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141.
Pınar Şen Fatih Dumludağ Bekir Salih Ali Rıza Özkaya Özer Bekaroğlu 《Synthetic Metals》2011,161(13-14):1245-1254
The new s-triazine-bridged trinuclear Zn(II) and Cu(II) phthalocyanines have been synthesized from the reaction of corresponding anhydrous metal salts, Zn(OAc)2 and CuCl with 4,5-bis(hexylthio)-phthalonitrile and 2,4,6-tris(2-thiophthalonitrile)-s-triazine. The tris phthalonitrile derivative of s-triazine was prepared from the reaction of 4-nitrophthalonitrile and thiocyanuric acid in dry dimethylformamide as solvent using K2CO3 as the base. The same route was applied to prepare the trinuclear Lu(III) phthalocyanine analogue. The conversion of tris phthalonitrile into its isoindoline derivative was accomplished by bubbling ammonia gas through a solution in methanol in the presence of sodium methoxide. The cyclization of two different isoindoline derivatives and 4,5-bis(hexylhthio)-1,2-diiminoisoindoline, with lutetium (III) acetate in dimethylformamide gave trinuclear Lu(III) phthalocyanine. The reaction of this complex with octakis-hexylthio phthalocyanine led to the isolation of tris double-decker Lu(III) phthalocyanine. The structures of the target compounds were confirmed by elemental analysis, UV–vis, IR and MALDI-TOF mass spectroscopies. The d.c. and a.c. conductivities of the phthalocyanine compounds were measured as a function of temperature. The small value of pre-exponential factor suggested the conduction by localized states in the band tails and by localized states near the Fermi level. The temperature dependence of the frequency exponent showed that the conduction in these compounds is due to hopping of charge carriers. The tris double-decker phthalocyanine complex showed well-defined electrochromic behaviour with green-blue and blue-purple colour transitions. 相似文献
142.
The aim of this study is to assist users and to determine how digital proofing systems used in colour management effect print qualities. Also the main theme of this study is to determine the effects of digital proofing systems used in colour management on print quality by artificial neural network (ANN). The R2 values are obtained 0.99702 and 0.99688 for training data as matte and cuated papers, respectively. Similarly, these values for testing data are 0.994707 and 0.99629, respectively. The ANN approach shows greater accuracy for evaluating colour management. Based on the outputs of the study, ANN model can be used to estimate the effects of digital proofing systems used in colour management on print quality with highly confidence. 相似文献
143.
The aim of this paper is to use the simulation of some stochastic processes combined with the stochastic approximation technique, to determine the optimum sequence of moments of time for the reliability control. It is shown that the obtained stochastic approximation control plan is adaptive. 相似文献
144.
An exergy-based thermoeconomic optimization application is applied to a subcooled and superheated vapor compression refrigeration system. The advantage of using the exergy method of thermoeconomic optimization is that various elements of the system—i.e., condenser, evaporator, subcooling and superheating heat exchangers—can be optimized on their own. The application consists of determining the optimum heat exchanger areas with the corresponding optimum subcooling and superheating temperatures. A cost function is specified for the optimum conditions. All calculations are made for three refrigerants: R22, R134a, and R407c. Thermodynamic properties of refrigerants are formulated using the Artificial Neural Network methodology. 相似文献
145.
146.
Ilkay Orhan Murat Kartal Qamar Naz Asma Ejaz Gülderen Yilmaz Yüksel Kan Belma Konuklugil Bilge Şener M. Iqbal Choudhary 《Food chemistry》2007,103(4):1247-1254
Since Salvia species (Lamiaceae) have been recorded to be used against memory loss in European folk medicine, we herein examined in vitro anticholinesterase and antioxidant activities of 56 extracts prepared with petroleum ether, chloroform, ethyl acetate and methanol obtained from 14 Salvia species (Salvia albimaculata Hedge and Hub, Salvia aucheri Bentham var. canescens Boiss and Heldr, Salvia candidissima Vahl. ssp. occidentalis, Salvia ceratophylla L., Salvia cryptantha Montbret and Bentham, Salvia cyanescens Boiss and Bal., Salvia frigida Boiss, Salvia forskahlei L., Salvia halophilaHedge, Salvia migrostegia Boiss and Bal., Salvia multicaulis Vahl., Salvia sclarea L., Salvia syriaca L., Salvia verticillata L. ssp. amasiaca) growing in Turkey. The antioxidant activities were assessed by both chemical and enzymatic methods against 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical-scavenging and xanthine/xanthine oxidase (XO) system generated superoxide anion radical inhibition. Anticholinesterase effect of the extracts was tested against both acetylcholinesterase (AChE) and butyrylcholinesterase (BChE) at concentrations of 0.2 and 1 mg/ml using a microplate-reader assay based on the Ellman method. Most of the extracts did not show any activity against AChE at 0.2 mg/ml, while the chloroform extracts had noticeable inhibition against BChE between 47.7% and 74.7%. The most active extracts at 1 mg/ml for AChE inhibition were observed to be petroleum ether extract of Salvia albimaculata (89.4%) and chloroform extract of Salvia cyanescens (80.2%), whereas ethyl acetate extracts of Salvia frigida and Salvia migrostegia, chloroform extracts of Salvia candidissima ssp. occidentalis and Salvia ceratophylla, as well as petroleum ether extract of Salvia cyanescens were found to inhibit potently BChE (92.2%, 89.6%, 91.1%, 91.3%, and 91.8%, respectively). Particularly, the ethyl acetate and methanol extracts were observed to be highly active against both DPPH and XO. Our data indicates that nonpolar extracts of Salvia species for anticholinesterase activity and the polar extracts for antioxidant activity are worth further phytochemical evaluation for identifying their active components. 相似文献
147.
