Creep behavior and microstructure evolution of directionally solidified superalloy IC 10 at high temperature

The creep behavior of directionally solidified （DS） superalloy IC 10 was investigated under 192 MPa and 218 MPa at 980 ℃. Under the testing conditions, the marked creep characteristic of the superalloy is that the creep curve has a short primary and secondary stage and a long tertiary stage. Another creep characteristic is that the superalloy has excellent plasticity at high temperature. To study the creep behavior, the microstructure was observed by SEM and TEM. Different from other microstructure of Ni-base superalloys, superalloy IC10 forms incompletely rafted γ＇ phase during the creep processes. To understand the creep deformation mechanism of superalloy IC10, the movement of dislocations was analyzed. The results show that the dislocations moving in the γ matrix and climbing over the γ＇ precipitates is the main deformation mechanism under the experimental conditions.     

反向工程中测量点云配准的新方法

在光学非接触三维测量中，复杂对象的重构需要多组测量数据的配准。为了获得好的配准结果，提出一种新的配准方法——直接误差分析配准方法。该方法基于一种新型的双目CCD光栅投影测量系统进行测量和分析。实验结果表明该测量方法的配准误差大约0．2mm左右．从而证实该方法的可行性。     

Effects of different tempers on precipitation hardening of 6000 series aluminium alloys

By means of Vickers hardness,mechanical property and formability tests,the effects of different tempers on precipitation hardening of 6000 series aluminium alloys for automotive body sheets were investigated.The results indicate that the short-time pre-aging at 170℃makes for subsequent artificial aging precipitation hardening.With the increase of pre-aging time,the artificial aging hardenability increases.The aging hardening rate reaches the maximum when pre-aging time is up to 10 min,and then it decreases.The short-time pre-aging at 170℃benefits sheets to obtain lower strength under delivery condition and consequently to improve stamping formability of automotive body sheets.The effects of different tempers on precipitation hardening are much more obvious than those of the alloying elements.It is a good treatment schedule to perform pre-aging for 5 min at 170℃right after solution treatment.     

固体颗粒介质成形新工艺及变形研究

固体颗粒介质成形新工艺,是采用固体颗粒代替刚性凸模(或弹性体、液体)的作用,对金属板料成形的工艺。固体颗粒介质成形新工艺,即可以解决流体介质、粘性介质的密封难题,又具有内压非均匀分布、便于控制成形、提高材料成形极限、降低投资成本、所得零件表面质量高、成品率高的优点,且固体颗粒无工业污染,可重复使用。该工艺为材料的加工制备提供了新的方法和手段。利用塑性增量理论,对自由变形区任意一点的应变进行了分析,得到了自由变形区任一点的应变及厚度计算公式。采用固体颗粒介质成形工艺,进行板料成形试验,成功试制出多种典型工件;对试验件壁厚分布的计算值和实测值进行了比较,证明理论正确。     

锌粉颗粒形状对机械沉积无结晶镀层结构的影响

以球状锌粉和片状锌粉为原始锌粉借助于机械镀工艺制备了无结晶锌防护层，运用光学显微镜（OM）、扫描电子显微镜（SEM）观察了镀层的结构形貌；采用XRD技术分析了镀层的物相组成；采用贴滤纸法进行了镀层的孔隙率测试。研究结果表明，片状锌粉制备的镀层比球状锌粉制备的镀层表面要平滑、光亮。球状锌粉制备的镀层中锌粉颗粒呈紧密堆积，部分锌粉颗粒发生塑性变形；片状锌粉制备的镀层中的锌粉颗粒呈层片状叠加，镀层中锌粉颗粒没有发生明显塑性变形。两种形状锌粉制备的镀层均为锌基多相混合体系，镀层中没有固溶体、化合物等合金相产生，属于锌基复合镀层。锌粉颗粒形状对镀层中颗粒之间的结合机理没有显著影响，两种镀层中锌粉颗粒间均以机械咬合为主。     

基于变因素集和多语义粒度的用户满意度评价方法研究

文章提出了基于变因素集和多语义粒度的进行用户满意度评价的思想,采用模糊综合评价法构建了基于变因素集和多语义粒度的用户满意度评价模型,并给出了相应的应用实例.该方法充分考虑到用户的多样性,体现了以用户为中心的思想,使得评价的结果更加准确可靠.     

建筑安全管理与评价中的有关问题探讨

针对施工企业的性质、特点,对危害辨识的方法、步骤作了介绍,对危害危险因素进行了分类。指出危害辨识是进行安全评价和建立职业安全健康体系的基础和关键,应符合企业实际,与企业的经营管理和所采取危险控制措施的能力相适应。     

铝箔轧辊磨削缺陷及磨床精度检测和计算

列举了铝箔轧辊常出现的磨削缺陷。介绍了铝箔轧辊磨床使用中的精度检查和计算，对生产操作有着实际意义。     

Fabrication of niobium doped Pb（Zr, Ti）O3 fibers by viscous polymer processing

A technique based on viscous polymer processing （VPP） was described, which can produce high ceramic content green fibers. PZT-5 ceramic powders were ball milled to get high dispersibility. The slurry prepared for VPP was a composition of PZT-5 powder, PVA binder and glycerin. High ceramic content PZT-5 fibers were extruded with the slurry. The results show that the ceramic powders have fine mean particle size of 0.54 pan, high specific surface area of 3.55 m^2/g and zeta potential of 8.81 mV after 16 h milling. The fibers sintered at 1 280 ℃ for 4 h have pure perovskite structure and grains of 2-5 μm in size, with little pores or cracks. The ultimate tensile strength of sintered fibers is up to 13.84 MPa compared with 2.88 MPa of green fibers. The remnant polarization （Pr） and coercive field （Ec） of the fibers are 50.65 μC/cm^2 and 2.45 kV/mm, respectively. This fiber can withstand an electric field of 9 kV/mm higher than the ceramic （5 kV/mm）, which shows high directional and compact qualities.     

Preparation and photocatalytic activity of nano-TiO2 codoped with fluorine and ferric

Nano-F /Fe^3＋/TiO2 particles were prepared by hydrolysis of tetrabutyl titanate in a mixed CF3COOH-Fe（NO3）3-H2O solution. The photocatalytic decomposition of methylene blue in aqueous solution was used as a probe to evaluate their photocatalytic activities. The powders were characterized by X-ray diffraction （XRD）, energy dispersion X-ray spectrum （EDS） and Brunauer-Emmett-Teller （BET） surface area analysis. The results show that F- and Fe^3＋ are doped into TiO2. The F^- and Fe^3＋ doping can help to enhance the nano-TiO2 photocatalytic activity greatly. The appropriate codoping conditions for F-Fe are n（F）/n（TiO2）=2%, n（Fe）/n（TiO2）=0.05%, and the degradation rate of methylene blue at l h is improved from 73.2% to 87.5%. The codoped nano-F /Fe^3＋/TiO2 particles have higher BET specific surface area, smaller crystallite size and higher photocatalytic activity than those of undoped TiO2 particles.