Evaluating the mixing performance of a ribbon blender

This paper investigates the effects of processing and equipment parameters of a ribbon blender (i.e. loading method of lubricant, fill level, blade speed and blade design) on magnesium stearate homogeneity. A core sampling technique is used to obtain at least one hundred samples per sampling event, which are extracted throughout the blender and yield a thorough characterization of the entire bed. The results presented here can be used as a guideline to develop appropriate blending processes and characterization protocols for ribbon blenders.     

大孔径石蜡加氢精制催化剂的制备

采用氨吸附-程序升温脱附(NH3-TPD)、低温N2吸附(BET)、压汞法以及加氢精制活性评价等技术,探索SiO2-Al2O3载体在制备过程中孔结构和表面性质的变化。实验结果表明,采用特殊扩孔剂制备载体,当焙烧温度为700℃时,平均孔径可达到17.3nm,其中孔径大于20nm的孔占总孔体积的13.2%;同时载体表面上的中、强酸中心也全部丧失,均为弱酸中心。采用该载体制备的MoNiP/SiO2-Al2O3石蜡加氢精制催化剂,在MoO3用量减少了约1/4的情况下,比目前工业上使用的催化剂具有更高的脱金属能力和加氢精制活性。     

高压液氨泵出口止回阀的泄漏与维修

简要介绍了尿素装置高压液氨泵出口止回阀的损坏情况，并提出了解决办法。     

Growth of highly orientated strontium barium niobate thin films on Si substrates through the sol–gel process using a K: SBN template layer

We report the growth of highly C-axis orientation of Sr _x Ba_1−x Nb₂O₆ (SBN) thin films on p-type (100) Si substrates by using a potassium-substituted SBN template layer with the sol–gel method. The crystallization of SBN thin films was found closely related to the potassium ion doping concentration and the postannealing temperature of the K-SBN template layer. Secondary ion mass spectrometry analysis showed that potassium elements were accumulated at the interface of the template layer and silicon substrate. SBN films postannealed at 750 °C with K-SBN template layer has a smaller full width at half maximum of X-ray rocking curve of 2.45° than that of 5.40° for the pure SBN films. By introducing a template layer, the surface morphologies of SBN films fabricated on silicon substrate were greatly improved.     

Ring‐opening polymerization of D,L‐lactide by rare earth 2,6‐dimethylaryloxide

Ring‐opening polymerization of D,L ‐lactide (LA) has been successfully carried out by using rare earth 2,6‐dimethylaryloxide (Ln(ODMP)₃) as single component catalyst or initiator for the first time. The effects of different rare earth elements, solvents, monomers and catalyst concentration as well as polymerization temperature and time on the polymerization were investigated. The results show that La(ODMP)₃ exhibits higher activity to prepare poly(D,L ‐lactide) (PLA) with a viscosity molecular weight of 4.5 × 10⁴ g mol^?1 and the conversion of 97 % at 100 °C in 45 min. The catalytic activity of Ln(ODMP)₃ has following sequence: La > Nd > Sm > Gd > Er > Y. A kinetic study has indicated that the polymerization is first order with respect to both monomer and catalyst concentration. The apparent activation energy of the polymerization of LA with La(ODMP)₃ is 69.6 kJ mol^?1. The analyses of polymer ends indicate that the LA polymerization proceeds according to ‘coordination–insertion’ mechanism with selective cleavage of the acyl–oxygen bond of the monomer. Copyright © 2004 Society of Chemical Industry     

Research on Marine Boiler＇s Pressurized Combustion and Heat Transfer

The effect of pressure on combustion and heat transfer is analyzed. The research is based on the basic combustion and heat transfer theorem. A correction for the heat calculation method for pressurized furnace is made on the basis of the normal pressure case. The correction takes the effect of pressurizing into account. The results show that the correction is reasonable and the method is applicable to combustion and heat transfer of the marine supercharged boiler.     

羟基磷灰石涂层人工关节的应用研究

采用人工合成高纯度的羟基磷灰石粉末，喷涂在具有注册证的钛合金和钴铬钼合金人工关节上。通过生物学基础检测、动物实验和临床试用，证明所制作的各种羟基磷灰石涂层人工关节，能诱发骨质生长，起生物固定作用，对治疗丧失功能的骨胳效果甚佳。     

一种高精度的CMOS带隙基准电压源

设计了一种采用0.25 μm CMOS工艺的高精度带隙基准电压源.该电路结构新颖,性能优异,其温度系数可达3×10-6/℃,电源抑制比可达75 dB.还增加了提高电源抑制比电路、启动电路和省功耗电路,以保证电路工作点正常、性能优良,并使电路的静态功耗较小.     

LED交通信号灯系统的硬件设计

LED交通信号灯是传统交通信号灯的理想换代产品,文中介绍了一种LED交通信号灯系统的硬件设计方案,利用电流环具有光电隔离、抗干扰能力强、通信距离远的优点,结合串行移位、串并转换的数据传输方式,实现了对信号灯的远程弱电控制,并且能够直接实现倒计时显示功能.系统连线简单、安装方便、功能扩充性好,实现了亮度的自动控制.采用这种远程弱电隔离控制方式后,避免了传统的强电控制方式下可控硅容易损坏、系统故障率较高的缺陷,从而可以大大提高系统的可靠性.     

TM1300多媒体DSP的百兆以太网通信接口的设计实现

主要研究TM1300多媒体数字信号处理器(DSP)在pSOS嵌入式操作系统下的100 Mbit/s高速以太网接口的设计与实现.硬件方面,介绍了TM1300系统与RTL8139以太网驱动芯片通过PCI总线互连的实现方式,重点介绍了其中PCI仲裁器的设计和PCI配置空间地址的设置方法;软件方面,介绍了在DSP端内嵌的pSOS操作系统下开发软件驱动RTL8139芯片的方法,重点描述了pSOS的pNA 网络组件的NI接口、RTL8139芯片收发数据的控制方式、驱动程序的发送缓存管理、TM1300访问PCI空间的途径以及内存与数据缓存一致性等要点.最后从速率、可靠性、效率3个方面对实现的以太网通信接口进行了测试,给出了详细的实测结果.测试结果显示,与基于RTL8029芯片开发的以太网接口相比,各项性能均有较大提高.