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81.
82.
Min Jeong Noh Tae Gyun Kim In Kwon Hong Ki-Pung Yoo 《Korean Journal of Chemical Engineering》1995,12(1):48-55
A new transparent microscale circulation-type high pressure equilibrium cell with on-line sampling was devised. With this
apparatus, experimental solubility of molecularly complex species such as steroids (cholesterol, stigmasterol and ergosterol)
and fatty acids (palmitic acid and stearic acid) in supercritical carbon dioxide(sc-C02) were measured. Also, to find an appropriate substance for enhancing both the polarity and the solubility power of the SC-CO2 solvent, we arbitrarily selected three polar substances such as acetone, methanol and water and the effect of these cosolvents
on the solubility of solutes in SC-CO2 are examined. The supercritical phase equilibrium data of solute-cosolvent-sc-CO2 systems were quantitatively correlated using a new equation of state based on the lattice fluid theory incorporated with
the concept of multibody interaction. We found that the addition of tracer amount of acetone or methanol to SC-CO2 enhances the solubility of all solutes about thirty to sixty times when compared with the case of pure sc-CO2 However, for the case of cosolvent water, no further enhancement of the solubility of solutes was realized. Also, the versatile
fittability of the equation of state proposed in this work was demonstrated with the newly measured ternary supercritical
equilibrium data. 相似文献
83.
Production by N-nitroso compounds of O6-alkylguanine (O6-alkylG) in DNA directs the misincorporation of thymine during DNA replication, leading to G:C to A:T transition mutations, despite the fact that DNA containing O6-alkylG:T base pairs is less stable than that containing O6-alkylG:C pairs. We have examined the kinetics of incorporation by Klenow fragment (KF) of Escherichia coli DNA polymerase I of thymine (T) and of cytosine (C) opposite O6-MeG in the template DNA strand. Both T and C were incorporated opposite O6-MeG much slower than nucleotides forming regular A:T or G:C base pairs. Using various concentrations of dTTP, dCTP, or their phosphorothioate (Sp)-dNTP alpha S analogues, or a mixture of dTTP and dCTP, the progress of incorporation of a single nucleotide in a single catalytic cycle of a preformed KF-DNA complex was measured (pre-steady-state kinetics). The results were consistent with the kinetic scheme (Kuchta, R. D., Benkovic, P., & Benkovic, S. J. (1988) Biochemistry 27, 6716-6725): (1) binding of dNTP to polymerase-DNA; (2) conformational change in polymerase; (3) formation of phosphodiester between the dNTP and the 3'-OH of the primer; (4) conformational change of polymerase; (5) release of pyrophosphate. The results were analyzed mathematically to identify the steps at which the rate constants differ significantly between the incorporation of T and C. The only significant difference was the 5-fold difference in the rates of formation of the phosphodiester bond (for dTTP, kforward = 3.9 s-1 and kback = 1.9 s-1; for dCTP, kforward = 0.7 s-1 and kback = 0.9 s-1). These pre-steady-state progress curves were biphasic with a rapid initial burst followed by an apparently steady-state rise. Deconvolution of these curves gave direct evidence for the importance of the conformational change after polymerization by showing that the curves represented the sum of the rapid accumulation of the product of step 3 followed by the slow conversion of that to the product of step 5 (because of the rapidity of the release of pyrophosphate there was no significant accumulation of the product of step 4). The equilibrium constants for each step suggest that the greatest change in the Gibbs free energy occurs at the conformational change after polymerization and that while the formation of the phosphodiester bond to T is slightly exothermic, that to C is slightly endothermic.(ABSTRACT TRUNCATED AT 400 WORDS) 相似文献
84.
本文对采用区内C/I平衡的多区蜂窝CDMA系统下行链路的性能进行分析,给出两种区内C/I平衡算法并比较它们的性能,考虑呈对数正态分布的阴影和R^-4规律的路径损失的综合影响,采用与传统不同的小区平均中断概率来评价系统的性能。 相似文献
85.
水溶性防氧化剂在SMT用印制板上的应用 总被引:1,自引:0,他引:1
水溶性的防氧化剂是一种有机可焊性保护剂。其方法是在印制板完全阻焊、字符层的印刷,并经电检之后,通过表面浸渍在裸铜的贴片位或通孔内形成一种耐热性的有机可焊性膜层。这种有机、可焊、耐热的膜层,膜厚可达0.3-0.5mm,其分解的温度可达约300℃,传统的印制板的热风整平法亦无法满足QFP愈来愈密集的需求,同时也无法满足SMD表面平整度的要求,更无法适应PCB薄型化生产。烷基苯并咪唑的OSP法能弥补这项缺陷,因而在PCB业乃至SMT产业中得到了广泛的应用。 相似文献
86.
锗γ能谱测量中的符合相加修正 总被引:4,自引:1,他引:3
本文介绍了锗γ能谱测量中符合相加修正的原理和方法,给出了修正公式。分别计算了不同几何条件下两个锗探测器对一些放射性核素的符合相加修正因子,估计了符合相加修正因子对活度测量结果的误差贡献。 相似文献
87.
88.
Delay-dependent state estimation for delayed neural networks 总被引:3,自引:0,他引:3
Yong He Qing-Guo Wang Min Wu Chong Lin 《Neural Networks, IEEE Transactions on》2006,17(4):1077-1081
In this letter, the delay-dependent state estimation problem for neural networks with time-varying delay is investigated. A delay-dependent criterion is established to estimate the neuron states through available output measurements such that the dynamics of the estimation error is globally exponentially stable. The proposed method is based on the free-weighting matrix approach and is applicable to the case that the derivative of a time-varying delay takes any value. An algorithm is presented to compute the state estimator. Finally, a numerical example is given to demonstrate the effectiveness of this approach and the improvement over existing ones. 相似文献
89.
本文针对大型储罐罐顶整体桁架结构尺寸大、质量大、易变形的特点,详细介绍了一种切实可行的整体吊装及旋转就位方法。从选定吊装方案入手,阐叙了实现本方法的思路和技术细节,提出了实施过程中的注意事项。实践证明,该方法能保证安装质量,安全、可靠、可行。 相似文献
90.
对国产加氢裂化热高分油管线的弯头开裂原因进行了分析 ,对预防连多硫酸腐蚀提出了相应的防范措施 :选用碳含量 <0 .0 3 %并含有稳定化元素Ti、Nb的奥氏体不锈钢或双相钢 ;控制焊缝硬度不大于HB2 0 0并焊后热处理 ;12CrMo和 15CrMo耐应力腐蚀性能好 ;设备停运后马上进行清洗并用碱液中和 相似文献