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Fe-Si机械合金化过程的研究 总被引:2,自引:0,他引:2
采用高能行星球磨的方法研究了原子配比3:1的Fe、Si混合粉末的机械合金化过程。用XRD、TEM、SEM及EPMA对球磨不同时间粉末的结构、组织、形貌、截面进行了分析。结果表明:Fe75Si25混合粉末在球磨的过程中出现两种形态变化,一种是Fe与Si形成层状形态,另一种为Si及Fe—Si合金包覆Fe形成包覆形态;球磨至30h,合金化基本完成;球磨产物为α—Fe(Si)固溶体,颗粒粒径约为1~20μm。利用一个简单的模型来对Fe75Si25混合粉末合金化过程进行了描述。 相似文献
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贝氏体结构及其相变机制一直是人们研究的重点。贝氏体钢是为了获得某种物理、化学或力学特性而有意添加了一定量的合金元素Cr、Nb、Mo、Ti、B等元素,并对杂质和有害元素加以控制的特殊性能钢。我厂进行过一炉低碳贝氏体钢PC80Q试制生产,存在的问题主要是该钢的冲击韧性值很低,为此笔者从冶炼、轧制及热处理整个工艺过程中的关键点进行了研究改进,以求使其性能得到提高。 相似文献
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Hydrothermal preparation and crystal habit of X-zeolite powder 总被引:1,自引:0,他引:1
The preparation of X-zeolite powder was investigatedin hydrothermal system, the crystal growth process of X-zeolite in hydrothermal condition was characterized by means of X-ray diffraction, scanning electron microscope and infrared ray. The results show that X-zeolite powder with uniform granularity and intact crystal shape can be obtained in hydrothermal system of acid-treated stellerite-NaOH-NaAl(OH)4-H2O; the crystallite size is in the range of 2 - 3μm. The best reaction time of hydrothermal preparation is 6 h. The formation phases of X-zeolite crystal are as follows: dissolution of feedstocks → formation of [SiO4]4- and [AlO4]5- tetrahedron, many-membered ring,β cage → formation of crystal nucleus and nano-particle → aggregation growth of nano-particle → coalescence growth of crystallite. The crystal habits of X-zeolite are intimately related with crystallization orientation ofβ cage in crystal and with its coupling stability on every crystal face family. 相似文献
959.
Dynamic grey model of verification cycle and lifecycle of measuring instrument and its application 总被引:2,自引:0,他引:2
Two dynamic grey models DGM (1, 1) for the verification cycle and the lifecycle of measuring instrument based on time sequence
and frequency sequence were set up, according to the statistical feature of examination data and weighting method. By a specific
case, i. e. vernier caliper, it is proved that the fit precision and forecast precision of the models are much higher, the
cycles are obviously different under different working conditions, and the forecast result of the frequency sequence model
is better than that of the time sequence model. Combining dynamic grey model and auto-manufacturing case the controlling and
information subsystems of verification cycle and the lifecycle based on information integration, multi-sensor controlling
and management controlling were given. The models can be used in production process to help enterprise reduce error, cost
and flaw.
Foundation item: Project (70272032) supported by the National Natural Science Foundation of China 相似文献
960.
The solution chemical and optical characteristics of formation of amine-terminated polyamidoamine dendrimer G2.0(NH2-PAMAM G2.0)-Au nanocomposites in the aqueous solution of NH2-PAMAM G2.0 at various mole ratios of Au(III) to NH2-PAMAM G2.0 were studied by both UV-visible spectrometry and fluorospectrometry. The NH2-PAMAM G2.0-Au nanocomposites, with a type of structure in which one Au nanoparticle is surrounded by several NH2-PAMAM G2.0 dendrimers, emit strong bluish violet fluorescence, and are uniform, water soluble and biocompatible as well as
very stable in frozen conditions. The size of gold nanoparticles in the nanocomposites is about 2.5 nm and decreases with
the increase of NH2-PAMAM G2.0 concentration. The NH2-PAMAM G2. 0 plays an important role in acting as host or micro-reactor for Au(III) before Au(III) reduction and acting as dispersant
and stabilizer for gold nanoparticles after Au(III) reduction. Preliminary experiments of cells staining to human embryonic
lung fibroblast cell lines show that the NH2-PAMAM G2.0-Au nanocomposites can be used as optical imaging markers for bioanalyses and medical diagnoses. 相似文献