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31.
采用CO2 作为保护气体消除大熔深激光焊接低碳钢时易发生的气孔问题 ,并对比研究了CO2 和Ar气保护条件下 12mm厚低碳钢板激光焊缝的组织和韧性。焊接试验利用 4kWNd :YAG激光器 ,采用双面深熔焊的方法 ,焊接条件为 4kW激光功率和0 .3 ,0 .5m/min的焊接速度。冲击试验采用一种自行设计的带侧面缺口的三缺口冲击试样 ,以保证断裂全部发生在焊缝。结果表明 ,利用CO2 作保护气体焊接低碳钢板 ,可以有效消除大熔深激光焊接时的气孔问题 ,并获得比Ar气保护下硬度较低 ,冲击韧性高的焊缝。研究工作为解决大功率激光深熔焊时容易发生的气孔问题提供了一条有效途径 相似文献
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33.
Dr. Daisuke Okuno Dr. Noriho Sakamoto Dr. Mohammed S. O. Tagod Yoshiko Akiyama Dr. Sakiko Moriyama Dr. Takuto Miyamura Dr. Atsuko Hara Dr. Takashi Kido Dr. Hiroshi Ishimoto Prof. Yuji Ishimatsu Prof. Takashi Tanaka Prof. Jun Ishihara Prof. Kohsuke Takeda Prof. Yoshimasa Tanaka Prof. Hiroshi Mukae 《ChemMedChem》2021,16(16):2515-2523
Heat shock protein 47 (HSP47), a collagen-specific molecular chaperone, is causally related to fibrotic diseases, including idiopathic pulmonary fibrosis. The identification of Compounds that interfere with the HSP47-collagen interaction is essential for the development of relevant therapeutics. Herein, we prepared human HSP47 as a soluble fusion protein expressed in E. coli and established an assay system for HSP47 inhibitor screening. We screened a natural and synthetic Compound library established at Nagasaki University. Among 1023 Compounds, 13 exhibited inhibitory activity against human HSP47, of which three inhibited its function in a dose-dependent manner. Epigallocatechin-3-O-gallate, one of these three Compounds, is a typical polyphenol Compound derived from tea leaves. Structurally related Compounds were synthesized and examined for their activity, revealing a hydroxyl group at A-ring position 5 as important for its activity. The present findings provide valuable insight for the development of natural product-derived therapeutics for fibrotic diseases, including idiopathic pulmonary fibrosis. 相似文献
34.
F. Otsubo K. Kishitake T. Akiyama T. Terasaki 《Journal of Thermal Spray Technology》2003,12(4):555-559
It is known that the corrosion resistance of stainless steel is deteriorated by blasting, but the reason for this deterioration
is not clear. A blasted austenitic stainless steel plate (JIS-SUS304) has been characterized with comparison to the scraped
and non-blasted specimens. The surface roughness of the blasted specimen is larger than that of materials finished with #180
paper. A martensite phase is formed in the surface layer of both blasted and scraped specimens. Compressive residual stress
is generated in the blasted specimen and the maximum residual stress is formed at 50–100 μm from the surface. The corrosion
potentials of the blasted specimen and subsequently solution treated specimen are lower than that of the non-blasted specimen.
The passivation current densities of the blasted specimens are higher those of the non-blasted specimen. The blasted specimen
and the subsequently solution treated specimen exhibit rust in 5% sodium chloride (NaCl) solution, while the non-blasted specimen
and ground specimen do not rust in the solution. It is concluded that the deterioration of corrosion resistance of austenitic
stainless steel through blasting is caused by the roughed morphology of the surface. 相似文献
35.
Reaction rates in the Mg2Ni---H2 system are still unclear, although they are needed for the process/optimization of hydrogen storage reactors. In this article, the rates of hydrogen absorption and desorption of the magnesium nickel alloy were investigated at different pressures up to 2.0 MPa using a constant-temperature thermogravimetric method. The powder of the alloy was microencapsulated with copper to improve the alloy properties (such as cycling strength) as a pretreatment. In the experiments, weight changes of the smallest amount possible of samples were monitored with the help of an ultra-accurate thermobalance, in order to avoid changes of the sample temperature due to the heat of the reaction. The reaction curves obtained revealed unique dependence of temperature and pressure and influence of thermal hysterisis. It is also possible that hydrogen-absorption and-desorption rates of this hydrogen storage alloy are expressed by the rate equation of first-order reversible reaction. 相似文献
36.
