Synthesis and kinetic studies of UV‐curable urethane‐acrylates

The UV‐curable urethane‐acrylates based on 2‐hydroxyethyl methacrylate (HEMA)‐terminated polyurethane (PU) for lithographic and coating applications are investigated in this study. Series of PU prepolymers were made from 4,4‐diphenyl methane diisocyanate (MDI), poly(propylene oxide) glycol (PPG 400), poly(butylene adipate)glycol (PBA 500), or poly(tetramethylene oxide) glycol (PTMO 1000) and are terminated with HEMA. The 2,2‐azobisisobutyronitrile (AIBN) was used as a UV‐initiator under air atmosphere. The curing kinetics of HEMA‐terminated PU film were studied. The curing analysis, using FTIR and reaction kinetics, indicate the reaction rate equation correlates well with the film thickness [T], initiator concentration [I], unreacted double bond concentration [C?C], and exposed energy [E] of the reaction system. The kinetic rate equation for the UV‐curable reaction can be written as © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 91: 3162–3166, 2004     

Win7控制面板三大功能应用技巧

每个市场客户的需求是不一样的,使用情况也有差异.Win7的推出也是褒贬不一.Win7系统是微软开发的操作系统,在桌面、主题、功能、安全上相对于上一代系统有着很大的改进.以功能的强大及全面、存储空间小、操作系统简单和新增功能的人性化而受到用户的喜爱,且智能性上来说,Win7比XP要好很多.但是通过调查研究地发现,很多的用户对于Win7系统的使用仅仅停留在了表面阶段,对于系统中很多新的、提高便捷性的功能了解不足.因此,笔者通过这篇文章来研究和探讨win7系统的控制面板中三大功能的应用技巧,让win7系统能更好的为用户服务.     

控制燃煤硫的污染与动力煤全硫比价划分

讨论了中国煤炭资源中全硫分布的特点，指出加强动力煤洗选，降低硫含量的重要性；采用ＩＧＣＣ工艺和热煤气脱硫技术，可以实现高硫煤的有效利用。并提出制定合理的动力煤全硫比价问题。     

A301型氨合成催化剂在NC—1020合成塔内件中的应用

根据Ａ３０１型催化剂的具体特点，介绍了该催化剂在兴平化肥厂ＮＣ－１０２０合成塔内件中的装填，还原情况及应用效果。     

新膜及膜过程的研究现状及发展动向

本文综述了双极性膜及其电渗析、膜蒸馏、膜萃取、无机膜等新膜及膜过程，简要说明其研究状况，应用前景和发展动向。     

社会性别视野下的多婚女性个案探讨

对一个有三次婚姻经历的女性进行了深度访谈.针对受访者的口述,分析了女性在婚姻中的社会性别观念,认为当今社会中,以父权制意识形态为中心的价值体系仍然存在,而且影响着妇女的婚姻角色选择.     

MACD与K线图技术在证券投机中的实证研究

利用MACD趋势指标与K线形态图进行相互验证技术,改进一般的基于MACD的证券买卖准则。实证结果表明,基于改进后的MACD买卖准则进行证券投机,几乎能使投机者捕捉到每一波段行情,从而获取较高收益。     

Effects of annealing temperature on the microstructure and properties of the 25Mn-3Si-3Al TWIP steel

Microstructures and mechanical properties of the 25Mn twinning induced plasticity (TWIP) steel at different annealing temperatures were investigated. The results indicated that when the annealing temperature was 1000°C,the 25Mn steel showed ex-cellent comprehensive mechanical properties,the tensile strength was about 640 MPa,the yield strength was higher than 255 MPa,and the elongation was above 82%. The microstructure was analyzed by optical microscopy (OM),X-ray diffraction (XRD),and transmission electron...     

基于multi-agents的网络防卫体系中预警定位系统的研究与实现

传统的网络安全措施,如加密认证、防火墙和入侵检测系统等,虽然在保护信息的保密性、完整性、可用性和控制访问方面有一定的效果,但在协同和预警方面依然存在不足.文章提出了1个基于multi-agents的网络安全防卫系统,该系统由协同预警定位系统、协同审计系统、安全隔离系统、事故恢复系统等多个模块构成,模块之间由多个多级分层agents来负责通信任务.系统控制中心的agent server负责控制和协调整个安全体系,制定全网统一的安全控制策略.在该系统中,整个网络被划分成不同级别的分区,建立不同级别的协同预警定位系统,各分区既相互协作,又能够独立自治,通过协作的方式共同维护着整个网络的安全.在IPv6环境下测试的结果表明,该系统可以高效进行预警,IDS的捕获率约为95%、漏报率小于6%、误报率小于7%.     

Application of polymerizable surfactant in the preparation of polystyrene/nano-Fe<Subscript>3</Subscript>O<Subscript>4</Subscript> composite

Monooctadecyl maleate, as a polymerizable surfactant, was synthesized by the mono-esterification of maleic anhydride and octadecanol, and was utilized to surface-modify nano-Fe₃O₄ particles. A polymerizable magnetic fluid was obtained by directly dispersing modified nano-Fe₃O₄ particles into styrene monomer, and the polystyrene/nano-Fe₃O₄ composite was prepared through free radical polymerization of polymerizable magnetic fluid. The structure and dispersion status in different dispersion phases of modified nano-Fe₃O₄ particles were studied by Fourier transform infrared (FTIR) spectrometry, X-ray diffraction (XRD) and transmission electron microscopy (TEM), respectively. The experimental results show that the nano-Fe₃O₄ particles modified by monooctadecyl maleate with the size of about 7–10 nm can be uniformly dispersed into styrene and fixed in the composite during the procedure of polymerization. Thermogravimetric analysis (TGA) and vibrating sample magnetometry (VSM) indicate that the thermal stability of polystyrene/nano-Fe₃O₄ composite is improved compared to that of pure polystyrene, and the composite is a sort of superparamagnetic materials.