硫脲型整合树脂在分析上的应用 Ⅰ.岩样中微量银的中子活化分析

前言银和其他贵金属元素一样,在地壳中比较稀少,按其自然丰度为第67号元素,平均含量仅0.07 ppm。由于地质样品成分非常复杂,为测定其微量银,必须进行严格的化学分离。但是迄今文献中报道的许多分离分法,步骤都相当冗长,一般采用氯化银反     

Assessment of underground cable ratings based on distributed temperature sensing

Numerous power utilities have installed advanced distributed temperature sensing (DTS) systems to measure the temperature of underground cables. This paper presents a general procedure for real-time assessment of underground cable ratings based on DTS. After the identification and location of hot spots on a cable, the cable installation data, load, and DTS-recorded temperature over a period of time are used to estimate soil thermal parameters and assess cable ratings under normal and overloading conditions. In order to accurately estimate soil thermal parameters, a combined technique of the finite-element method and gradient-based optimization is used. The technique was validated in the laboratory and applied to a rating assessment of a 230-kV/500-MVA cable circuit. The assessed continuous and emergency ratings are helpful in improving the operation of this circuit.     

二次型时频分析技术的开发与应用

基于二次型的时频分析是高分辨率时频分析技术的有效方法之一，该项技术能够有效反映时变信号的频谱特性，具有分辨率高、能量集中和跟踪瞬时频率的特点。从时变信号的特点出发，阐述了二次型时频分析技术的基本方法原理，采用正演模型分析验证了该方法的有效性，并在实际地震资料中应用于识别物源方向、划分沉积相带、预测储层结构以及相对厚度等诸多方面，均取得了较好的效果。     

FINITE ELEMENT ANALYSIS OF THE FLOW INDUCED BY ROTATING BLADES IN AN INCOMPRESSIBLE VISCOUS FLUID

Aerodynamic loads on a multi-bladed helicopter rotor in hovering flight were calculated by solving the three-dimensional incompressible Navier-Stokes equations. The rotor wake effects were accounted by the correction of local geometric angle of attack according to a free-wake modeling in addition to an empirical modification for the tip flow effect. The validity and efficiency of the present method were verified by the comparisons between numerical results and experimental data.     

厌氧胶快速渗补技术在汽车发动机上的应用

将金属铜易与过氧化物发生氧化还原反应生成游离基的原理应用于厌氧胶，开发了针时金属零件表面微孔进行局部渗补的实用技术。在相关技术可靠性和工艺可行性得以论证的前提下。将局部渗补技术成功地应用于渗补发动机泄漏缸盖，减少了废品损失，取得了良好的经济效益。     

Effect of storage temperature on phenolics stability in hawthorn (Crataegus pinnatifida var. major) fruits and a hawthorn drink

The stability of five major phenolics, namely (−)-epicatechin (EC), procyanidin B₂ (PC-B₂), chlorogenic acid (ChA), hyperoside (HP) and isoquercitrin (IQ), in hawthorn fruits and a canned hawthorn drink were evaluated during 6 months of storage in the dark at three different temperatures (4, 23 and 40 °C). HPLC with a diode-array detector was used to determine the contents of the individual compounds. The results showed that the studied phenolics in the hawthorn fruits and the drink were both stable at 4 °C and relatively unstable at 23 and 40 °C with varied extents of degradation. At room temperature (23 °C), marked degradations of EC and PC-B₂ were observed in both the fruits and the drink with around 50% and 30% decrease after a 6-month storage, respectively. A more significant decrease of the phenolics was observed at 40 °C, especially for EC and PC-B₂, which were almost completely degraded after a 6-month storage. HP, IQ and ChA were relatively stable at 23 °C, but unstable at 40 °C. Therefore, low-temperature storage is recommended for maintaining the quality and efficacy of hawthorn fruits and its preparations.     

降低过滤机滤饼水分和细粒煤脱水浅析

根据对选煤厂细粒煤样的实验室优化脱水试验、工业试验及分析结果 ,对真空系统、气水分离器和分配头实施了技术改造 ,细粒煤脱水系统的运行状况得到显著改善 :圆盘真空过滤机滤饼水分降到 2 0 %左右 ,脱饼率在 95 %以上 ,每年的直接经济效益可达 30 0多万元     

端羟基聚乳酸微球的制备与降解

以1,4-丁二醇和D,L-乳酸为原料,经缩合聚合法制备了端羟基聚乳酸,并用溶剂挥发法制备了端羟基聚乳酸微球.考察了乳化剂浓度、油水相比例及聚乳酸浓度对微球平均粒径和形貌的影响,并在pH=7.4缓冲溶液中进行了微球的降解.结果表明以二氯甲烷为溶剂,PVA作为乳化剂,室温和600r/min搅拌速度下可制得平均粒径0.5-1.0m的较均匀的、表面平滑的端羟基聚乳酸微球.随着在pH=7.4下降解时间增加,微球表面变得粗糙.     

纸张用有机硅抗水剂的制备

采用氨基硅油、十二烷基三甲氧基硅烷、甲基三乙氧基硅烷配成11种抗水剂,用于纸张的抗水处理.通过渗透法和接触角法测试发现,有机硅抗水剂对实验选择的9种纸张均有明显的抗水效果;其中采用氨基硅油配制的抗水剂效果最好,经其处理的生宣纸与空白样相比,接触角由完全润湿提高到125°,渗透时间由0提高到18 s.最佳应用工艺为:将氨基硅油配制成质量分数为2.041%的甲苯溶液,按照10g/m2的涂布量喷涂于纸张表面,自然晾干3～5天至恒定质量.