精密恒温消解仪的研制

采用干浴恒温块加热方式及WD-1型温度转换模块,7/2位双积分A/D转换器,研制了一种精密恒温消解仪。控温范围为室温至250℃,控温精密度±3℃。有60个消化孔可同时消化60个样品。用于智力碘口嚼片中碘测定的样品酸消比处理,消化温度130℃,消化时间70分钟,碘测定均值为193.2mg/kg时的标准差为2.59,变异系数1.34％,平均回收率98.4％,检测限0.2μg/L。     

基于AutoCAD的折边肘板参数化实体造型的设计与实现

肘板是钢结构中常用的连接构件,折边肘板经常用于船舶主构件的折边对接中。为了提高折边肘板建模的效率,设计了折边肘板参数化三维实体造型过程;根据造型过程,探讨了肘板轮廓参数化生成及折边信息存储方法;给出了坐标转换及折边旋转算法;研究了面向对象的程序设计方法;以AutoCAD为开发平台,VS.Net为编程环境,ObjectARX为开发工具,实现了面向对象的折边肘板参数化实体造型。     

基于FPGA的MEMS陀螺仪SAR150实时数据采集系统设计

针对传统MEMS陀螺仪输出信息为模拟量且易受干扰、噪声较大的问题,结合SAR150陀螺仪可以直接输出数字信号的特点,提出了一种新型的数字陀螺仪实时数据采集系统;该系统以FPGA为主控制器,通过SPI接口完成对MEMS陀螺仪SAR150的控制与数据的传输,实现了对陀螺仪输出信号的采集、实时传输及存储;通过将所研制的数据采集系统应用于SAR150陀螺仪测量角速率实验,并对测得数据进行误差分析,实验结果表明:数据采集系统采集输出的角速率值与理论值的绝对误差标准差均小于0.2°/s;且该系统的可靠性高、实时性好,为后续的陀螺仪测试及标定奠定了基础,有一定的工程应用价值。     

3-甲基吡啶的合成工艺研究

以离子液体为催化剂,高压釜为反应器,采用三聚乙醛、乌洛托品合成3-甲基吡啶.系统地考查了催化剂种类、原材料摩尔比、反应温度及反应压力的影响,筛选出合适的反应条件.反应的最优条件为:乙基醋酸铵离子液体为催化剂,反应温度200℃,反应压力3.5 MPa,三聚乙醛:乌托洛品=2:1,此时3-甲基吡啶的收率达93％以上.该工艺操作简单,安全性高,产品收率高,适合工业化生产.     

15%联苯菊酯·氟啶虫酰胺悬浮剂防治桃蚜药效试验

为明确15%联苯菊酯·氟啶虫酰胺悬浮剂对桃蚜的田间防效,2017—2018年分别在河南、河北、辽宁3省的不同桃园进行了药效试验。结果表明,15%联苯菊酯·氟啶虫酰胺悬浮剂有效剂量为33.3~37.5 mg/L时对桃蚜防效很好,药后7、14 d的防效均在90%以上,对所有供试桃树安全。建议最好在春季桃蚜初发期至初盛期喷洒用药。     

TiO2/MOFs的制备及污染物降解现状

TiO2是较为成熟的半导体光催化材料,但因TiO2分散性差、量子利用率低、比表面积小、难回收等问题难以工业化.多孔金属有机框架(MOFs)的引入可增强TiO2/MOFs复合材料的光吸收性能,提高电子-空穴对分离效率和提高回收率.基于TiO2/MOFs制备时前驱体添加顺序不同,综述了TiO2/MOFs的3种制备方法(即Ship-in-a-bottle法、Bottle-around-ship法、One-pot法)及TiO2/MOFs光催化机理与性能影响因素,并探讨不同MOFs与TiO2结合的作用机理.最后,对TiO2/MOFs存在的问题提出建议.     

热处理工艺对BT9合金疲劳和高温持久性能的影响

本文研究了不同的热处理工艺对BT9钛合金的疲劳寿命和高温持久强度的影响,并对其组织、断口进行了光学和电子金相分析。指出了获得良好的综合机械性能的热处理工艺,并讨论了在不同区域内疲劳裂纹扩展的方式。     

Effect of ultrasonic power and bonding force on the bonding strength of copper ball bonds

Copper wire, serving as a cost-saving alternative to gold wire, has been used in many high-end thermosonic ball bonding applications. In this paper, the bond shear force, bond shear strength, and the ball bond diameter are adopted to evaluate the bonding quality. It is concluded that the ef/~cient ultrasonic power is needed to soften the ball to form the copper bonds with high bonding strength. However, excessive ultrasonic power would serve as a fatigue loading to weaken the bonding. Excessive or less bonding force would cause cratering in the silicon.     

Synthesis of LaF3 superfine powder by microwave heating method

LaF3 superfine powder was synthesized from La(CH3COO)3 and NH4 F by microwave heating method,using ethanol or pure water as dispersants respectively. The results of XRD and SEM indicate that the superfine powder has high purity, regular particle shape and narrow distribution of granularity. The granularity of the best sample is in the range of 100 -200 nm. The influence of different dispersants on the crystal degree and microstructure was discussed. After the superfine powder was formed into a slice at pressure of 25 - 60 MPa, its electrochemical impedance spectroscopy was tested by electrochemical impedance spectroscopy (EIS) measurement. The result shows that the grain refining of LaF3 powder increases its ionic conductivity. Compared with traditional preparation methods of LaF3 powder, the advantages of microwave heating method were summarized.