscopy
(SEM) and scanning probe microscopy (SPM). A homogeneous distribution of Ti over the disc surface was corroborated by elemental
mapping. A comparison of the hydroxyapatite hardness before and after deposition was performed using SPM nanoindentation.
Transmission Electron Microscopy (TEM) showed that the Ti nanoparticles obtained were covered by an oxygen shell. It is shown
that surface modifications of the covered HAp by Ti result in better mechanical properties, reducing the possible damage to
the HAp ceramic by friction or impacts as it often happens in meniscus, bone junctions and the inclusion of prosthesis for
human treatments. 相似文献
84.
In this paper we consider A(θ)-stable finite difference methods for numerical solutions of dissipative partial differential equations of parabolic type.
Combining two rational approximation methods with different orders of accuracy, where the lower order method is applied n
0 times (n
0 fixed) at each time step, we prove the existence of a second order method which is contractive for all time steps. Moreover,
we shed light on the conditions on the lower order method which are sufficient (and sometimes necessary) to obtain the optimal
order of accuracy. For the one-dimensional heat equation we construct a family of numerical methods which are contractive
in the maximum norm for all values of the discretization parameters. We also present numerical examples to illustrate our
results.
Received: May 2002 / Accepted: January 2003 相似文献
85.
M. Del C. Ruiz J. A. González J. B. Rivarola 《Metallurgical and Materials Transactions B》2004,35(3):439-448
The mechanism and kinetics of β-Ta2O5 chlorination, mixed with sucrose carbon, have been studied by a thermogravimetric technique. The investigated temperature
range was 500 °C to 850 °C. The reactants and reaction residues were analyzed by scanning electronic microscopy (SEM), X-ray
diffraction (XRD), and Brunauer-Emmett-Teller method for surface area (BET). The effect of various experimental parameters
was studied, such as carbon percentage, temperature, chlorine partial pressure, and flow, use of the multiple sample method,
and carbon previous oxidation. The carbon percentage and previous treatment have an effect on the system reactivity. The temperature
has a marked effect on the reaction rate. In the 500 °C to 600 °C temperature interval, the apparent activation energy is
144 kJ/mol of oxide, while at higher temperatures, the activation energy decreases. With high chorine partial pressures, the
order of reaction is near zero. The kinetic contractile plate model, X=kt, considering carbon oxidation as the controlling stage, is the one with the best fit to the experimental data. A probable
mechanism for the carbochlorination of β-Ta2O5 is proposed: (1) activation of chlorine on the carbon surface, (2) chlorination of Ta2O5, (3) oxidation of carbon, and (4) recrystallization of β-Ta2O5. 相似文献
86.
Talita Moreira de Oliveira Nilda de Fátima Ferreira Soares Rodrigo Magela Pereira Kátia de Freitas Fraga 《Packaging Technology and Science》2007,20(2):147-153
Conservation of food products depends on product quality and packaging suitability. The objective of this work was to develop and evaluate the antimicrobial efficiency of natamycin‐incorporated film in the production process of Gorgonzola cheese. It aims to optimize the production process and increase shelf‐life and food safety for the consumer. Films with different concentrations of natamycin were produced and tested in Gorgonzola cheeses to evaluate its efficiency against Penicillium roqueforti on the cheese surface. Films with 2 and 4% natamycin presented satisfactory results for fungus inhibition and the amount of natamycin released to the cheese was below that allowed by the legislation. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
87.
88.
We present some new lower bounds on the optimal information rate and on the optimal average information rate of secret sharing schemes with homogeneous access structure. These bounds are found by using some covering constructions and a new parameter, the k-degree of a participant, that is introduced in this paper. Our bounds improve the previous ones in almost all cases. 相似文献
89.
90.
Francisco Jos Alguacil Concepcin Caravaca María Isabel Martín 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2003,78(10):1048-1053
The transport of chromium(VI) through a flat‐sheet supported liquid membrane containing Cyanex 921 as a carrier has been investigated. The permeation of the metal is investigated as a function of various experimental variables: hydrodynamic conditions, concentration of chromium(VI) and HCl in the feed phase, carrier concentration and diluent in the membrane and strippant concentration in the stripping phase. The mass transfer coefficient and the thickness of the aqueous boundary layer were calculated from the experimental data. Furthermore, the selectivity of Cyanex 921‐based flat‐sheet supported liquid membrane towards different metal ions and the behaviour of the system against other carriers are presented. Copyright © 2003 Society of Chemical Industry 相似文献