电石包装桶中乙炔气处理简述

电石在远距离运输过程中，受潮湿，生成乙炔气，遇明火燃烧或发生爆炸。对从业人员造成巨大危害。如何处理包装桶中的乙炔气成为电石产业的物流运输瓶颈。我公司在原来包二化比较实用的氮气置换基础上，逐渐形成了成熟的可使200KG大桶和100KG小桶中各种粒度电石包装桶中乙炔气浓度有效降低的出口电石质量控制体系。     

F离子掺杂TiO2的性能研究

以NH4F为掺杂剂，采用溶胶-凝胶法制备F离子掺杂型TiO2光催化剂，对其进行XRD、XPS和PL表征，结果表明，F离子掺杂ToO2由于Ti—F配位体的形成而能抑制金红石相的生成，同时F离子掺杂能增加TiO2表面缺陷浓度并降低Ti2P键的结合能，另外，由于F离子能取代Ti—OH配位体而降低了表面羟基氧浓度．光催化研究结果表明，F离子掺杂提高了TiO2光催化活性近1．5倍．     

Studies on multilayer film coextrusion III. The rheology of blown film coextrusion

Multilayer blown film coextrusion was studied, both experimentally and theoretically. For the experimental study, an annular die with a feed-port system was designed and multilayer blown films were produced by rotating the inner mandrel with a one horsepower variable-speed drive at speeds from nearly 2 to 6 rpm, and by inflating the tubular molten film with air. The die has 16 feed slots and melt pressure transducers are mounted along the axial direction of the outer wall of the annular flow channel. The transducers were used to determine the pressure gradient in the annular flow channel, which then permitted determination of the reduction in pressure drop when different combinations of two polymer systems were coextruded. Polymers used for b own film coextrusion were: (1) low-density polyethylene with ethylene-vinyl acetate; (2) low-density polyethylene with high-density polyethylene; (3) low-density polyethylene with polypropylene; (4) high-density polyethylene with ethylene-vinyl acetate. For the theoretical study, stratified helical flow was analyzed using a power-law non-Newtonian model. A computational procedure was developed to predict the number of layers, layer thickness, and the volumetric flow rate as functions of certain processing variables (namely, the pressure drop in the die, and the angular speed of rotation of the inner mandrel of the die) and the rheological parameters of the individual polymers concerned. Comparison was made of the theoretical prediction of volumetric flow rate with experimental ones. Some representative results are presented of the theoretically predicted axial and angular velocity distributions, shear stress profiles, and shear rate profiles.     

MACROPROCESS OF PARTICLE FORMATION IN SUSPENSION POLYMERIZATION OF STYRENE WITH INORGANIC STABILIZER SYSTEM

The macroprocess of particle formation from suspension droplets of styrene in a pdymerizationsystem was investigated.Inorganic hydroxyapatite or its mixture with polyvinyl alcohol as thepolymerization system was used.Those items such as the effects of the Weight fraction of dispersed-phase,the amount of the inorganic stabilizer and the agitation speed on the breakup and coalescence of thetransient dispersed drops etc.Were examined.Results showd that the dynamic behavior of the transi-ent polymer droplets changed in the presence of the suspension stabilizer during the reaction.     

混合电解质NaBr+NaAc十H_2O体系的活度系数的测定

用电势法测定了298.15K以及I为0.1、0.5、1.0、1.5、2.0、2.5和3.0 mol/kg时,NaBr在混合电解质溶液NaBr+NaAc+H_2O中的活度系数.实验结果用Harned、SRJ和Pitzer方程拟合,得到各种方程的相互作用参数,由拟合的标准偏差得知,Pitzer方程的拟合精度略好于前2个方程.用Pitzer混合参数θ_(Br-Ac)和ψ_(Br-Na-Ac)计算了NaAc在该混合体系中的活度系数和体系的过量Gibbs自由能.     

棉籽油间歇式酯交换反应动力学的研究

生物柴油(棉籽油甲酯)可以由棉籽油与甲醇在催化剂KOH存在下通过酯交换反应制得。故对棉籽油间歇式酯交换反应动力学进行了研究,并考察了反应温度和催化剂浓度对产物棉籽油甲酯浓度的影响。用液相色谱法分析棉籽油的组成;用气相色谱法分析产物中棉籽油甲酯的含量。由实验数据绘制的动力学曲线得到酯交换反应在开始阶段为准二级反应,以后紧接转为一级反应和零级反应,与文献报导的棕榈油酯交换反应动力学结果一致。由实验数据求出酯交换反应在开始阶段的动力学参数,35℃、45℃时的反应速率常数分别为0.9179Lmol-1min-1和1.049Lmol-1min-1,酯交换反应的活化能为10.88kJmol-1。根据实验结果得到棉籽油酯交换反应的最佳反应温度为45℃,最佳催化剂为1.1%KOH。     

Precise localization of eye centers with multiple cues

Automatic detection and precise localization of human eye centers are the essential processes in photo related multimedia applications. Since eye center points are used as reference base points for further intelligent processing, precise eye center localization is very important. In face recognition the accuracy of localization of eye centers directly influences the identification accuracy. A multiple stage approach with multiple cues for detection and precise localization of eye centers is presented in this paper. Multiple scopes searching strategy is used for correctly extracting eye patch images from the background. Dedicated gradient based features and curvelet based features are constructed and used for comprehensively revealing the intensity distribution characteristics and the edge based texture around eye centers. A rebuilt score calculation mechanism is proposed and the rebuilt scores are used as a specific measurement index reflecting the matching accuracy. The final localizations of eye centers are determined with integrating the gradient based scores and curvelet based scores. The experiment results testing on public face datasets show that the localization accuracy of proposed approach outperforms the accuracy with other state of the art methods.     

压缩机废油回收工艺小结

介绍了压缩机废油回收的原理、工艺及操作要点,达到了节油降耗的目的。     

改性膨润土对甲基橙的吸附

在用Cu^2 A‘^3 Fe^3 对膨润土改性中，Fe^3 改性的膨润土对甲基橙的吸附性能最好，在振荡20分钟后即可达到吸附平衡。pH=3～7、用量为3g／L、25℃时对甲基橙的吸附量达到最大，在pH=7及常温条件下，铁基膨润土的用量为11g／L时，对浓度为250mg／L甲基橙的吸附量和去除率分别为22.2mg／g98．6％；对浓度为40mg／L的甲基橙去除率达97.1％。     

Image Mosaic Techniques OptimizationUsing Wavelet

This essay concentrates on two key procedures of image mosaic--image registration and imagefusion.Becauseof the character of geometric transformation invariance of edge points, wecalculate the angle difference of the direction vector ofedge points in different images anddraw an angle difference histogramto adjust the rotationproblem. Through this way, algorithm based on gray information is expandedandcan be used in images withdisplacementand rotation. Inthe term of image fusion, wavelet multi-scale analysis is used to fuse spliced images. In order to choose the best method of imagefusion,weevaluate the results of different methods of image fusion by cross entropy.