化学还原法制备纳米铜粉的研究

本文采用KBH4在液相中化学还原CuSO4,并加入KOH和络合剂EDTA ,制得了纳米级的纯净的铜粉 ,通过调整反应物的浓度 ,可以消除Cu2 O等杂质。制备的纳米铜粉还存在一定程度的团聚 ,需试验加入分散剂来改善。     

ZL101合金锶变质效果及热处理工艺的改进

对现场生产的ZLl01合金铸件材质进行了全面分析，针对存在的产品成分不准，变质效果不好，力学性能不合格的问题，通过改进合金的锶变质工艺和热处理工艺，改善了合金的组织和性能，达到了对材料的成分、性能的各项要求。     

我国矿业城市实现可持续发展的途径分析

详细分析我国矿业城市可持续发展所面临的社会、经济、资源和生态环境等问题，提出了我国矿业城市应树立可持续发展目标及其内涵，系统分析矿业城市可持续发展的结构和模式，结合我国矿业城市发展存在的主要问题，以矿业城市可持续发展理念为指导，提出我国矿业城市实现可持续发展的途径及其建议。     

反应离化团束（RICB）法生长CN硬质薄膜

用反应离化团束（ＲＩＣＢ）法，以低分子量聚乙烯为蒸发材料，氨气为反应气体，在ＮａＣｌ（１００）和Ｓｉ（１００）衬底上淀积Ｃ－Ｎ薄膜，透射电子衍射（ＴＥＭ）分析表明薄膜中含有β－Ｃ３Ｎ４晶粒，Ｘ射线光电子谱（ＸＰＳ）和红外吸收谱（ＩＲ）表明存在Ｃ，Ｎ原子的化学键合。     

关于彩色火焰蜡烛的研制

本文阐述了利用焰色反应的原理研制彩色火焰蜡烛，着重分析并解决了在研制工作中出现的几个技术关键，如主燃剂的选取、蜡烛成型和强度、发色剂的选择与用量等．     

冷成型模具低温锌系磷化

研制出适用于冷成型模具高硬度表面的低温锌系磷化工艺。其中磷化液含Zn(H2 PO4 ) 2 ·2H2 O 6 0g/L ,Zn(NO3) 2 ·6H2 O 90g/L ,NaNO2 1.5g/L ,稀土促进剂 0～ 1.0g/L ,游离酸度 4～ 6点 ,总酸度 70～ 75点。该磷化液在 4 0℃下 ,处理 30～ 4 0min后可获得厚约 10 μm的磷化膜。性能测试表明 ,其减摩、润滑性能良好 ,摩擦系数约降 0 .1,与未处理试样相比磨损量下降 96 % ,附着力 1级。     

粘土矿物对低渗透储层性质的影响——以鄂尔多斯盆地三叠系低渗透储层为例

粘土矿物是低渗砂岩储层的主要胶结物，对储层物性及开发过程中储层物性变化趋势有着重要的影响和控制作用。另外，粘土矿物也蕴含着大量沉积环境介质的物理化学信息，认识其自然规律，可以有效地指导预测有利储层，认识和改造油层。以鄂尔多斯盆地砂岩储层中的粘土矿物为研究对象，探讨分析粘土矿物对低渗储层性质的影响，该研究对含油气盆地低渗储层有效开发具有一定的参考价值。     

Microstructure and Mechanical Properties of Heat-treated GeSb_2Te_4 Thin Films

The effect of annealing on microstructure,adhesive and frictional properties of GeSb 2 Te 4 films were experimentally studied.The GeSb 2 Te 4 films were prepared by radio frequency(RF)magnetron sputtering,and annealed at 200℃and 340℃under vacuum circumstance,respectively.The adhesion and friction experiments were mainly conducted with a lateral force microscope(LFM)for the GeSb 2 Te 4 thin films before and after annealing.Their morphology and phase structure were analyzed by using atomic force microscopy(AFM)and X-ray Diffraction(XRD)techniques,and the nanoindention was employed to evaluate their hardness values.Moreover,an electric force microscope(EFM)was used to measure the surface potential. It is found that the deposited GeSb 2 Te 4 thin film undergoes an amorphous-to-fcc and fcc-to-hex structure transition;the adhesion has a weaker dependence on the surface roughness,but a certain correlation with the surface potential of GeSb 2 Te 4 thin films.And the friction behavior of GeSb 2 Te 4 thin films follows their adhesion behavior under a lower applied load.However,such a relation is replaced by the mechanical behavior when the load is relatively higher.Moreover,the GeSb 2 Te 4 thin film annealed at 340℃presents a lubricative property.     

溶胶-凝胶法制备疏水型SiO-2气凝胶

以正硅酸乙酯 (TEOS)为硅源 ,用三甲基氯硅烷 (TMCS)为疏水试剂 ,通过溶胶 凝胶法在室温下制备出疏水型SiO2 气凝胶。用傅立叶变温红外 (FT IR)、扫描电镜 (SEM)、透射电镜 (TEM)和吸水性能对疏水型SiO2气凝胶的结构和性能进行了研究     

Thermal Expansion Behavior of La1—xSrxMn1—yCoyO3—δ Perovskites

The thermal expansion behavior of La1-xSrxMn1-yCoyO3-δ (x=0.2-0.4, y=0.1-0.3) perovskites in air has been investigated. The average linear thermal expansion coefficients increased with increasing Sr content up to 40 mole fraction or Co content up to 30 mole fraction. The expansion is generally attributed to an increase in the average cation radius as some of the cations in the perovskite are reduced in valence when oxygen ions are removed from the structure.