The thermal behavior of mechanically activated galena by thermogravimetry analysis

The thermal decompositions of mechanically activated and nonactivated galenas were studied by thermogravimetry analysis (TGA) at the heating rate of 10 K min⁻¹ in argon. Results indicate that the initial temperature of thermal decomposition (abbreviated as T _di) in the TGA curves for different galenas decreases gradually with increased grinding time. The specific granulometric surface area (S _G), the structural disorder, and the content of elemental sulfur of mechanically activated galenas were analyzed by an X-ray diffraction (XRD) laser particle-size analyzer, XRD analysis, and the gravimetric method, respectively, which shows that the specific granulometric surface area of mechanically activated galenas remains almost constant after a certain grinding time, but the lattice distortions (ε) rise, the crystallite sizes (D) decrease, and the elemental sulfur contents of mechanically activated galenas increase with increased grinding time. The results imply that the decrease of the initial temperature of thermal decomposition in the TGA curves for mechanically activated galenas is mainly caused by the increase of lattice distortions, and the formation of new dangling bonds resulted from the production of elemental sulfur of mechanically activated galenas with increased grinding time. Finally, the differences in the thermal-decomposition reactivity between nonactivated and mechanically activated galenas were also discussed.     

开发稀土铝合金镀层油管的设想

叙述了热浸镀铝钢的镀层组织、耐蚀性能及研究进展，介绍了稀土对铝合金耐蚀性的影响作用，在此基础上提出了开发稀土铝合金镀层油管的设想。     

裂缝性潜山储层地震描述技术

裂缝是潜山油气藏的重要储集层 ,潜山的油气产出与裂缝的发育情况密切相关 ,因此 ,对裂缝发育控制因素和裂缝发育规律进行了分析和探讨。尽管单条裂缝在地震资料上难以识别 ,但是裂缝带在地震资料上有其特征。描述了裂缝储层的地球物理特征 ,并利用测井约束反演技术、吸收系数技术、地震相分类和相干分析技术对潜山储层进行预测。通过在车古 2 0 1潜山的应用实例分析 ,说明以上 4种储层描述技术比较有效     

合成2,4-二叔丁基苯酚工业试验

以离子交换树脂为催化剂，苯酚和甲基叔丁基醚为原料合成2，4-二叔丁基苯酚(简称2，4酚)，合成产物经过滤再经间歇真空精馏精制提纯，得到高纯度的2，4酚成品。成品精馏后釜中残液在酸性白土催化剂的作用下通过歧化反应生成对叔丁基苯酚，再经精馏提纯得到成品对叔丁基苯酚。通过工艺优化，使2，4酚、对叔丁基苯酚形成联产生产工艺，降低了生产原料消耗和成本。     

PH值对化学沉积制备CdS薄膜性质的影响

实验研究了pH值对化学沉积制备CdS薄膜性质的影响。表明：在柠檬酸钠作为络合剂的体系中随着溶液中氨水浓度的提高CdS薄膜会发生相变，从立方相变为六方相，即当氨水浓度为0．31M时，得到立方相的CdS薄膜；而当氨水的浓度大于0．51M时，得到六方相的CdS薄膜。氨水浓度的提高也使得CdS薄膜的形貌有了很大的改善，且制备得到的CdS薄膜从富CA变为富S，但是薄膜仍是n型。氨水浓度对CdS薄膜的光学性质也有很大的影响，随着氨水浓度的提高所得到的CdS薄膜的禁带宽度增大。     

丁基橡胶及卤化丁基橡胶市场分析

根据国内外丁基橡胶和卤化丁基橡胶现状，分析了未来几年的市场需求情况，并对国内丁基橡胶工业的发展提出了建议。     

基于IP视频监控系统云台控制的设计与实现

I2C总线和PCI_XIO是Philips公司最新DSP芯片PNX1302的两个常用接口.文中介绍了采用上述两个接口设计与实现基于IP视频监控系统的云台控制方法以及比较.基于I2C总线的云台控制方法是利用PNX1302 DSP芯片所集成的I2C总线,根据I2C总线的工作原理、传输速率以及云台控制信息比特数少的综合因素考虑实现的.基于PCI_XIO接口的云台控制方法是根据PNX1302 DSP芯片的PCI总线接口为实现8 bit数据传输而特别设计的PCI_XIO接口实现的.     

MHD simulation of high-current subsonic vacuum arc under different distributed axial magnetic fields

Based on two-temperature magnetic hydrodynamic (MHD) model, the influence of saddle-shaped distributed axial magnetic field (AMF, linearly increases along radial position) and bell-shaped distributed AMF (linearly decreases along radial position) on plasma loss and heat flux density to anode in subsonic high-current vacuum arc (HCVA) is simulated and analyzed. According to the simulation results, the saddle-shaped AMF can more effectively inhibit plasma loss from arc column than that of bell-shaped AMF. Comparisons between simulation results and experimental results further verify the correctness of model and simulation.     

催化技术在降低汽油机排放方面的应用

本文介绍了当前催化技术在改善和降低汽油机排放方面的应用情况，指出：催化技术是改善汽油机排放的一种有效措施和重要手段。