异丁烯两段催化氧化制甲基丙烯酸催化剂研究 Ⅰ．异丁烯气相氧化制甲基丙烯醛多元复合氧化物催化剂的研究

本文报导用于异丁烯（叔丁醇）选择氧化制ＭＡＬ（甲基丙烯醛）的多元复合氧化物催化剂的研究结果。同共沉淀法制备的催化剂的活性主要决定于其化学组成，同时受到制备条件的影响。最佳催化剂的主要物相组成为ＰｂＯ３，Ｂｉ２ＭｏＯ３．３、ＮｉＭｏＯ４、Ｓｂ２Ｏ３及ａ－Ｆｅ２Ｏ３小颗粒。在３５５℃，１０００～２５００ｈ－１空速范围，叔丁醇：水：空气＝１：３．３：７（摩尔比）的条件下可获得异丁烯转化率达９６％，ＭＡＬ选择性达８９％的结果。     

下河沉积型瓷石的工艺特性与开发应用的探讨

本文论述了新近在江西下河发现的沉积型瓷石的地质特点、矿石特征、精泥性能、成瓷工艺及其开发应用前景。     

印刷胶带生产中的几个问题

对印刷胶带生产中的几个问题如稀释剂、印刷中参数、涂布工艺等作了简述。     

Engineering all-aromatic polyamide surface from hydrophilic to superhydrophobic and the accelerated strategy

Being a new kind of nanomaterials, aromatic polyamide nanofibers (ANF) have been much highlighted in recent studies. We here demonstrate an isopropyl alcohol (IPA) accelerated chemical cleavage on poly (p-phenylene terephthalamide) chopped fibers, which provides an efficient preparation method of ANF. The comprehensive study on the processes accelerated by different alcohols revealed that the preparation time of ANF in the mixed medium of dimethyl sulfoxide (DMSO)-alcohol (20:1 in volume) was shorten to 45 min and 75 min for methanol (ethanol) and isopropanol, respectively. However, the nanofibers prepared in DMSO-IPA exhibited the minimum in axial and radial dimensions, providing the finest and most uniform diameter of 16 nm. The corresponding ANF films through vacuum assisted filtration also showed the highest tensile strength of 150 MPa, in comparison with those of the ANF films prepared using other alcohols, which were about 110 MPa. Furthermore, ANF/silicon hybrid films were prepared by the ionic ring-opening reaction followed by the alkoxysilane condensation and nanoparticle fabrication. By changing the organo functional groups in the alkoxysilane, the surface of the films were adjustable in a wide contact angle range from 56° (hydrophilic) to 150° (superhydrophobic), suggesting the amendable interfacial properties potential applicable to composite fabrication with most of the resin matrix.     

冷轧工作辊摩擦不稳定分析及其抑制对策

对冷轧机工作辊由于摩擦力引起的垂直、横向振动作了定性分析，指出了它们的危害，提出了预防措施。     

新时期研究生挫折教育略论

加强对研究生的挫折教育,已成为新时期研究生教育的一项非常重要而迫切的任务。研究生挫折教育的途径主要有:培养研究生树立良好的挫折观;将远大志向与正确、切实的短期目标有机结合;研究生导师要将挫折教育作为自身工作的重要职责和内容;要创设挫折情境,加强实践体验;在研究生中积极开展抗挫互助活动;帮助研究生学会自我调适、自我超越、自我教育。     

对高校图书馆智能化管理的探究

随着现代信息的蔓延,学校素质教育的全面推进,学校图书馆的地位在不断提高,作用也会逐渐的凸现出来.图书馆是落实素质教育的一个重要阵地,把图书活动作为一个栽体,充分发挥图书馆现有的物质基础,大力开展全校师生的读书活动,形成爱书,读书的良好风尚,使图书馆成为师生最大、最亲近的学习课堂.由此,大力加强和广泛发展高校图书馆的建设,是一项非常重要而迫切的艰巨任务,也是高校图书馆顺应时代发展的必要,这样就要求正确面对管理,加强对图书馆智能化的探究.     

模拟器在嵌入式软件开发中的应用实现

嵌入式系统在电子产品中的应用,加快了电子产品更新换代的速度,要想在技术竞争中立于不败之地,唯有加快应用软件开发进程,缩短产品开发周期.模拟器在嵌入式系统应用软件开发中的使用,大大简化了软件调试过程.本文基于μ C/OS-II嵌入式实时操作系统,研究开发出一款利用模拟器进行应用软件开发的多媒体播放器智能菜单,具有很大的实际应用价值,加快了产品的开发速度,增加了产品的核心竞争力.     

Testing the equality of proportions for correlated otolaryngologic data

In otolaryngologic (or ophthalmologic) studies, each subject usually contributes information for each of two ears (or eyes), and the values from the two ears (or eyes) are generally highly correlated. Statistical procedures that fail to take into account the correlation between responses from two ears could lead to incorrect results. On the other hand, asymptotic procedures that overlook small sample designs, sparse data structures, or the discrete nature of data could yield unacceptably high type I error rates even when the intraclass correlation is taken into consideration. In this article, we investigate eight procedures for testing the equality of proportions in such correlated data. These test procedures will be implemented via the asymptotic and approximate unconditional methods. Our empirical results show that tests based on the approximate unconditional method usually produce empirical type I error rates closer to the pre-chosen nominal level than their asymptotic tests. Amongst these, the approximate unconditional score test performs satisfactorily in general situations and is hence recommended. A data set from an otolaryngologic study is used to illustrate our proposed methods.     

基于重要目标区的三维地形快速渲染方法

三维地形的显示需要绘制大量的三角形网格,为了提高地形显示速度目前广泛采取了三角形网格简化技术。针对弹道导弹作战区域地形的特殊性,提出了一种基于重要目标区的网格简化方法。从BMP位图读取地形高度信息,以四叉树保存网格数据,按照区域重要性静态确定地形网格疏密程度。并采用DirectX平台,实现了导弹战区三维地形显示,提高了渲染效率。