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91.
La1?xAgxFeO3/halloysites nanotubes (HNTs) nanocomposite was synthesized by sol–gel method. It was characterized by X-ray diffraction, transmission electron microscope, Fourier transform infrared spectroscopy and UV–visible diffused reflectance spectroscopy measurements. The photo-activity of the La1?xAgxFeO3/HNTs nanocomposite was evaluated via degradation of methylene blue (MB) under visible-light irradiation. The results showed that the HNTs with unique pore structure favored the adsorption of organic molecules. Adequate Ag+ doping improved the absorption ability for visible light. The La0.95Ag0.05FeO3/HNTs demonstrated the best photocatalytic performance, which achieved as high as 99 % for MB degradation exposed 2 h irradiation. However,further increasing of Ag+ doping gradually reduced the photocatalytic activity. The nanocomposite catalyst showed outstanding recyclability after eight cycles which still remained up to 90 %.  相似文献   
92.
93.
本文采用光泽度仪对漆膜的60°镜面光泽进行了测量,对产生测量不确定度的因素进行了分析,并对其A类和B类不确定度进行了分别评定,最终获得其测量结果的扩展不确定度。  相似文献   
94.
Rolling texture and its effect on tensile properties of Ti60 alloy plates were investigated in the present study. The plates wereβ-rolled at 1070℃ and(α+β)-rolled at 980℃, using uni-directionally rolling(UDR) and cross-directionally rolling(CDR) processes, respectively.β-rolled plates exhibited weak textures, which were attributed to the dispersive orientations of secondary α during the β→α phase transformation. Strong deformation textures formed in(α+β)-rolled plates as a result of slipping mechanisms: the strong T-type texture in UDR plate was related to {10 1 0}[11 2 0] slipping, while the B-type texture in CDR plate was relevant with {0001}[11 2 0] slip. Strong T-type textures led to anisotropic tensile properties. B-type textures would decrease such an anisotropy. The(α+β)-CDR process was found to be a candidate process for reducing anisotropy of Ti60 alloy plates.  相似文献   
95.
Zan  Wu  Zhang  Qiaochu  Xu  Hu  Liao  Fuyou  Guo  Zhongxun  Deng  Jianan  Wan  Jing  Zhu  Hao  Chen  Lin  Sun  Qingqing  Ding  Shijin  Zhou  Peng  Bao  Wenzhong  Zhang  David Wei 《Nano Research》2018,11(7):3739-3745
Nano Research - A spin-coating method was applied to obtain thinner and smoother PEO/LiClO4 polymer electrolyte films (EFs) with a lower level of crystallization than those obtained using a...  相似文献   
96.
BACKGROUND AND PURPOSE: Mood disorders are common after stroke and may impede physical, functional, and cognitive recovery, making early identification and treatment of potential importance. We aimed to compare the accuracy of the General Health Questionnaire (GHQ-30) and the Hospital Anxiety and Depression (HAD) Scale in detecting psychiatric morbidity after stroke and to determine the most suitable cutoff points for different purposes. METHODS: One hundred five hospital-referred stroke patients completed both the GHQ-30 and HAD Scale 6 months after onset before a blinded psychiatric assessment in which the Schedule for Affective Disorders and Schizophrenia with some supplementary questions was used to determine a DSM-IV (Diagnostic and Statistical Manual of Mental Disorders, Fourth Edition) diagnosis. Measures were compared in terms of sensitivity, specificity, and receiver operating characteristic curves. RESULTS: No significant differences were found between the GHQ-30 and the HAD Scale in identifying those patients with any DSM-IV diagnosis (P=0.95), grouped depression (P=0.56), or anxiety (P=0.25) disorders. The previously recommended cutoff points for identifying "cases" for the GHQ (4/5) and for the HAD Scale (8/9 and 11/12) were found to be suboptimal in this population. CONCLUSIONS: The GHQ-30 and HAD scale exhibited similar levels of sensitivity and specificity. Data are presented, taking into account the "cost" of false-positives and negatives, to allow a choice of cutoff points suitable for differing situations.  相似文献   
97.
