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1.
Ivan Fortelný Monika Lapčíková František Lednický Zdeněk Starý Zdeněk Kruliš 《Polymer Engineering and Science》2008,48(3):564-571
This article is focused on the phase structure development in immiscible polymer blends during melt mixing. Nonuniformity of the phase structure, i.e., the coexistence of areas containing particles with markedly different size distribution, was detected in quenched and compression molded samples of a number of various blends prepared by long and intensive mixing in the chamber of a Plasticorder. The same effect was found also for polystyrene/polyamide blends prepared in a twin‐screw extruder. It was shown that neglecting nonuniformity of the phase structure can lead to considerable error in evaluation of the effect of system parameters on the blend morphology. The reasons for the effect were discussed and it was found that inhomogeneous flow field in mixers is a plausible explanation of the nonuniform phase structure. POLYM. ENG. SCI., 2008. © 2008 Society of Plastics Engineers 相似文献
2.
ZnO-based varistor samples were prepared by the direct mixing of the constituent phases (DMCP) and sintering at 1100 °C for 2 h. The influence of the starting powder mixture's composition – the amounts of the pre-reacted varistor compounds and their composition – and its preparation, either with or without mechano-chemical activation (MCA), on the microstructure, phase composition and electrical characteristics of the varistor samples was studied. It showed that MCA improved the density and microstructural homogeneity of the varistor samples. MCA strongly affected the grain growth: it enhanced the nucleation of inversion boundaries (IBs) in the ZnO grains and the IBs-induced grain-growth mechanism resulted in uniform grain growth and hence a microstructure with smaller ZnO grains and a narrower grain size distribution. The final phase composition of the samples prepared by the DMCP method mainly depended on the presence of varistor dopants that can prevent the formation of the pyrochlore phase, especially Cr2O3, while MCA can affect it mostly by providing a homogeneous distribution of those dopants. The DMCP varistor samples prepared with MCA had much better current–voltage characteristics than the samples of the same composition prepared from unactivated powders. 相似文献
3.
The hydration phase and pore structure formation in the blends of sulfoaluminate-belite cement with Portland cement 总被引:1,自引:0,他引:1
Sulfoaluminate-belite (SAB) cements are an attractive class of low-energy cements from the viewpoint of saving energy and releasing less CO2 into the atmosphere during their production. Their hydraulic activity, however, does not match that of the ordinary Portland cement (PC) and needs improvement before they can be used on their own. However, SAB cements when blended with PC have the potential to be used effectively in traditional applications as shown by this study. Mortars made with blends of SAB cements and PC, and a cement-to-sand ratio of 1:3 by weight and a water-to-cement ratio of 0.5, indicate a superior protection against corrosion of steel to those made with blends of PC and blast-furnace slag (BFSPC). The prepared mortars were stored at 20 °C for 90 days under either a 60% relative humidity (RH)-dry air, or 100% RH-wet air conditions. With further improvement in the SAB cement quality through better understanding of their characteristics, a genuine competition between SAB/PC and BFSPC can be expected in practice. 相似文献
4.
5.
We study the error probability performance of rotated lattice constellations in frequency-flat Nakagami-m block-fading channels. In particular, we use the sphere lower bound on the underlying infinite lattice as a performance benchmark. We show that the sphere lower bound has full diversity. We observe that optimally rotated lattices with largest known minimum product distance perform very close to the lower bound, while the ensemble of random rotations is shown to lack diversity and perform far from it. 相似文献
6.
A El?i 《Canadian Metallurgical Quarterly》1994,50(12):8882-8884
7.
8.
The dependence of the magnetic momentm obtained from the hysteresis loops on the speed of the magnetic field sweep
=dH
ext/dt is explained on the basis of Anderson's interpretation of the magnetic flux creep. In addition, a phenomenological model is suggested which predicts a linear dependence ofm on ln
with the slope m/ ln
, numerically equal to the relaxation rate m/ ln(t) from the usual magnetic relaxation. Such linear relations betweenm and ln
were observed experimentally in single crystals of YBaCuO. Preliminary experiments on the complementary time dependent relaxation ofm after a simulated step change ofH
ext gave mostly relaxation rates close to the predicted values. The model here presented also enables one to compare the critical state in the superconductor at a field sweep rate
with the critical state at some timet
eff after a step change ofH
ext. The values of
analyzed in our experiments actually correspond to the critical state at timest
eff between0.04 and4 sec after an imaginary large step change ofH
ext. 相似文献
9.
B. Klaić 《Scientometrics》1990,19(1-2):11-24
The research activity of chemists from the Rugjer Bokovi Institute (RBI, Zagreb, Yugoslavia) was analyzed for the period 1976–1985, covering 2018 research years of scientific work, and 1149 SCI registered papers (0.57 publications per research year). At the average, one paper was published by 3.05 scientists. The papers were published in 235 different journals, most frequently is the nationalCroatica Chemica Acta (171 papers). The publications were divided into two groups: for the periods 1976–1980 and 1981–1985, and for each paper citations were collected in the respective time period. An average publication had 2.58 citations. Chemical papers from the second period had 2.73 citations per paper, which is 85% of the expected value, and this was considerably more than for Yugoslav papers (66%) in general. The papers were classified according to the subfields used in theJournal Citation Reports, and the results compared with the data published bySchubert, Glänzel andBraun. The distribution of citations was also analyzed. 相似文献
10.
The microstructure and properties of NdFeB sintered permanent magnets were analysed by different methods. Samples analysed were sintered and thermally treated. The hard magnetic Nd2Fe14B phase and amorphous neodymium-rich phase were observed by TEM. The neodymium-rich phase contained iron and boron, in elemental and in B2O3 form, which is known as a glass former. At the sintering temperature, Nd2Fe14B and the neodymium-rich phase are supersaturated with iron, which should be dissolved at the annealing temperature to react with neodymium and boron and form additional Nd2Fe14B phase. Iron precipitates of size up to 2 nm were detected in the Nd2Fe14B phase. These superparamagnetic precipitates of -Fe could affect the hard magnetic properties of NdFeB magnets. 相似文献