氧化钇纳米粉体材料的制备

以YCl3为原料 ,以Na2 CO3为添加剂 ,聚乙二醇 4 0 0为分散剂 ,首先制备出晶粒细小的碳酸钇前驱体。在 70 0℃焙烧 1h后制得Y2 O3纳米粉体材料 ,经XRD和TEM检测 ,粒径为 5 0nm ,粒度均匀     

一种新型的激光—等离子体辅助化学气相沉积装置的研究

为探索用激光离子体共同辅助化学气相沉积过程以实现室温沉积的可能性，设计并制造了一种新型的ＣＶＤ装置，实际了ＳｉＨ４－ＮＨ３－Ｎ２体系制取Ｓｉ３Ｎ４膜的试验。结果表明，激光和等离子体是可以相互促进，共同辅助ＣＶＤ过程的，且两者均处于较代的能量水平。     

Torsion sensor based on two cascaded long period fiber gratings fabricated by CO2 laser pulse irradiation and HF etching technique respectively

A novel torsion sensor is proposed, which is composed of one long period fibre grating and one asymmetrically corrugated long period fibre grating based on the high-frequency CO₂ laser pulses technology and burning fibre coating and etching cladding technology, respectively. By combing the advantages of the two aforementioned elements, a sensitivity of 331.7 and 310.3 pm/(rad/m) towards clockwise and anticlockwise direction, respectively, is reached in the experiments.     

南沱河堤下采煤数值模拟与河堤加高培厚设计

运用FLAC3D对受百善矿6123首采工作面开采影响而引起的南沱河河堤(以北堤为例)的垂直位移进行数值模拟,得出河堤断面上各监测点的最终下沉量,为河堤的加固和设计加高培厚的断面提供科学依据。     

尖晶石相型LiM_(0.2)Mn_(1.8)O_4(M=Mg、Cd)相的晶格畸变与红外吸收峰频移

通过室温固相法制备了不同元素掺杂的前驱体,并采用分步煅烧法获得了尖晶石型LiMn2O4和LiM0.2Mn1.8O4(M=Mg、Cd)相。采用XRD和FTIR技术就元素掺杂对产物晶格畸变、Mn—O键长和键能强度等微观结构参数和光谱频移现象进行分析。结果表明,不同元素掺杂导致产物产生不同程度的晶格畸变。Mg元素掺杂使晶格收缩,Mn(Ⅳ)—O和Mn(Ⅲ)—O键收缩和键能强度增加,对应吸收峰发生蓝移;Cd元素掺杂使晶格膨胀,Mn(Ⅳ)—O和Mn(Ⅲ)—O键增长和键能强度降低,对应吸收峰发生红移。     

多菌灵抗性基因在球毛壳中的转化

利用PEG方法将多菌灵抗性基因通过质粒pRB129转化到球毛壳原生质体，并在含0.5μg/ml多菌灵浓度下筛选转化子，转化率可达6－7个转化子／μgDNA。转化子可在1000μg/ml多菌灵处理条件下正常生长。将转化子在非选择压力下连续培养10代，其抗性稳定不变。     

无机/有机纳米复合聚酯材料——技术开发和应用市场

层状硅酸盐经过有机化相容处理后,通过聚合插层法或熔体插层法将无机层状硅酸盐与聚酯复合,形成新的层状硅酸盐聚酯纳米复合材料。纳米聚酯的种类包括属于饱和聚酯的PET、PBT、PTT、PCT、PC、PLA及属于不饱和聚酯的各种配方。纳米聚酯材料在塑料、包装、纤维、农业等领域的诸多应用,如塑料啤酒瓶、PET工程塑料、抗茵纤维、回收再生料、纳米PC塑料、抗菌不饱和树脂制品等,使其具有巨大的开发应用价值。     

Effect of postmolding heat treatment on in vitro properties of a polyanhydride implant containing gentamicin sulfate

A polyanhydride implant containing gentamicin sulfate was fabricated using a laboratory-scale injection-molding machine. After injection molding, the implants were subject to heat treatment at 60°C for various time periods with or without nitrogen protection. The impact of this heat treatment on the in vitro properties of the implants including copolymer molecular weights, mechanical properties, and in vitro drug-release profiles was investigated. This heat treatment caused a drastic drop in the molecular weight of the copolymer. Heating without nitrogen protection resulted in the hardening of the implant, but heating in the presence of nitrogen rendered the implant less rigid. It was also found that a faster in vitro drug release profile was shown by implants heated without nitrogen protection and a pronounced slowing down in drug release was exhibited by implants heated with nitrogen protection.     

汽车塑料标牌的表面处理工艺

汽车标牌不仅要求造型美观、字迹图案流畅,而且表面应具有金属的装饰感,同时其耐蚀性和耐候性也必须符合汽车外饰装饰件的要求,如中国第一汽车集团公司汽车外饰件需符合ＴＬ－ＶＷ５２８／Ｂ标准。目前绝大多数汽车标牌都采用塑料立体标牌,其制造工艺流程大体为：注塑...