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81.
Bader B. Alsulays Ahmed Alalaiwe Saad M. Alshahrani Abdullah S. Alshetaili Sultan M. Alshehri 《Drug development and industrial pharmacy》2018,44(9):1520-1527
The objective of this study was to examine the influence of drug amount and mixing time on the homogeneity and content uniformity of a low-dose drug formulation during the dry mixing step using a new gentle-wing high-shear mixer. Moreover, the study investigated the influence of drug incorporation mode on the content uniformity of tablets manufactured by different methods. Albuterol sulfate was selected as a model drug and was blended with the other excipients at two different levels, 1% w/w and 5% w/w at impeller speed of 300?rpm and chopper speed of 3000?rpm for 30?min. Utilizing a 1?ml unit side-sampling thief probe, triplicate samples were taken from nine different positions in the mixer bowl at selected time points. Two methods were used for manufacturing of tablets, direct compression and wet granulation. The produced tablets were sampled at the beginning, middle, and end of the compression cycle. An analysis of variance analysis indicated the significant effect (p?.05) of drug amount on the content uniformity of the powder blend and the corresponding tablets. For 1% w/w and 5% w/w formulations, incorporation of the drug in the granulating fluid provided tablets with excellent content uniformity and very low relative standard deviation (~0.61%) during the whole tableting cycle compared to direct compression and granulation method with dry incorporation mode of the drug. Overall, gentle-wing mixer is a good candidate for mixing of low-dose cohesive drug and provides tablets with acceptable content uniformity with no need for pre-blending step. 相似文献
82.
Metal spinning is a plastic forming process in which a disk or tube of metal is rotated at high speed and forced onto a mandrel. It is widely used in industry as an efficient, modern and economical production technique. This research proposes to develop a versatile robotic forming method and expand the application areas of robotic manufacturing processes to the metal spinning area. A lathe-type laboratory setup has been built and an industrial robot manipulator has been used to implement the metal spinning process. Experiments have been conducted with enhanced cascaded trajectory tracking algorithms with an add-on vibration suppressor. The potential of the proposed method has been illustrated with extensive case studies using both constant and variable speed trajectory profiles. Analyses for the growth of wrinkles have been performed through the topographical measurements of the products and the forming forces have been inspected. Results indicate that the efficiency of the process can be significantly improved with suitably selected variable speed trajectory profiles and the process parameters. The developed scheme successfully reduces the excessive oscillations of the manipulator during the metal spinning process and it requires no additional hardware to employ. The investigations demonstrate the feasibility of robotic metal spinning using an industrial serial link manipulator. 相似文献
83.
Roghayeh Abbasalipourkabir Aref Salehzadeh Rasedee Abdullah 《Journal of Experimental Nanoscience》2016,11(3):161-174
An in vitro study was conducted to determine the apoptosis induced by tamoxifen (TAM) and TAM-loaded solid lipid nanoparticles (SLNs) in breast cancer cell lines, MCF-7 and MDA-MB231 cells. The effect of free drug and drug-loaded SLN on the cell lines was characterised by cell morphology and cell cycle distribution using phase contrast microscopy, nuclear morphology and flow cytometry, respectively. The results showed that TAM-loaded SLNs have an equally efficient cytotoxic activity against MCF-7 and MDA-MB231 cells, compared to free TAM, and the half maximal inhibitory concentration (IC50) of TAM-loaded SLNs was generally lower than that of free TAM. In the presence of TAM and TAM-loaded SLN, the viability of the both cells diminishes and the cancer cells lose their normal morphological characteristics, detaches, aggregates and later develops apoptotic bodies. Flow cytometry analysis showed that TAM-loaded SLN like the free TAM caused a dose- and time-dependent apoptosis without cell cycle arrest of human breast cancer cells. Therefore, TAM-loaded SLN has great potential in human medicine for the treatment of breast cancers. 相似文献
84.
Supriya Pulparambil Youcef Baghdadi Abdullah Al-Hamdani Mohammed Al-Badawi 《Service Oriented Computing and Applications》2017,11(2):217-232
The most successful enterprises plan its SOA adoption process as a series of maturity stages, where each stage acts as a foundation for the next. Various SOA maturity models (SOAMMs) are available to judge the current level of SOA adoption maturity of an enterprise. However, only a very few models review the formal use of SOA methods in the maturity assessment process. In this work, the SOAMMs are evaluated in terms of how they assess the methodological aspects of SOA adoption at each level of maturity. Based on methodical features, we introduce a set of building blocks for different maturity levels to assist the method engineers in SOA method definition. Welke’s SOAMM is selected as a base model to derive maturity guidelines for SOA methods. This work establishes the role of SOAMM in realizing the true potential of SOA and discusses why CMMI models are inapplicable to assess SOA adoption maturity. The main intention of this work is to develop a conceptual framework that describes the building block of SOA methods at different levels of maturity, including their processes, tools and technologies, and sourcing mechanisms. We adopt a real case study to determine the maturity level of SOA methodology dimension and to demonstrate how SOA adoption maturity can be improved by focusing on the methodical building blocks identified. 相似文献
85.
