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121.
122.
In-situ composites based on dispersed poly (ethylene terephthalate) (PET) or polyamide (PA),and continuous Polyethylene (PE) were prepared through a single screw extruder of Haake rheometer system with a rod-die relatively small in diameter.The extrudate was drawn at a drawing ratio of 3.1,and then quickly cooled in cold water.The specimens were obtained by injection molding at processing temperatures less than 190℃,far below the melting temperature of PET (265℃) and PA (230℃),which can maintain the solid state of PET and PA microfiber phase in the composites.Morphological observation with scanning electron microscopy (SEM) indicated that PET and PA can more or less form in-situ microfibers at compositions studied (0-20 wt pct PET or PA),and especially,PET and PA were almost deformed into fibers at the concentration of 15wt pct.Eensile strength and especially.PET and PA were almost deformed into fibers at the concentration of 15wt pct.Tensile strength and modulus of the blends reinforced by PET or PA microfibers showed to be increased from the tensile test results.The most noticeable improvement of the tensile properties occurred at 15wt pct of PET in PET/PE system,corresponding to the highest microfiber content,where the tensile strength reached 32.5 MPa,whereas only 19.5 MPa for the pure PE. 相似文献
123.
The two-dimensional finite-element method is applied to analyze the shrinkage and splitting of microcracks regularly arranged
on or perpendicular to a grain boundary under pressure. Grain-boundary and surface diffusions are coupled by the boundary
conditions at the triple point of the microcrack surface and the grain boundary. The shrinkage and splitting processes for
the two kinds of microcracks are revealed by detailed finite-element analyses. For the microcrack lying on a grain boundary,
it first shrinks to a small void shape, then the void is split by the grain boundary and the two split voids assume a cylindrical
shape under the capillary force of the surface. For the microcrack perpendicular to the grain boundary, it is split into two
segments by the grain boundary during the early stage of shrinkage. Then, the split microcracks stop shrinking and evolve
into two cylindrical channels with a circular section by the capillary force of the surface. These evolution processes are
controlled by the applied pressure, microcrack spacing, ratio of grain-boundary diffusion to surface diffusion, and equilibrium
dihedral angle, defined by surface and grain-boundary tensions. The influences of these controlled parameters on the evolution
processes are numerically clarified based on a great number of finite-element analyses. 相似文献
124.
石油系油浆与煤系闪蒸油的焦化性能——I.热解条件的影响 总被引:3,自引:2,他引:1
通过偏光显微镜观察了石油系油浆(LH)与煤系闪蒸油(SN)焦化后所得焦块的光学结构。结果表明,在较宽条件下两种原料单独焦化均得不到取向度高的流线型结构。将两种原料以一定比例混合后先热解丙焦化所得焦块的光学结构明显好于二者混合后直接焦化所得焦块的光学结构,其中LH和SN以3:2的重量比混合后在440℃、1MPa下热解3.5h然后再在530℃、1MPa下焦化8h所得焦块为具有较高取向度的流线型结构,适合于作为针状焦的起始原料。 相似文献
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129.
Yaping KeLU 《材料科学技术学报》2002,18(6):492-496
In this paper,glass transition and thermal stability of the Zr-Al-Cu-Ni metallic glasses were investigated by using electrical resistance measurement(ERM),DSC and X-ray diffraction techniques.The experimental results show that the ERM is capable of detecting the glass transition of the amorphous alloys and can help to distinguish the crystallization products of the Zr-Al-Cu-Ni metallic glasses owing to the difference of the electrical resistivity between the precipitation phases. 相似文献
130.
通过对MgO:LiNbO3参量过程温度相位匹配及走离角,允许参量等运转参数的理论计算与分析,确定了晶体的切割角度θ=82℃,以近非临界相位匹配(NCPM)取代NCPM,将温度调节范围控制在较低的温度上,研制了532nm泵浦的MgO:LiNbO3温度调谐脉冲光学参数振荡器(OPO),在800~1700nm波段实现连续调谐输出。参量泵浦功率密度阈值为57.3MW/cm^2,泵浦能量约2倍阈值处,单谐振(SRO)参量转换效率为11%以上。 相似文献