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991.
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以超声波处理的梅毒螺旋体为抗原,致敏经醛化、鞣化处理的绵羊红血球,应用血凝试验检测梅毒患者血清中梅毒螺旋体特异性抗体。同时以国际上公认的标准方法——FTA-ABS作为对照试验。共检测1125份血清(其中梅毒血清205份,非梅毒血清920份).两种方法检测结果完全相符,即敏感性皆为100%,血凝试验的特异性为99%。 相似文献
995.
Summary The synthesis and thermal degradability of poly (DL-lactide) were investigated. Key factors affecting the polymer molecular weight were found to be monomer recrystallization, initiator concentration and the vacuum level during drying/sealing of the polymerization reaction ampoule. It was found that poly (DL-lactide) is thermally unstable above its melting temperature. Monomer recrystallization, polymer precipitation and a low initiator content of the polymer significantly inhibited the rate and extent of thermal degradation. 相似文献
996.
80年代黄河中游来沙量减少,主要原因是降雨量减少和降雨强度减小,流域综合治理也起到了减沙作用。据分析,降雨因素减沙约占总减沙量的70%,流域综合治理减沙约占30%。 相似文献
997.
最大熵在感应测井反演中的应用 总被引:1,自引:0,他引:1
常规的反演方法是对感应测井资料进行线性反褶积。由于感应测并获得的响应曲线是地层非线性时变滤波的结果,感应测井响应随地层电导率发生非线性变化。本文把熵的概念引入到感应测井反演中。用最大熵方法分别设计出实部信号和虚部信号所对应的反滤波因子,两条反映测井响应随电导率非线性变化的非线性函数也被拟合出来。文章最后用设计出的滤波因子及被拟合出的非线性函数对模拟相量感应测井资料进行了相量反褶积。处理结果表明,围岩效应和趋肤效应基本被消除。本方法与常规的三点反褶积法相比,克服了过聚焦现象,提高了精度。 相似文献
998.
DNA and amphiphilic N,N,N‐trimethyl‐N‐hexadecylammonium bromide (THAB) were stoichiometrically mixed together to produce a DNA–lipid complex, which was dissolved in dimethyl sulfoxide (DMSO) at 65°C and then crosslinked with isophorone diisocyanate (IPDI). The obtained organogel swelled reversibly in DMSO, responding to the variation of temperature. Interestingly, we observed that the gel exhibited a temperature‐dependent shape‐memory behavior. Above 65°C, whatever the shape the gel was deformed to, it could retain the new shape as the temperature was decreased to room temperature, while, when the gel was heated to 65°C again, it could recover its initial shape. The shape‐memory characteristic is supposedly originated from the transition between the close‐packed and the destroyed DNA/lipid conformation. The elastic urethane crosslinking bonds between base‐pair sites act as a fixing phase. The gel holds promise in its application as a gentle actuator. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 259–263, 2002 相似文献
999.
Free‐radical solution copolymerization of itaconic acid and acrylonitrile was carried out in DMSO using azodiisobutyronitrile as an initiator, changing the feed rate of itaconic acid. The resulting polymerization solution was spun to form polyacrylonitrile (PAN) precursors of carbon fibers. The precursors were treated with a CoSO4 aqueous solution on‐line. The structure and properties of untreated and treated PAN precursors and the resultant carbon fibers were characterized by SEM and TEM, a stabilization process, etc. It is suggested that CoSO4 acts as a catalyst in the formation of a ladder structure and reduces the temperature of cyclization, and the carbon fibers developed from treated PAN fibers showed improvement in the tensile strength and the Young's modulus. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 153–158, 2002 相似文献
1000.
The equations for predicting the number-average molecular weight are derived on the basis of the three stage polymerization model (TSPM) in this paper. By applying the equations, a plotting approach is proposed to determine the apparent initiator efficiency defined as f[(αtd+1)/2] and the constant of chain transfer to monomer, where f is the initiator efficiency and αtd denotes the fraction of the termination rate constants by disproportionation. Using the approach to plot the experimental data in the literature, it is found that the chain transfer to monomer can be neglected for both methylmethacrylate (MMA) and styrene (St) polymerizations, but it can exert a significant effect on ethylmethacrylate (EMA) polymerization. In addition, the apparent initiator efficiency is found to be independent of reaction temperature and initiator concentration at each stage. The values of f[(αtd+1)/2] at gel effect stage are slightly reduced as compared with that at low conversion stage for MMA and EMA polymerizations. However, it decreases significantly at gel effect stage for St polymerization. Using the equations derived and the apparent initiator efficiencies obtained from TSPM plots, the number-average molecular weights at different conversions can be predicted. Comparisons show that the agreement between predictions and experimental data is satisfactory. 相似文献