86.
This work described the preparation of dysprosium oxide, Dy2O3, nanoparticles using the homogeneous precipitation method. Dy3+ ions were precipitated using NaOH solution. The obtained product was filtered, dried, and then calcined for 1 h at the temperature range of 300–700 °C in static air. The calcination temperature of the Dy-precursor was chosen based on its decomposition as indicated by the TGA analysis. The crystalline structure and surface morphology of the calcined solids were studied by X-ray diffraction(XRD), field emission scanning electron microscopy(FE-SEM), transmission electron microscopy(TEM) and X-ray photoelectron spectroscopy(XPS). The obtained results revealed that Dy2O3 with crystallites size of 11–21 nm was formed at 500 °C. Such value increased to 25–37 nm for the sample calcined at 700 °C. 相似文献
87.
88.
Yin Fong Yeong Ahmad Zuhairi Abdullah Abdul Latif Ahmad Subhash Bhatia 《Journal of Porous Materials》2011,18(2):147-157
Propylsulfonic acid-functionalized partially crystalline silicalite-1 materials were synthesized via one step co-condensation
technique by varying the molar ratio of organosilane source, 3-mercaptopropyltrimethoxysilane (3MP) to tetraethylorthosilicate
(TEOS) in the range of 0.05–0.30, and subsequent oxidation of thiol group to propylsulfonic acid using hydrogen peroxide (H2O2). These materials were characterized by X-ray diffraction (XRD), high resolution transmission electron microscopy (HRTEM),
scanning electron microscopy (SEM) and nitrogen adsorption–desorption method. The structure of these materials was determined
by Fourier transform infrared spectroscopy (FT-IR) and 29Si and 13C solid state NMR. XRD results show that % crystallinity of the materials decreased with the increase in 3MP concentration
in the synthesis mixture. Selected area electron diffraction (SAED) showed the presence of crystalline and amorphous phases
in the samples. An amorphous phase was formed when 3MP concentration was 30 mol% of the total silica source. After elimination
of the structure directing agent (SDA) by calcination at 420 °C, thermogravimetric analysis (TGA) shows that the structure
was thermally stable up to 550 °C. Ammonia temperature-programmed desorption (NH3-TPD) shows that the acid capacity of these materials was in the range of 1.19–1.83 mmol H+/g, which shows that these materials could be used as potential heterogeneous acid catalyst. 相似文献
89.
90.
Investigation on the effect of spinning conditions on the properties of hollow fiber membrane for hemodialysis application 下载免费PDF全文
Sumarni Mansur Mohd Hafiz Dzarfan Othman A. F. Ismail Siti Hamimah Sheikh Abdul Kadir Fatmawati Kamal Pei Sean Goh Hasrinah Hasbullah Bee Cheer Ng Mohd Sohaimi Abdullah 《应用聚合物科学杂志》2016,133(30)
Polyethersulfone (PES) hollow fiber membranes were fabricated via the dry‐wet phase inversion spinning technique, aiming to produce an asymmetric, micro porous ultrafiltration hollow‐fiber specifically for hemodialysis membrane. The objective of this study is to investigate the effect of spinning conditions on the morphological and permeation properties of the fabricated membrane. Among the parameters that were studied in this work are air gap distance, dope extrusion rate, bore fluid flow rate, and the take‐up speed. The contact angle was measured to determine the hydrophilicity of the fibers. Membrane with sufficient hydrophilicity properties is desired for hemodialysis application to avoid fouling and increase its biocompatibility. The influences of the hollow fiber's morphology (i.e., diameter and wall thickness) on the performance of the membranes were evaluated by pure water flux and BSA rejection. The experimental results showed that the dope extrusion rate to bore fluid flow rate ratio should be maintained at 1:1 ratio to produce a perfectly rounded asymmetric hollow fiber membrane. Moreover, the flux of the hollow fiber spun at higher air gap distance had better flux than the one spun at lower air gap distance. Furthermore, spinning asymmetric hollow fiber membranes at high air gap distance helps to produce a thin and porous skin layer, leading to a better flux but a relatively low percentage of rejection for BSA separation. Findings from this study would serve as primary data which will be a useful guide for fabricating a high performance hemodialysis hollow fiber membrane. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43633. 相似文献