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101.
Soft X‐ray Ptychographic Imaging and Morphological Quantification of Calcium Silicate Hydrates (C–S–H) 下载免费PDF全文
Sungchul Bae Rae Taylor David Shapiro Peter Denes John Joseph Rich Celestre Stefano Marchesini Howard Padmore Tolek Tyliszczak Tony Warwick David Kilcoyne Pierre Levitz Paulo J. M Monteiro 《Journal of the American Ceramic Society》2015,98(12):4090-4095
Morphological details of calcium silicate hydrate (C–S–H) stemming from the hydration process of Portland cement (PC) phases are crucial for understanding the PC‐based systems but are still only partially known. Here we introduce the first soft X‐ray ptychographic imaging of tricalcium silicate (C3S) hydration products. The results are compared using both scanning transmission X‐ray and electron transmission microscopy data. The evidence shows that ptychography is a powerful method to visualize the details of outer and inner product C–S–H of fully hydrated C3S, which have fibrillar and an interglobular structure with average void sizes of 20 nm, respectively. The high‐resolution ptychrography image enables us to perform morphological quantification of C–S–H, and, for the first time, to possibly distinguish the contributions of inner and outer product C–S–H to the small angle scattering of cement paste. The results indicate that the outer product C–S–H is mainly responsible for the q?3 regime, whereas the inner product C–S–H transitions to a q?2 regime. Various hypotheses are discussed to explain these regimes. 相似文献
102.
Xuetao Shi Serge Ostrovidov Yihua Zhao Xiaobin Liang Motohiro Kasuya Kazue Kurihara Ken Nakajima Hojae Bae Hongkai Wu Ali Khademhosseini 《Advanced functional materials》2015,25(15):2250-2259
Engineering living tissues that simulate their natural counterparts is a dynamic area of research. Among the various models of biological tissues being developed, fiber‐shaped cellular architectures, which can be used as artificial blood vessels or muscle fibers, have drawn particular attention. However, the fabrication of continuous microfiber substrates for culturing cells is still limited to a restricted number of polymers (e.g., alginate) having easy processability but poor cell–material interaction properties. Moreover, the typical smooth surface of a synthetic fiber does not replicate the micro‐ and nanofeatures observed in vivo, which guide and regulate cell behavior. In this study, a method to fabricate photocrosslinkable cell‐responsive methacrylamide‐modified gelatin (GelMA) fibers with exquisite microstructured surfaces by using a microfluidic device is developed. These hydrogel fibers with microgrooved surfaces efficiently promote cell encapsulation and adhesion. GelMA fibers significantly promote the viability of cells encapsulated in/or grown on the fibers compared with similar grooved alginate fibers used as controls. Importantly, the grooves engraved on the GelMA fibers induce cell alignment. Furthermore, the GelMA fibers exhibit excellent processability and could be wound into various shapes. These microstructured GelMA fibers have great potential as templates for the creation of fiber‐shaped tissues or tissue microstructures. 相似文献
103.
Magnificent elongation of bridge span length, especially of recently constructed cable stayed bridges and suspension bridges, can be achieved by technological as well as new material development of orthotropic steel deck systems. One such effort is to install curved bulkhead plates inside longitudinal u-ribs, which was analytically and experimentally demonstrated to reduce significant amount of concentrated stresses without sacrificing self-weight of the whole structure. In this paper, the optimal shape of more effective bulkhead plates is characterized by computational analysis. And it is verified from fatigue tests of a 3-dimensional full-scale structure that the fatigue performance can be significantly improved by installing the optimal bulkhead plates and by fabricating the structure out of recently developed high performance steel for bridges. 相似文献
104.
Joung Hyun La Ki Tae Bae Sang Yul Lee Myung Kon Song Kyung Hoon Nam Yong Hwa Jung 《Journal of Mechanical Science and Technology》2016,30(10):4417-4421
For the purpose of utilizing induction heating in the evaporation process, the effects of induction coil design and droplet size on induction heating efficiency are investigated. Electro-magnetic simulations with various induction coil designs were conducted to predict the electro-magnetic field distribution. The induction coils were fabricated in order to verify the simulation results under atmospheric evaporation test conditions. The electro-magnetic simulation results indicated that the magnetic field became widened around the Zn droplet when the size of the Zn droplet increased. This in turn attributed to the increase in induction heating energy efficiency. The energy efficiency of the induction coil with 4-windings was the highest among the 3-, 4-, and 5-windings induction coils. Energy efficiency tendencies derived by the atmospheric evaporation tests corresponded well to the simulation results, and maximum energy efficiency was measured to be 42% under the atmospheric evaporation tests. 相似文献
105.
Moon Jae-Sung Kim Choonghyun Youm Youngil Bae Joonbum 《Journal of Mechanical Science and Technology》2018,32(5):2289-2298
Journal of Mechanical Science and Technology - This paper presents the design and modeling of the UNI-Copter, a portable spherical unmanned aerial vehicle (UAV) that is powered by a single rotor.... 相似文献
106.
