PSoC-based embedded design and quartz tuning fork for low-temperature measurement system design

This article describes a commercial quartz tuning fork (QTF), 8 mm in height by 3 mm in diameter, holding a two-terminal electronic component with a nominal frequency of 32.768 kHz and 12.5 pF typical load capacitance packed in a vacuum-sealed metal container, which has been used as a sensor for low-temperature measurement with good sensitivity, repeatability, and reliability. An embedded readout design with the support of a programmable system on-chip (PSoC) and virtual instrument control program, which uses a personal computer as an input/output device, provides online data acquisition of the QTF frequency data, which will in turn provide the measurement of the low-temperature bath in which the QTF is immersed. The embedded PSoC readout captures the varying frequency signals from the QTF as a response to the measurement temperature, processes it, and sends the frequency value to a personal computer, where LabVIEW, a graphical language ("G" language), displays the data in a graphical format. The QTFs for low temperature (300 K to 77 K) are well studied, whereas a sensor using a PSoC embedded design as a readout is a novel design implementation.     

State of the academic field of IS in India

The field of information systems (IS) remains ill-defined, facing problems of recognition and identity crisis. Several papers and debates have been dedicated on this topic for over three decades. The focus of these debates have largely centered on the state of the IS field in Americas and Europe and with a limited study conducted in the Asia–Pacific context. This study attempts to assess the field in the Indian context and highlight the challenges and issues faced by IS faculties in India. Based on literature survey of the seminal papers in the field, we identified the salient topics of interest to IS researchers: identity of the IS field; diversity of the field; research approaches, methods and rigor; reference disciplines; journals and conferences; and IS course and curriculum. A two-phase study was carried out to explore the interest generated by the IS field in India. In the first phase, secondary data review of leading business schools in India was carried out to understand their focus on IS as an academic discipline. In the second phase, we conducted interviews of IS researchers from the premium business schools in India. In our study, we analyze the research focus of IS faculties in B-schools in India, analyze the composition of the faculty pool and the nature of research work undertaken by them. Our study points at the restricted focus of IS researchers in India around a few narrow areas, with a significant breadth of topics not being explored for research. We found the identity struggle of the field to be prominent, which was further compounded by the limited number of active, IS researchers. The growing importance of qualitative techniques in IS research, the challenges of developing a sound base in multiple reference disciplines and the need for making IS course interesting for business school students were some of the other significant observations. Our study also highlighted the paradox of the success of the IT industry in India leading to reduced enrollment of IS courses in B-Schools. We conclude by providing recommendations to B-school deans and directors.     

Developing a limb repositioning robotic interface for persons with severe physical disabilities

Limb repositioning is necessary for individuals with severe physical disabilities to sustain muscle strength and prevent pressure sores. As robotic technologies become ubiquitous, these tools offer promise to support the repositioning process. However, research has yet to focus on ways in which individuals with severe physical disabilities can control robots for these tasks. This paper presents a study that examines the needs and attitudes of potential users with physical disabilities to control a robotic aid for limb repositioning. Subjects expressed interest in using brain–computer interface (BCI) and speech recognition technologies for purposes of executing robotic tasks. The performance of four subjects controlling arm movements on an avatar through the keyboard, mouse, BCI, and Dragon NaturallySpeaking speech recognition was evaluated. Although BCI and speech technologies may limit physical fatigue, more challenges were faced using BCI and speech conditions compared to the keyboard and mouse. This research promotes accessibility into mainstream robotic technologies and represents the first step in the development of a robotic prototype using a BCI and speech recognition technologies for limb repositioning.     

Aluminum phosphate sealing to improve insulation resistance of plasma-sprayed alumina coating

The insulation resistance of conventional atmospheric plasma-sprayed alumina coatings with 10–15% porosity is ～10¹¹ Ω. The presence of pores, lamellae boundaries, and other non-fillings dampens the insulation resistance of the coating. In the present study, aluminum phosphate was used to seal the surface of plasma-sprayed alumina coating and evaluate the effect of sealing on the insulation resistance and its thermal cycling response. Sealing was carried out with three concentrations of sealant (P/Al molar ratio of 3, 10, and 15). Characterization by X-ray diffraction and scanning electron microscopy revealed the primary sealing phase as aluminum metaphosphate and effective sealing of the pores by the aluminum phosphate phases. Insulation resistance is improved by two orders of magnitude after sealing the coated samples. Sealing with P/Al molar ratio 3 exhibited maximum insulation resistance of ～10¹³ Ω at room temperature. Thermal cycling studies between 650°C and 200°C on the sealed samples showed deterioration in thermal cycling life after sealing.     

Investigation of machining characteristics in rotary ultrasonic machining of alumina ceramic

Alumina ceramic is well documented as a much-demanded advanced ceramic in the present competitive structure of manufacturing and industrial applications owing to its excellent and superior properties. The current article aimed to experimentally investigate the influence of several process variables, namely: spindle speed, feed rate, coolant pressure, and ultrasonic power, on considered machining characteristics of interest, i.e., chipping size and material removal rate in the rotary ultrasonic machining of alumina ceramic. Response surface methodology has been employed in the form of a central composite rotatable design to design the experiments. Variance analysis testing has also been performed with a view to observing the consequence of the considered parameters. The microstructure of machined rod samples was evaluated and analyzed using a scanning electron microscope. This analysis has revealed and confirmed the presence of plastic deformation that caused removal of material along with brittle fractures in rotary ultrasonic machining of alumina ceramic. The validity and competence of the developed mathematical model have been verified with test results. The multi-response optimization of machining responses (material removal rate and chipping size) has also been attempted by employing a desirability approach, and at an optimized parametric setting the obtained experimental values for material removal rate and chipping size were 0.4166?mm³/s and 0.5134?mm, respectively, with a combined desirability index value of 0.849.     

