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51.
Summary A group of new polyimides has been prepared by solution condensation of 2,6-bis[1-(p-dimethylaminophenylimino)ethyl] pyridine containing pendant NMe2 units and various dianhyrides in N-methylpyrrolidone (NMP). The tridentate (N-N′-N) pydim ligands were prepared by Schiff-base condensation of 2,6-diacetylpyridine and 4-dimethylaminoaniline in the presence of formic acid as catalyst. These polymers were investigated for their extraction capabilities for Zn(II), Mn(II), Cu(II), Cd (II) and Ni(II) and at different pH. Under different conditions enhanced selectivity was observed. Up to 98% quantitative recoveries were observed for all metals. 相似文献
52.
Pablo Esquinazi Miguel A. Ramos Reinhard König 《Journal of Low Temperature Physics》2004,135(1-2):27-38
We discuss the strain dependence of the acoustic properties of amorphous metals in both normal and superconducting states, in the temperature range 0.1 mK<T<1 K. A crossover is found when the strain energy is of the order of the effective interaction energy between tunneling systems at the corresponding temperature. Our results provide clear evidence for the interaction between tunneling systems, whose energy is in quantitative agreement with theoretical expectations, and reveal that without the knowledge of the corresponding strain dependences, the measured temperature dependences below ~50 mK of the acoustic properties of disordered solids are rather meaningless. 相似文献
53.
Matthias Zobel Joachim Denzler Benno Heigl Elmar Nöth Dietrich Paulus Jochen Schmidt Georg Stemmer 《Machine Vision and Applications》2003,14(1):26-34
Abstract. This contribution introduces MOBSY, a fully integrated, autonomous mobile service robot system. It acts as an automatic dialogue-based
receptionist for visitors to our institute. MOBSY incorporates many techniques from different research areas into one working
stand-alone system. The techniques involved range from computer vision over speech understanding to classical robotics.
Along with the two main aspects of vision and speech, we also focus on the integration aspect, both on the methodological
and on the technical level. We describe the task and the techniques involved. Finally, we discuss the experiences that we
gained with MOBSY during a live performance at our institute. 相似文献
54.
Ravi Joshi Jörg Engstler P. Kesavan Nair Prathap Haridoss Jörg J. Schneider 《Diamond and Related Materials》2008,17(6):913-919
Carbon nanotubes (CNTs) have been synthesized using the arc discharge method with a rotating graphite disc as the cathode. Arcing was carried out in open air and without the use of catalysts. The current density was maintained constant through out the experiment, while, the rate of rotation of the cathode and atmosphere under which arcing was carried out were changed during experimentation. Characterization of the samples produced indicates that rotation of the cathode has a significant impact on the quality and yield of the process. It is proposed that rotation of the cathode drags plasma formed between two electrodes away from high temperature region. This results in a sudden quenching of the reactive plasma. The time available for nucleation and growth phenomena is significantly reduced and thus leads to the formation of highly graphitic multi walled CNTs (yield 60%) and traces of double walled CNTs. 相似文献
55.
56.
57.
M Isabel Sánchez de Rojas Julián Rivera Moisés Frías Félix Marín 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(3):209-217
Copper slag is a by‐product generated during smelting to extract copper metal from the ore. The copper slag obtained may exhibit pozzolanic activity and may therefore be used in the manufacture of addition‐containing cements. In this paper the effect of the incorporation of the copper slag in cement is measured. Blends of copper slag with Portland cement generally possess properties equivalent to Portland cement containing fly ash, but very different to the silica fume incorporation. Copper slag and fly ash reduce the heat of hydration more effectively than silica fume in mortars. The replacement of 30% cement by copper slag reduces the flexural and compressive strength in a similar way to fly ash; however, after 28 days, the reduction is less than the percentage of substitution. Hydrated calcium aluminate phases were analysed using scanning electron microscopy (SEM) and X‐ray diffraction (XRD) techniques. The pozzolanic activity of copper slag is similar to that of fly ash and higher than silica fume. In the presence of low water/cement ratios, certain pozzolanic materials produce a very compact cement paste that limits the space available for hydration products, a determining factor in the formation of hydrated calcium aluminates. SEM was found to be a useful analytical technique when aluminates are formed and can be clearly detected by XRD. Copyright © 2008 Society of Chemical Industry 相似文献
58.
Agglomeration and networks in spatial economies 总被引:1,自引:0,他引:1
We consider the parallel developments in the economics of agglomeration and the economics of networks. We explore the complementarities between the productivity benefits of agglomeration and those of network linkages, arguing that networks of actors dispersed over space may substitute for agglomerations of actors at a single point.JEL Classification:
D20, L14, R30 相似文献
59.
60.
Jürgen Schönbeçk 《NTM》2004,12(2):80-99
Thomas Fincke (January 6th, 1561–April 24th, 1656), born in Flensburg (Germany), was one of the very most important and significant scientists in Denmark during the
seventeenth century, a mathematician and astrologer and physician in the beginning of modern science, a representative of
humanism and an influentual academic organizer. He studied in Strasbourg (since 1577) and Padua (since 1583) and received
his M.D. in Basel (1587), he practised as a physician throughout his life (since 1587 or 1590) and became a professor at Copenhagen
(1591). But he was best known because of his Geometriae rotundi libri XIIII (1583), a famous book on plane and spherical trigonometry, based not on Euclid but on Petrus Ramus. In this influentual work,
in which Fincke introduced the terms tangent and secant and probable first noticed the Law of Tangents and the so-called Newton-Oppel-Mauduit-Simpson-Mollweide-Gauss-formula,
he showed himself to be „abreast of the mathematics of his time“.
相似文献