A thermally cured epoxy‐siloxane hybrid material that is curable at low temperature (L‐expoxy hybrimer) was investigated for use as an LED encapsulant. This new hybrimer was fabricated using thermally initiated, cationic polymerization of cycloaliphatic epoxy oligosiloxane (CAEO) resin, derived from non‐hydrolytic sol – gel, mixed with oxetane hardener in the presence of a hexafluoroantimonate‐type thermo‐cationic initiator. The L‐epoxy hybrimer was cured at a lower temperature (below 120 ° C) than previously reported for an epoxy hybrimer with anhydride hardener (above 180 ° C). The L‐epoxy hybrimer showed high thermal resistance to yellowing under long‐term high temperature condition, and maintained good optical transmittance. Also, it had a high refractive index (up to 1.57), as well as the hardness (Shore D 80), and low water‐vapor permeability, w hen the new hybrimer was used to encapsulate an LED, it showed good adhesion without cracks or delamination and maintained their initial performance after the long‐term aging tests (120 and 85 ° C at 85% humidity). © 2013 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2014 , 131, 39968. 相似文献
107.
The electric field induced microdomain orientations has been an interesting research topic. In this article, the effect of nanoparticle surface functionality on microdomain alignments in block copolymer/nanoparticle hybrid thin films was investigated with transmission electron microscopy experiments. The presence of gold nanoparticles influenced the microdomain orientation behaviors of block copolymer/nanoparticle thin films. The possibility for complete alignment normal to the substrate was illustrated by controlling electric field strength, concentration, and surface ligands of nanoparticles. This work provides basic and essential data to understand the properties and behaviors of emerging block copolymer/nanoparticle hybrid thin films. 相似文献
108.
Ik-Hwan Han Chanmi Jeong Juwon Yang Seung-Hyeok Park Deok-Sang Hwang Hyunsu Bae 《International journal of molecular sciences》2022,23(6)
Melanoma is an immunogenic tumor and a serious type of skin cancer. Tumor-associated macrophages (TAMs) express an M2-like phenotype and are involved in all stages of melanomagenesis; it is hence a promising target for cancer immunotherapy. We herein investigated whether melittin–dKLA inhibits the growth of melanoma by inducing apoptosis of M2-like macrophages. For the in vitro study, a conditioned medium of macrophages was prepared from M0, M1, or M2-differentiated THP-1 cells with and without melittin–dKLA. The affinity of melittin for M2 macrophages was studied with FITC (fluorescein isothiocyanate)-conjugated melittin. For the in vivo study, murine melanoma cells were inoculated subcutaneously in the right flank of mice, melittin–dKLA was intraperitoneally injected at 200 nmol/kg every three days, and flow cytometry analysis of TAMs was performed. Since melittin binds preferentially to M2-like macrophages, melittin–dKLA induced more caspase 3 expression and cell death in M2 macrophages compared with M0 and M1 macrophages and melanoma cells. Melittin–dKLA significantly inhibited the proliferation and migration of M2 macrophages, resulting in a decrease in melanoma tumor growth in vivo. The CD206+ M2-like TAMs were reduced, while the CD86+ M1-like TAMs were not affected. Melittin–dKLA is therapeutically effective against melanoma by inducing the apoptosis of M2-like TAMs. 相似文献
109.
Hee-Kyun Shin Hyunho Shin Shin-Tae Bae Sangwook Lee Kug Sun Hong 《Journal of the American Ceramic Society》2008,91(1):132-138
Microstructural evolution and microwave dielectric properties of liquid-phase-sintered 0.9MgTiO3 –0.1CaTiO3 dielectric ceramic material have been investigated as a function of oxygen partial pressure ( ) during sintering. Sintering in a weakly reducing atmosphere ( =10−14 atm) generally increased the density, permittivity, quality factor ( Q × f ), and the temperature coefficient of resonance frequency (τf ), but further reducing atmosphere down to of 10−14 atm generally decreased Q × f and τf . When the 5 wt% lithium borosilicate glass-added specimen was sintered at 950°C and =10−14 atm, it demonstrated a permittivity of 18.8, Q × f of 19 000 GHz, and τf of 10 × 10−6 K−1 . 相似文献
110.
The formation of covalent bonds between silanols in copolymer and those in silica prevents organic–inorganic phase separation. Two series of hybrid composite materials, poly(vinyl acetate‐co‐vinyl trimethoxysilane)/TEOS and poly[vinyl acetate‐co‐3‐(trimethoxysilyl)propyl methacrylate]/TEOS, were fabricated using a modified sol‐gel process. The hybrids were transparent. Two kinds of silane coupling agents, vinyl trimethoxysilane (VTS) and 3‐(trimethoxysilyl)propyl methacrylate (γ‐MPS), were used to prevent macrophase separation through formation of covalent bonds. Thermal analysis showed that γ‐MPS was more effective than VTS for the formation of covalent bonds. Enhancement of thermal stability of the hybrids was investigated by thermogravimetric analysis. Photomicrographs of scanning electron microscopy and images of atomic force microscopy indicated that inorganic silica particles were homogeneously dispersed in less than 50 nm in organic matrix. The morphological properties of hybrids were strongly dependent on the organic–inorganic composition. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 2310–2318, 2001 相似文献