New bismaleimides containing ether bonds were prepared. The thermal properties of the bismaleimides were investigated by differential scanning calorimetry (DSC). The effects of structure of the bismaleimides and curing conditions on the thermal and mechanical properties of the cured resins such as initial decomposition temperature (Td), glass transition temperature (Tg), and flexural strength were studied. The introduction of ether bonds to bismaleimide resins decreased the brittleness of the resins without reductions in their heat-resistant properties. 相似文献
37.
In membrane filtration, solution environment factors such as pH and solvent density are important in controlling the filtration
rate and the rejection of the particles and/or the macromolecules. The filtration rate and the rejection in membrane filtration
have been investigated from physicochemical aspects. It was shown that the properties of the filter cake formed on the membrane
surface play a vital role in determining the filtration rate in mem-brane filtration. It was clearly demonstrated that such
filtration behaviors as the filtration rate and the rejection are highly dependent on the electrical nature of the particles
and/or the macromolecules. Furthermore, it was shown that the solvent density ρ has a large effect on the steady filtration
rate in upward ultrafiltration. 相似文献
38.
Hai -Hang Li Masafumi Inoue Hiroyuki Nishimura Junya Mizutani Eiji Tsuzuki 《Journal of chemical ecology》1993,19(8):1775-1787
Phenolic compounds have been identified as the most common allelochemicals produced by higher plants. Inhibitions of cinnamic acid, its related phenolic derivatives, and abscisic acid (ABA) on seedling growth and seed germination of lettuce were studied.trans-Cinnamic acid, ando-,m-, andp-coumaric acids inhibited the growth of etiolated seedlings of lettuce at concentrations higher than 10–4 M and seed germination above 10–3 M. Coumarin inhibited seedling growth and seed germination at 10–5 M or above. Chlorogenic acid inhibited seedling growth above 10–4 M, but did not inhibit seed germination at 10–5–5×10–3 M. Low concentrations (below 10–3 M) of caffeic and ferulic acids promoted the elongation of hypocotyls, but higher concentrations (over 10–3 M) inhibited seedling growth and seed germination. These phenolic compounds and abscisic acid had additive inhibitory effects both on seedling growth and seed germination. The inhibition on lettuce was reversed by caffeic and ferulic acids at concentrations lower than 10–3 M except for the inhibition of germination by coumarin. These results suggest that in naturetrans-cinnamic acid,o-, m-, p-coumaric acids, coumarin, and chlorogenic acid inhibit plant growth regardless of their concentration. However, caffeic and ferulic acids can either promote or inhibit plant growth according to their concentration. 相似文献
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40.
Takamasa Ishigaki Ya-Li Li Eiji Kataoka 《Journal of the American Ceramic Society》2003,86(9):1456-1463
The phase formation and microstructure of titanium oxides and composites produced by Ar–O2 thermal plasma oxidation of titanium carbide powders were investigated in detail by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Relationships between the phase compositions and microstructures of the oxides were established by combined structural and phase analyses, in correlation with synthesis conditions and phase formation mechanisms. It is revealed that vapor condensation favored the formation of anatase, which existed as smaller particles, while liquid/solid oxidation favored the formation of rutile, which appeared as larger particles or composites. A higher oxygen input in the plasma gases (Ar + O2 ) enhanced the formation of anatase due to impeded oxidation and evaporation. A small amount of Ti4 O7 and Ti3 O5 was detected in the larger particles coexisting with rutile or TiC. These suboxides were formed as intermediates in solid oxidation of TiC or precipitated from the Ti–C–O melt during cooling. Furthermore, extensive cracks, dislocations and stresses were observed in the monolithic rutile and composites, in association with the rapid quenching in this high-temperature in-flight oxidation process. 相似文献