由乙腈一步法制备乙酸丁酯的研究

以丁醇和制备丙烯腈的副产物乙腈为原料 ,采用一步法合成了乙酸丁酯。通过正交实验得到了影响反应的 4种因素。确定了最佳的工艺条件为 :催化剂的量为样品质量的 40 % ;n(CH3CN)∶ n(C4 H9OH) =1∶ 1 .0 5 ;反应温度为 1 0 5℃ ;反应时间为 8h。在此反应条件下 ,乙酸丁酯的收率为 88.8% ,纯度可达 99.5 %。并用气相色谱及红外光谱对产品的纯度进行了表征     

吹风气余热回收锅炉在我厂的应用

介绍了吹风气余热回收锅炉在兖矿鲁南化肥厂的应用情况。实践证明，系统运行稳定，取得了良好的经济效益。     

GALILEO频率结构和信号设计的分析

描述并分析了由欧盟GALILEO信号特别工作组提出的GALILEO全球卫星导航定位系统的频率结构和信号设计。     

用面向对象方法建立人事信息系统

应用先进的面向对象设计方法开发了技术中心人事信息系统，采用E－R数据库建立了数据库逻辑模型，通过VFP语言设计了友好直观的用户使用界面。实践表明，新开发的人事信息系统速度快、容量大，操作性强，对实现信息管理标准化，尤其是人力资源的动态管理和科学决策具有很强的实用性。     

上海东方艺术中心柔性索网体系曲面幕墙安装技术

上海东方艺术中心玻璃幕墙安装在钢架-索网-支撑复杂的钢结构体系上，由立柱横杆、撑杆、钢索组成的空间三维曲面，造型独特别致，对定位测量精度要求高，由于构件刚度小，施工顺序安排及工艺控制对构件安装成型过程的变形和应力影响较大.通过分析比较，介绍了施工顺序和过程控制技术措施，使安装偏差均在5 mm以内。     

Failure analysis used for remanufacturing of steel rolling components

The guide-pieces, used in the process line of steel rolling, were the important components. The guidepieces, which were slide contacting with the rolled-piece, had a high temperature and high speed. The wear was very serious. The results from failure analysis showed that there were three failure forms in the guide-pieces: the first was the wear during heat friction, the second was the heat fatigue under the cycle of deep heating and deep cooling, and the third was the impact rupture. Among them, the wear was the main reason. To the wear of guidepieces, there were four mechanisms, namely abrasive wear, adhesive wear, fatigue wear and corrosion wear. The failure analysis to the guide-piece laid the foundation for its remanufacturing. Foundation item: Project(50235030) supported by the National Natural Science Foundation of China     

Quantitative analysis of Ni effect on CCT diagrams of novel air-cooled bainite steels using artificial neural network models

The quantitative effect of Ni content on continuous cooling transformation （CCT） diagrams of novel air-cooled bainite steels was analyzed using artificial neural network models. The results showed that Ni may retard the high- and medium-temperature transformation and martensite transformation. The results conform to the materials science theories.     

燃烧—气体容量法测定冶金石灰中的二氧化碳

冶金石灰是石灰石经过工业煅烧的产品。其二氧化碳含量低，且经过高温煅烧后基本不含有机物。无需按照《石灰石、白云石化学分析国家标准中二氧化碳的化学分析方法》中用酸进行试样分解，只需在1200℃高温中灼烧，使石灰中残留的或煅烧后吸收空气中二氧化碳而形成的碳酸盐分解，象通常测定含碳耐火材料中二氧化碳那样，采用气体容量法进行测定。