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A series of novel block polymers of polyurethane (PU) and chitosan have been prepared in two steps. The first step is the preparation of PU prepolymer, obtained from polytetramethylene oxide glycol (PTMO, Mn = 1000), isophrone diisocyanate (IPDI), and 2,2′-dimethylol propionic acid (DMPA), followed by ionizing PU prepolymer with triethylamine (TEA). The second step involves PU chain-extended by water-soluble chitosan of low molecular weight (Mn = 5000) by self-emulsion polymerization method. The sizes of the latex particles, morphology, and copolymer architecture have been characterized by dynamic light scattering (DLS), general tensile test, infrared spectroscopy (IR), surface contact angle measurement, and transmission electron microscopy (TEM). Furthermore, it shows that the addition of chitosan remarkably increases anticoagulative property of PU elastomers confirmed by the recalcification time. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
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Piezoelectric Nanogenerators for Self-Powered Nanodevices 总被引:1,自引:0,他引:1
A novel approach converts nanoscale mechanical energy into electric energy for self-powering nanodevices.In our own work, we've used piezoelectric zinc-oxide nanowire (ZnO NW) arrays to demonstrate a novel approach for converting nanoscale mechanical energy into electric energy. Here, we review the fundamental principle behind the nanogenerator, present an approach for improving its performance, and discuss some of the challenges we face in pushing this technology to reach its potential. 相似文献
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Global adaptive control of nonlinearly parametrized systems 总被引:1,自引:0,他引:1
Xudong Ye 《Automatic Control, IEEE Transactions on》2003,48(1):169-173
In this paper, we consider global adaptive control of nonlinearly parametrized systems in parametric-strict-feedback form. Unlike previous results, we do not require a priori bounds on the unknown parameters, which is as in the linear parametrization case. We also allow unknown parameters to be time-varying provided they are bounded. Our proposed adaptive controller is a switching type controller, in which the controller parameter is tuned in a switching manner via a switching logic. Global stability results of the closed-loop system have been proved. 相似文献
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Optimization of a Ductile-Particle-Toughened Ceramic 总被引:2,自引:0,他引:2
The nature of the interfacial bond has a major effect on the degree of toughening that can be achieved in a ductile-particle-reinforced ceramic-matrix composite. The effect of variation of oxygen partial pressure during fabrication on the bonding in an alumina-nickel composite has been investigated. Calculations suggest that wetting of alumina by nickel should always be accompanied by spinel (NiAl2 O4 formation. A range of microstructures within a single specimen have been produced, however, indicating that wetting occurs more rapidly than spinel formation and that reduction of oxygen partial pressure during the hot-pressing process can prevent spinel formation after wetting has occurred. Within this specimen, interfaces that have been formed under nonwetting conditions or conditions under which spinel formation has occurred are weak, whereas wetting without spinel formation produces chemically strengthened and mechanically interlocked interfaces that lead to crack interaction with the metallic particles and a higher toughening increment than for other microstructures. Subsequent specimens fabricated from preconsolidation-heat-treated powder exhibit favorable microstructures throughout, are tougher, and show more-desirable resistance-curve behavior in double-cantilever-beam tests than specimens produced from unreacted powder. 相似文献
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