Zhu X  Cassidy DT 《Applied optics》1996,35(24):4689-4693
A liquid detection system consisting of a diode laser with multiple short external cavities (MSXC's) is reported. The MSXC diode laser operates single mode on one of 18 distinct modes that span a range of 72 nm. We selected the modes by setting the length of one of the external cavities using a piezoelectric positioner. One can measure the transmission through cells by modulating the injection current at audio frequencies and using phase-sensitive detection to reject the ambient light and reduce 1/f noise. A method to determine regions of single-mode operation by the rms of the output of the laser is described. The transmission data were processed by multivariate calibration techniques, i.e., partial least squares and principal component regression. Water concentration in acetone was used to demonstrate the performance of the system. A correlation coefficient of R(2) = 0.997 and 0.29% root-mean-square error of prediction are found for water concentration over the range of 2-19%.  相似文献   
98.
An electro-optically modulated intensity interrogation method based on tunable waveguide coupled surface plasmon resonance sensors has been proposed. It has been theoretically and experimentally demonstrated that the proposed scheme can enable sensitive measurement of measurand variations. By modulating the refractive index in the waveguide layer, this interrogation method yields modulated signal whose amplitude is related to measurand's refractive index. This amplitude modulated signal offers a higher signal to noise ratio and eliminates additive noise in the sensor system. A preliminary investigation using saline buffers with different NaCl concentrations shows a resolution of 2.3 × 10?6 refractive index unit by our approach. Resolution can be controlled by the amplitude of the applied modulation voltage and can be further enhanced by optimizing the device structure or improving the electro-optical (E-O) coefficient of the E-O material. This approach is simple, stable, and promising for low-cost or multi-channel SPR biosensor applications.  相似文献   
99.
Surgery to reshape the nose with an implant has been a regular procedure for enhancing a patient’s appearance and self-confidence. The purpose of this study was to establish a computed tomography (CT) based three-dimensional assistant plastic surgery systems, which can provide the patients with realistic prediction of their own postoperative appearance in computer and specifically produce a nose implant for an individual patient. Preoperative CT data and 3D reconstruction techniques were employed to generate 3D model of the patient’s skull. 3D collision detection and finite elements model deformation were then applied to simulate nose augmentation surgery and predict postoperative appearance. According to the patient’s expectation, digital models of the nose implants were constantly modified. When the patient is satisfied with the simulated results, custom made silicone implants were produced by a computer controlled device. Accurately regeneration of 3D images and realistic operative simulations could be achieved with this system. The implants produced exactly conformed to the results of simulation. No curving and reshaping were needed during operating. The clinical results extremely matched with the simulations. The system enhances surgeon patient communication and facilitates preoperative planning. It is especially desirable for implant surgery with less guesswork of size, contour, and orientation of the implant. The best chance of optimal results could be achieved.  相似文献   
100.
Segmenting center of interests (COIs) from pictures is an important but highly challenging problem for researchers in computer vision and image processing. The capability of understanding the meanings of pictures by computers can lead to breakthroughs in a wide range of applications including Web image search and online picture-sharing communities. In this paper, a two-level strategy is presented, which consists of a rough segmentation stage and a fine segmentation stage. In the first level, a picture is partitioned into four regions by using a block clustering method based on color and texture features, and the COI within the picture is distinguished from the background according to the principles of photographic composition. This stage aims to determine the approximate region of the target. In the second level, a novel active contour model is established based on shape information and vector method, where the image energy is defined by a hue gradient and the external energy is generated from either a triangular inner force or a supplementary force. This stage tries to extract the boundary of the target accurately. Experimental results on photos downloaded from the Internet show the feasibility and effectiveness of the proposed method.  相似文献   
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