A Comparative Investigation of Optical and Structural Properties of Cu-Doped CdO-Derived Nanostructures

In this report, we studied various structural and optical properties of pure and copper-doped cadmium oxide (CdO) thin films. Nanostructured Cu-doped CdO films were deposited using sol–gel spin-coating technique. The structural and morphological changes have been observed by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and atomic force microscopy (AFM) studies. The optical and electrical properties of the pure and Cu-doped CdO thin films were studied by UV–vis spectroscopy and four-point probe method, respectively. The XRD peaks show the formation of nanocrystalline CdO with cubic face-centered crystal structure. The band gaps of the as deposited films were found in the range of 2.32–2.73 eV, while after doping, it decreases due to structural deformation. The electrical resitivity was found to decrease approximately ～10 in Cu-doped CdO thin films.     

Mesoporous titanium dioxide nanocatalyst: a recyclable approach for one‐pot synthesis of 5‐hydroxymethylfurfural

The present study deals with the production of 5‐hydroxymethyl furfural (HMF) from fructose by chemo‐conversion method using chemical catalyst, conventionally achieved by microwave‐assisted dehydration process. Five different chemical catalysts, namely oxalic acid, phosphotungstic acid and mesoporous titanium dioxide nanoparticles (TNPs) were compared at constant conditions of which TNPs yielded a maxima of 33.95%. The optimum temperature and catalyst loading were found to be 200°C and 20%, respectively, at a 5% optimum substrate concentration during 15 min optimum reaction time to yield 61.53% HMF. The efficiency of synthesised TNPs was investigated further through reusability studies. TNPs were properly recycled and the catalytic activity recovery was good even after a 14 batch reactions. The specific surface area of the TNP obtained is about 105.46 m² /g and its pore‐volume is about 0.42 cm³ /g according to single point adsorption. A large accessible surface area combined with a minimal pore size (15.92 nm) obtained with mesoporous TNPs is desirable for better catalyst loading, high‐yield HMF, retention and reduced diffusion constraints.Inspec keywords: mesoporous materials, recycling, production management, dissociation, nanoparticles, nanotechnologyOther keywords: mesoporous titanium dioxide nanocatalyst, recyclable approach, one‐pot synthesis, 5‐hydroxymethyl furfural production, HMF, chemo‐conversion method, chemical catalyst, microwave‐assisted dehydration process, oxalic acid, phosphotungstic acid, mesoporous titanium dioxide nanoparticles, TNP     

Green synthesis of highly stable carbon nanodots and their photocatalytic performance

The present study reports a novel, facile, biosynthesis route for the synthesis of carbon nanodots (CDs) with an approximate quantum yield of 38.5%, using Musk melon extract as a naturally derived‐precursor material. The synthesis of CDs was established by using ultraviolet–visible (UV–vis) spectroscopy, Dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy and Fourier transform infrared (FTIR) spectroscopy. The as‐prepared CDs possess an eminent fluorescence under UV–light (λ _ex  = 365 nm). The size range of CDs was found to be in the range of 5–10 nm. The authors further explored the use of such biosynthesised CDs as a photocatalyst material for removal of industrial dye. Degradation of methylene blue dye was performed in a photocatalytic reactor and monitored using UV–vis spectroscopy. The CDs show excellent dye degradation capability of 37.08% in 60 min and reaction rate of 0.0032 min⁻¹. This study shows that synthesised CDs are highly stable in nature, and possess potential application in wastewater treatment.Inspec keywords: carbon, nanostructured materials, nanofabrication, catalysis, photochemistry, ultraviolet spectra, visible spectra, photoluminescence, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectra, fluorescence, dyesOther keywords: green synthesis, highly stable CD, photocatalytic performance, biosynthesis route, carbon nanodots, quantum yield, Musk melon extract, naturally derived‐precursor material, ultraviolet‐visible spectroscopy, dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy, FTIR spectroscopy, fluorescence, biosynthesised CD, photocatalyst material, industrial dye, methylene blue dye degradation, photocatalytic reactor, UV‐vis spectroscopy, wastewater treatment, size 5 nm to 10 nm, time 60 min     

VMI versus information sharing: an analysis under static uncertainty strategy with fill rate constraints

A vendor-managed inventory (VMI) relationship between a downstream retailer and an upstream vendor consists of two distinct components: (i) information sharing (IS) and (ii) a shift in decision-making responsibility. This study compares these two components of VMI in a two-stage serial supply chain based on the ‘static uncertainty’ strategy under dynamic and random demand with fill rate constraints. Numerical experiments are conducted using analytical models to identify the conditions where the incremental value of VMI over IS is significant. The results provide guidelines relevant to academia and supply chain practitioners in taking VMI adoption decision above and beyond IS according to their specific business environment.