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21.
Micro-grinding using micro-tools has become very prevalent due to the miniaturization of products with increased process requirements. Moreover, this process provides an edge over other competitive processes, especially as a final process step. The quality of the part produced by the micro-scale grinding process can be influenced by various factors, particularly by the induced mechanical forces. Therefore, predictive model of cutting force can provide guidance for further development and optimization of the process. Although there has been a lot of a research conducted on conventional grinding, little knowledge has been accumulated on micro-scale grinding due to the fact that it is an emerging field of research. The early grinding models developed are mostly based on parameters such as wheel and workpiece velocity, depth of cut and grit size of the grinding wheel. Those early models narrated that the grits penetrate and cut the material from the workpiece surface with the generated grinding forces proportional to the removed material. However, those models may not be appropriate for micro-scale grinding due to the mode of material removal and the method of contact between surfaces which is different from the macro-scale method. In addition to that, due to the small feed rate used in brittle material machining, ploughing force needs to be considered intensively in addition to the chip formation force. Therefore, a new analytical model has been proposed to evaluate cutting forces of micro-grinding process based on the process configuration, workpiece material properties and micro-grinding tool topography. The size effect of micro-machining has been carefully considered in this proposed model. Therefore, this approach allows the derivation of cutting force comprising of both the chip formation force and ploughing force. Experimental investigation in a micro-grinding configuration has been pursued to validate the proposed predictive model. The estimated cutting force showed a good correlation with the experimental values except for higher depth of cut and lower feed rate. Additionally, paired T test has been performed to quantify the difference between the predicted and experimental results.  相似文献   
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The so‐called “deficiency diseases” among children in developing countries are not always the result of inadequate diets. Many cases of childhood anaemia, for example, show little correlation with mineral or vitamin intakes, and, in this latter situation, infestations by various parasitic worms appear to be primarily responsible, with related infections adding to the misery. The role of medication in alleviating this problem is somewhat limited, and the real hope must lie in the education of parents, particularly mothers, in respect of personal and food hygiene.  相似文献   
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The experimental study of the system Sb–Zn by differential calorimetry made it possible to plot the whole phase diagram. We found the stability domains of existence of the stoichiometric compound SbZn and the solid solutions which extend on both sides from the compositions corresponding to Sb3Zn4 (forms γ and β) and Sb2Zn3 (forms η and ζ). Sb3Zn4 and Sb2Zn3 are both congruent melting compounds at 566 and 568 °C respectively with an eutectic transformation at 563 °C:
liquid(43% Zn) ↔ Sb3Zn4(γ) + Sb2Zn3(η).
Sb2Zn3(ζ) is formed at 407 °C starting from Sb3Zn4(β) and zinc. The decomposition, by cooling, occurs around 360 °C.  相似文献   
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Protection of Metals and Physical Chemistry of Surfaces - This paper presents experimental aspects of two triazolodiathiazine derivatives 1...  相似文献   
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Self-healing materials have been attracting the attention of the scientists over the past few decades because of their effectiveness in detecting damage and their autonomic healing response. Self-healing materials are an evolving and intriguing field of study that could lead to a substantial increase in the lifespan of materials, improve the reliability of materials, increase product safety, and lower product replacement costs. Within the past few years, various autonomic and non-autonomic self-healing systems have been developed using various approaches for a variety of applications. The inclusion of appropriate functionalities into these materials by various chemistries has enhanced their repair mechanisms activated by crack formation. This review article summarizes various self-healing techniques that are currently being explored and the associated chemistries that are involved in the preparation of self-healing composite materials. This paper further surveys the electronic applications of self-healing materials in the fields of energy harvesting devices, energy storage devices, and sensors. We expect this article to provide the reader with a far deeper understanding of self-healing materials and their healing mechanisms in various electronics applications.  相似文献   
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The present work describes the synthesis of porous BaSnO3 by eco‐friendly sol‐gel method using albumin as a bio‐template agent, and its application as a solid base catalyst in biodiesel production from waste cooking oil. The physico‐chemical, textural, and morphological properties of the catalyst were evaluated by X‐ray diffraction (XRD), Brunauer‐Emmett‐Teller (BET), field emission scanning electron microscopy (FESEM), and temperature programmed desorption (TPD)–CO2 techniques. The synthesized catalyst showed considerable stability, efficient catalytic activity, and negligible metal leaching. The satisfactory performance of the catalyst could be ascribed to the presence of basic sites of different strength on the surface of the catalyst. The catalyst produced maximum biodiesel yield of 96% at optimum reaction conditions of 90°C reaction temperature, methanol to oil molar ratio of 10:1, catalyst dosage of 6 wt%, and reaction time of 2 hours. Moreover, the catalyst showed substantial reusability up to five reaction cycles without any considerable decrease in transesterification activity.  相似文献   
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The potential of FTIR combined with chemometrics was studied to classify five Moroccan varieties of olives by analysis on the endocarps. Attenuated total reflectance (ATR) enabled the samples to be examined directly in the solid state. The spectral data were subjected to a preliminary derivative elaboration based on the Norris gap algorithm to reduce the noise and extract larger analytical information. Linear discriminant analysis (LDA) was adopted as classification method, and Principle component analysis (PCA) was employed to compress the original data set into a reduced new set of variables before LDA. The calibration set was built by using the IR data from seventy‐five samples scanned in reflectance mode, and the ranges 3000–2400 and 2300–600 cm?1 were selected because furnishing the most useful analytical information. PCA allowed clustering the samples in five classes by using the first two principal components with an explained variance of 98.16%. Application of LDA on an external test set of twenty‐five samples enabled to classify them into five variety groups with a correct classification of 92.0%.  相似文献   
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