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51.
Michel Dorbon Pierre Henri Bigeard Jacques Denis Christian Bernasconi 《Petroleum Science and Technology》1992,10(8):1313-1341
As established by several previous works, nitrogen compounds play a prominent role in the evolution of middle distillates containing cracked components, particularly regarding sediment formation and color evolution.
In a first part, this paper describes and compares stability properties of fuel blends using both an accelerated ageing method at 120°C (248°F ) and long term storage methods at 43°C(110°F) -ASTM 0 4625 - and at ambient temperature. Effectiveness of stabilizing additives is also evaluated. In mixtures containing LCOs, insoluble products are formed progressively during ageings, more or less rapidly according to the chemical constitution of the mixtures.
Then, it reports the complete identification of nitrogen compounds using gas chromatography equipped with a selective nitrogen detector and mass spectrometry showing that in light cycle oils, alkyl indoles and carbazoles are the main families.
Evolution of these compounds was followed kinetically during ageings in absence and presence of additives and alkyl indoles appeared as the moat evolutionary.
It appeared that some additives avoided evolutions of alkyl indoles without preventing sediment formation and color evolution. Oxidation mechanism involving nitrogen compounds should not be the only one to explain the storage evolutions of middle distillates.
Hydrotreatment converts all the alkyl indoles of LCO and prevents coloration end deposits in the storage of the mixtures of steaight-run distillates and LCOs. 相似文献
In a first part, this paper describes and compares stability properties of fuel blends using both an accelerated ageing method at 120°C (248°F ) and long term storage methods at 43°C(110°F) -ASTM 0 4625 - and at ambient temperature. Effectiveness of stabilizing additives is also evaluated. In mixtures containing LCOs, insoluble products are formed progressively during ageings, more or less rapidly according to the chemical constitution of the mixtures.
Then, it reports the complete identification of nitrogen compounds using gas chromatography equipped with a selective nitrogen detector and mass spectrometry showing that in light cycle oils, alkyl indoles and carbazoles are the main families.
Evolution of these compounds was followed kinetically during ageings in absence and presence of additives and alkyl indoles appeared as the moat evolutionary.
It appeared that some additives avoided evolutions of alkyl indoles without preventing sediment formation and color evolution. Oxidation mechanism involving nitrogen compounds should not be the only one to explain the storage evolutions of middle distillates.
Hydrotreatment converts all the alkyl indoles of LCO and prevents coloration end deposits in the storage of the mixtures of steaight-run distillates and LCOs. 相似文献
52.
Despite the common use of tapping-mode atomic force microscopy to image composites or polymer blends, very few studies have focused on the measurement of the interdiffusion at an interface between two polymers in contact. In this study, we show how to assess the interphase between two polymers with two methods. First, stable and robust tapping conditions are established, and the problem of the phase contrast is discussed. Second, a contact-resonance method is presented: the tip in contact with the sample is electrostatically excited at its resonance frequency by a self-controlled oscillator. The gain and frequency images allow us to measure the interdiffusion width. Both methods (using high and weak mechanical solicitation) give the same assessment of the interdiffusion width. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
53.
Barrier options are financial derivative contracts that are activated or deactivated according to the crossing of specified
barriers by an underlying asset price. Exact models for pricing barrier options assume continuous monitoring of the underlying
dynamics, usually a stock price. Barrier options in traded markets, however, nearly always assume less frequent observation,
e.g. daily or weekly. These situations require approximate solutions to the pricing problem. We present a new approach to
pricing such discretely monitored barrier options that may be applied in many realistic situations. In particular, we study
daily monitored up-and-out call options of the European type with a single underlying stock. The approach is based on numerical
approximation of the transition probability density associated with the stochastic differential equation describing the stock
price dynamics, and provides accurate results in less than one second whenever a contract expires in a year or less. The flexibility
of the method permits more complex underlying dynamics than the Black and Scholes paradigm, and its relative simplicity renders
it quite easy to implement. 相似文献
54.
Guillaume Bernard-Granger Christian Guizard Ahmed Addad 《Journal of Materials Science》2007,42(15):6316-6324
Sintering in air of an ultra pure α-alumina powder has been investigated. Isothermal experiments have been conducted on green
samples shaped by slip casting. The grain growth and densification kinetics have been established. The “relative density/grain
size” trajectory, called “sintering path”, has been drawn. Hypotheses concerning the mechanisms controlling grain growth and
densification have been formulated. For the first time, it is shown that grain growth and densification kinetics exhibit two
distinct regimes, where an initial point defect formation step plays a key role. When point defects have been generated, the
diffusion of the associated Al3+ cations controls grain growth and densification. 相似文献
55.
Peter Mertens Christian Stary Konrad Walser Thomas Deelmann Franz Lehner Sebastian Günther Christian Scheer 《WIRTSCHAFTSINFORMATIK》2006,48(4):288-295
Ohne Zusammenfassung 相似文献
56.
The influence of ointment formulation on the stability, the in-vitro release and the in-vivo absorption through the skin of rabbits was investigated. The choice of the selected ointments has no influence on the drug stability with the exception of an acidified emulsion base. A good correlation between in-vitro release and in-vivo absorption was found revealing that metronidazole was quickly released and effectively absorbed from a polyethylene glycol base. 相似文献
57.
S. Salar Behzadi Silvester Ölzant Reinhard Länger Christian Koban Frank M. Unger Helmut Viernstein 《European Food Research and Technology》2006,223(2):238-245
Inversion of sucrose is a stability problem particularly of candies with acidic taste that contain sucrose and small amounts of organic acids such as citric acid, since the free d-fructose produced by hydrolysis is hygroscopic. The following possibilities were investigated for preventing the hydrolysis of sucrose in tablets containing sucrose and citric acid: Adding various amounts of tri-sodium citrate to the formulation to neutralize the citric acid, (Hot) melt coating of citric acid and tri-sodium citrate with a vegetable fat at different coating ratios, variation of the ratio of coated citric acid and tri-sodium citrate in formulations, and compressing the formulations with different compression forces. After tablet processing and storage of tablets, the concentration of d-fructose was determined on the basis of enzymatic reactions. A response surface central composite design was used. The above-mentioned variations were chosen as independent variables and the amount of d-fructose was chosen as response variable. The lowest rates of inversion could be achieved by increasing the content of tri-sodium citrate and the ratio of coating material and decreasing the ratio of coated citric acid and tri-sodium citrate in the tablet formulations. The compression force had no significant effect on the inversion of sucrose. 相似文献
58.
59.
60.
Markus Eisele Ralf Kolb Erwin Kraus Christian von Ehrenstein 《Informatik-Spektrum》2007,30(6):407-412
Zusammenfassung Das Schlagwort NetWeaver ist seit einiger Zeit in unserer Branche en vogue. Wie so oft, ist es nicht leicht, Marketingaspekte
vom informatischen Wesensgehalt zu unterscheiden. Dieser Beitrag m?chte hier helfen. 相似文献