强化两相混合的超临界技术制备聚乳酸微粒

针对商品化聚乳酸微球粒径分布较宽难于适用气溶胶给药要求的不足,采用水力空化混合强化超临界流体辅助雾化技术(SAA-HCM)制备聚乳酸(PLA)超细微粒.该技术主要特点是通过在超临界流体和液相进料处引入水力空化混合器,强化两相间的混合.考察SAA-HCM过程混合器压力、温度、沉淀器温度、进料中CO2与液体溶液质量流量比和溶液质量浓度等操作参数对微粒形态和粒径分布的影响,成功制备出球形度较好,粒径分布较窄(1～3μm)的PLA微球.经X射线衍射(XRD)分析和差示扫描量热(DSC)分析显示,与原料PLA相比,微球晶型及热曲线变化不大,但结晶度下降.同时把操作参数与相行为进行关联,探讨了影响颗粒形貌的机理.对比超临界流体辅助雾化法(SAA)的实验结果表明:水力空化的引入能有效强化混合器内的两相传质,混合更好,能制备出适用于气溶胶给药要求的超细微粒.     

Investigation on film cooling characteristics from a row of converging slot-holes on flat plate

Experimental and numerical researches were conducted to investigate the cooling performance of a single row of consoles (converging slot-hole) on a large-scale flat-plate model. The results show that the coolant flow from a row of consoles shows good lateral uniformity of adiabatic effectiveness, with regions of slightly enhanced cooling occurring between the consoles. For the console cooling geometry, the interaction between coolant jet from inclined console and the mainstream flow results in reasonable vo...     

导电涂料的研制

为了获得性能优良的导电涂料 ,采用对比试验和正交试验的方法对导电涂料进行了研究 ,分别对导电涂料的电阻、硬度、耐冲击强度、柔韧性等性能进行了测试 ,经过试验 ,确定了无机导电涂料的最佳配方为 :石墨 10 0g ,铅酸钡 10g ,三氧化二锑 5g ,二氧化钛 35g ,碳化硅 10g ,硅酸盐溶胶 170g。以此配方研制出了一种成本较低、生产工艺简单、具有良好的导电、导热性能的无机导电涂料。     

化学铣切槽液中Na2S的分析

本文采用“碘量法”测定化铣液中的硫化钠，分析结果的准确度和精密度完全能够满足生产要求。     

Research on Action Strategies and Simulations of DRL and MCTS-based Intelligent Round Game

International Journal of Control, Automation and Systems - The reinforcement learning problem of complex action control in multiplayer online battlefield games has brought considerable interest in...     

Fast method for SAR echo simulation of a three-dimensional ground scene

Due to huge calculation of SAR echo simulation of a three-dimensional (3D) ground scene, a fast simulation method is proposed. First, the data of a 3D ground scene are fractionally interpolated based on the Fractional Brownian Motion (FBM) model. Second, the data interpolated are divided into lots of small facets whose precision meets the simulation requirement, the backscattering coefficients of the small facets are calculated. Third, the shaded area is judged by the comparison method of overlook angles. Three parallel levels are analyzed and the kernel function is designed. Finally, the computing method of reduction adding and external thread are also utilized under the framework of GPU in order to get high efficiency. With the methods mentioned above, the imaging result of experimental DEM data verifies the validity and superiority of the proposed method.     

频率响应法研究噻吩在CeY分子筛上的吸附行为

以NaY、液相Ce离子交换改性的Y型分子筛(L-CeY)为研究对象,运用N2吸附、XRD、NH3-TPD和Py-FTIR等实验方法表征两种Y型分子筛的物化性能。采用频率响应技术(FR)和智能重量分析仪(IGA)研究噻吩在两种分子筛上的吸附行为,并考察噻吩在稀土离子改性Y型分子筛上的不同吸附作用模式。结果表明,频率响应技术能够有效识别分子筛孔道内发生的不同传质过程。噻吩在NaY分子筛上的吸附行为较为简单,存在孔道吸附和π电子相互作用两种吸附过程;而在L-CeY分子筛上吸附行为较为复杂,同时存在孔道吸附和"S-M"吸附等多种吸附过程,另外,在高温条件下,还存在复杂的催化反应过程。     

高职学生学习主动性意识的缺失与重塑

分析高职学生的特点和学习主动性意识缺失的症状,从学生的学习自觉自信、教师的课堂教学反思、学校的学生评价机制等方面,对高职学生学习主动性意识的重塑策略进行探讨,并提出相应的对策。     

我国宏观经济与证券市场关系的实证分析--基于名义 GDP 和上证指数发展速度的视角

宏观经济和证券市场的关系一直受到人们的关注,由于数据的选取和研究方法上的不同,导致宏观经济与证券市场的关系存在不同的结论或解释。从名义 GDP 和上证指数发展速度的视角,运用 HP 滤波以及 SVAR 等方法实证研究了宏观经济和证券市场的关系。研究发现：宏观经济和证券市场存在显著的因果关系;短期证券市场的波动是经济偶然性波动的预期,两者之间的滞后期效应与当期效应相互影响;方差分解表明宏观经济对于证券市场的长期贡献度很大。     

Degradability and biocompatibility of bioglass/poly(amino acid) composites with different surface bioactivity as bone repair materials

Bioglass (BG) possesses excellent bioactivity and has been widely used in the manufacture of biomaterials. In this study, a composite with different surface bioactivity was fabricated via in situ melting polymerization by incorporating BG and poly(amino acid) (PAA) at a suitable ratio. The structure of the composite was characterized by Fourier transform infrared spectroscopy and XRD. The compressive strength of the BG/PAA composites was 139 MPa (BG:PAA = 30:70). The BG/PAA composites were degradable, and higher BG in composite showed higher weight loss after 4 weeks of incubation in simulated body fluid. In addition, the BG/PAA composite maintained adequate residual compressive strength during the degradation period. The SEM results showed the differences in surface bioactivities of the composites directly, and 30BG/PAA composite showed thicker apatite layer and higher Ca/p than 15BG/PAA. in vitro MG-63 cell culture experiments showed that the composite was noncytotoxic and thus allows cells to adhere, proliferate, and differentiate. This indicates that the composite has good biocompatibility. The implantations in the bone defects of rabbits for 4 and 12 weeks were studied. The composites had good biocompatibility and were capable of guiding new bone formation without causing any inflammation. The composite may be successfully used in the development of bone implants.