热采注汽管线的腐蚀与安全性分析

对两段注汽管材料进行了宏观检察、化学成分、壁厚 与管径测量、光学金相组织、常温机械性能、断口扫描电镜、能谱元素等试验分析.结果表明，注汽管材料的局部腐蚀主要是氧化-氯化腐蚀.强度校核表明，两段注汽管目前的壁厚已不能满足内压P=172 MPa、温度T=354℃的使用条件.     

TiO_2/O-′Sialon界面反应过程

以反应烧结的O-′Sialon和金红石型TiO2为研究对象,设计制备了TiO2/O-′Sialon扩散偶,采用X射线衍射(XRD)、扫描电镜(SEM)及电子探针微区分析(EPMA)等方法,对扩散偶的扩散界面及垂直于界面的断面进行了物相分析、形貌观察及元素面分布分析,并在此基础上探讨了TiO2/O-′Sialon界面反应过程。XRD结果表明:TiO2与O-′Sialon在界面处发生反应生成TiN和SiO2,但在1200℃时扩散反应程度微弱,界面处存在Sm2O3偏析,并且与SiO2生成Sm2Si2O7;SEM照片显示TiO2/O-′Sialon界面处存在不规则硅酸盐熔融层;EP-MA元素面分布分析表明Ti、Si等元素富集于硅酸盐熔融层内,只有微量元素扩散至基体内。综合分析结果得出,TiO2/O-′Sialon界面反应过程可分为三个阶段:物理接触阶段、熔融层形成及元素富集阶段、熔融层增长阶段。     

单晶铜制备HSYV-5e 4×2×0.5数字通讯电缆的性能研究

用自制区域熔炼单晶化设备制备了直径为2.7 mm铜单晶线材,经过冷拔加工至直径为0.51 mm,采用信息产业部生产标准YD/T 1019-2001制成HSYV-5e 4×2×0.5数字通讯实心水平对绞电缆,分别对导体材料为变形单晶铜和普通无氧铜电缆的电气性能进行检测,对比试验结果表明:变形单晶铜比普通无氧铜电缆的直流电阻低4.59%;变形铜单晶电缆对信号的衰减作用有明显的改善;单晶铜线材冷拔变形后显微组织存在变形孪晶和晶界.     

筒形件正旋隆起及旋压力三维有限元模拟分析

应用有限元软件MSC．Marc，对TC4筒形件热旋正旋成形过程进行三维弹塑性有限元模拟研究，建立起正旋成形的三维有限元计算模型，分析了旋压加工中隆起现象，计算了旋压力，得到了工艺参数对隆起及旋压力的影响关系。该模拟计算对于探索复杂的旋压成形规律具有重要意义。     

GROWTH OF Bi(Pb)-Sr-Ca-Cu-O SUPERCONDUCTING WHISKERS

Amorphous Bi(Pb)-Sr-Ca-Cu-O strips of types(1112)and(2212)were made by means ofnon-equilibrium solidification of melt-quenching method,On the surface of glassy strip,theflexible(2212)superconducting whiskers have been obtained.The growth and feature ofsuperconducting whiskers were studied in detail.     

Inhibiting effects of some mercapto-triazole derivatives on the corrosion of mild steel in 1.0 M HCl medium

The effect of some mercapto-triazole derivatives synthesized in the laboratory containing different hetero atoms and substituents in the organic structures on the corrosion and hydrogen permeation of mild steel in 1.0 M HCl was investigated by weight loss and various electrochemical techniques. Results obtained reveal that all the mercapto-triazole derivatives perform excellently as corrosion inhibitors for mild steel in 1.0 M HCl. Potentiodynamic polarization studies have shown that all these compounds suppress both the anodic and cathodic process and they behave as mixed-type inhibitors. Double layer capacitance and charge transfer resistance values were derived from Nyquist plots obtained from AC impedance studies. Changes in impedance parameters are indicative of the adsorption of these compounds on the metal surface. The inhibition efficiency mainly depends on the nature of the investigated compounds. The values of the inhibition efficiency calculated from these techniques are in reasonably good agreement. The extent of reduction of hydrogen permeation current through mild steel surface was studied by the hydrogen electropermeation technique. The adsorption of these compounds on mild steel surface is found to obey Langmuir adsorption isotherm. The free energy of adsorption for inhibiting process was determined on the basis of Langmuir adsorption isotherm.     

激光快速成形Rene′88DT高温合金的时效强化研究

研究了时效时间对激光快速成形后时效硬化镍基高温合金Rene′88DT中沉淀相组织演化和力学性能的影响。发现随时效时间的增加，沉淀相y’略有长大，颗粒之间发生大颗粒吞噬小颗粒的粗化，时效40h后沉淀相颗粒粗化明显。对经不同时间时效后的激光快速成形Rene′88DT试样进行了硬度测试。结果显示，在时效时间为28h时，硬度有一峰值HRC49。在此基础上，采用1165℃，2h固溶、空冷＋760℃，28h时效的热处理工艺对激光快速成形标准拉伸棒样进行了热处理，拉伸结果显示成形件的抗拉强度较激光沉积态提高了400MPa，屈服强度接近同种材料的粉末锻造水平。     

铂钛不溶性阳极研制

主要研究了钛基镀铂工艺,确定了工艺中各种参数值,测定了铂钛不溶性阳极的各种性能.本工艺所得铂钛不溶性阳极耐腐蚀性强,与基体结合力好,镀层厚度2～5μm.     

SolidWorks软件在级进模标准件库建立中的应用

级进模设计中存在大量的标准件，因而级进模CAD系统开发过程中有必要建立具备良好实用性的标准件库。本文介绍了以SolidWorks 2001为开发平台，以VB6．0为编程语言创建级进模CAD系统标准件库的过程。     

防锈油膜在5% Na2SO4溶液中的半导体导电行为

采用电位—电容法及Mott-Schottky分析技术研究了自腐蚀电位条件下防锈油膜在5% Na2SO4溶液中失效过程的导电机制转变行为.防锈油膜在5% Na2SO4溶液中的失效过程存在半导体导电特征，随着浸泡时间的延长，防锈油膜从浸泡初期的p型半导体转变为n型半导体，转变过程中，防锈油膜中出现两个空间电荷过渡层.随着浸泡时间的延长，防锈油膜中的空间电荷层厚度皆逐渐减小，载流子密度则逐渐增加，并且计算了不同转变时期防锈油膜中的电子给体（ND）和电子受体（NA）密度大小.