Onur Şeker Bulent Akbas Jay Shen A. Zafer Ozturk 《The Structural Design of Tall and Special Buildings》2014,23(12):897-928
Steel moment‐resisting frames (SMRFs) are the most common type of structural systems used in steel structures. The first step of structural design for SMRFs starts with the selection of the structural sections on the basis of story drift limitation. ASCE 7 (2010) requires that the inelastic story drifts be obtained by multiplying the deflections determined by elastic analysis under design earthquake forces with a deflection amplification factor (Cd). For special moment‐resisting frames, Cd is given as 5.5 in ASCE 7 (2010). Lower Cd values will increase the overall inelastic response of the structure. On the other hand, the inelastic response of the structure is expected to be less severe when designed for higher Cd values. The performance objective is that the structure should sustain the inelastic deformation demand imposed due to design earthquake ground motions. This study aims at investigating the inelastic seismic response that low‐rise, medium‐rise and high‐rise SMRFs can experience under design earthquake ground motions and maximum considered earthquake (MCE) level ground motions and evaluating the deflection amplification factors (Cd) for SMRFs in a rational way. For this purpose, nonlinear dynamic time history and pushover analyses will be carried out on SMRFs with 4, 9 and 20 stories. The results indicate that the current practice for computing the inelastic story drifts for SMRFs is rational and the frames designed complying with the current code requirements can sustain the inelastic deformations imposed during design earthquake ground motions when seismically designed and detailed. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
148.
Victor Şeremet 《Acta Mechanica》2014,225(3):735-755
This paper is devoted to a new approach for the derivation of main thermoelastic Green’s functions (MTGFs), based on their new integral representations via Green’s functions for Poisson’s equation. These integral representations have permitted us to derive in elementary functions new MTGFs and new Poisson-type integral formulas for a thermoelastic octant under mixed mechanical and thermal boundary conditions, which are formulated in a special theorem. Examples of validation of the obtained MTGFs are presented. The effectiveness of the obtained MTGFs and of the Poisson-type integral formula is shown on a solution in elementary functions of a particular BVP of thermoelasticity for octant. The graphical and numerical computer evaluation of the obtained MTGFs and of the thermoelastic displacements of the particular BVP for an octant is also presented. By using the proposed approach, it is possible to derive in elementary functions many new MTGFs and new Poisson-type integral formulas for many canonical Cartesian domains. 相似文献
149.
Trond Nordfjærn Özlem Şimşekoğlu Hans Brende Lind Stig Halvard Jørgensen Torbjørn Rundmo 《Accident; analysis and prevention》2014
There is currently scant research on the role of transport priorities, risk perception and worry for travel mode use and preferences. The present study aims to examine these factors in relation to mode use and preferences among Norwegian commuters. A web-based survey was conducted in a randomly obtained representative sample of daily commuters in the extended greater Oslo area (n = 690). The results showed that those who prioritized efficiency and flexibility tended to commute by car, while those who prioritized safety and comfort used public (e.g. metro, tram, and train) or active (e.g. walking and cycling) transport. In a free choice scenario, the respondents who prioritized flexibility reported a preference for using a car, whereas those who prioritized safety and comfort preferred public and active transport for their commuter travels. Risk perception of high impact events, such as terrorism and major accidents, as well as risk perception related to personal impact risks (theft, violence etc.) were related to car use on commuter travels. Transport-related worry exerted weak influences on mode use and preferences. Increased speed on rail transport and more frequent departures may be effective in reducing car use on commuter travels. Risk communication should focus on highlighting the low risk of experiencing security and safety issues in the public transport sector, and this message should be complemented by efforts to reduce the probability of negative events affecting public transport. 相似文献
150.
This article is aimed at evaluating three designs of cylindrical-type electrostatic precipitators that might be installed at the output of household boilers in order to reduce the pollution due to burning wood or fossil fuels. The first design is the “standard” precipitator, which consists in a thin copper wire (0.16 mm in diameter), coaxial with a cylindrical aluminum cylinder, 345 mm in length, of constant radius (20 mm). The second and third designs, equipped with a similar wire electrode, are characterized by the same global length, but are divided into three sections, two having the same cross-section as the “standard” precipitator, while the third section, 20 mm in length and located between them, has a smaller radius (11.5 mm). The reduction of the diameter in this central section of the precipitator is done by introducing an aluminum ring, covered by a sleeve made of either aluminum (design #2) or polyvinyl chloride (design #3). Together with the modification of the conditions for mechanical collection of particles, the more intense corona (design #2) or dielectric barrier discharges (design #3) generated in these sections of reduced diameter contribute to a significant increase of precipitation efficiency. 相似文献