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Emel Ozel Hilmi Yurdakul Servet Turan Matteo Ardit Giuseppe Cruciani Michele Dondi 《Journal of the European Ceramic Society》2010,30(16):3319-3329
Cobalt-doped willemite is a promising blue ceramic pigment, but some important aspects concerning crystal structure, optical properties and technological behaviour are still undisclosed. In order to get new insight on these features, willemite pigments (Zn2?xCoxSiO4, 0 < x < 0.3) were synthesized by the ceramic route and characterized from the structural (XRPD with Rietveld refinement), optical (DRS and colorimetry), microstructural (SEM, STEM, TEM, EDX, EELS) and technological (simulation of the ceramic process) viewpoints. The incorporation of cobalt in the willemite lattice, taking preferentially place in the Zn1 tetrahedral site, induces an increase of unit-cell parameters, metal–oxygen distances, and inter-tetrahedral tilting. It causes shifting and enhanced splitting of spin-allowed bands of Co2+ in tetrahedral coordination, implying slight changes of crystal field strength Dq and Racah B parameter, but increasing spin-orbit coupling parameter λ. Willemite pigments impart deep blue hue to ceramic glazes and glassy coatings with a colouring performance better than commercial Co-bearing colorants in the 800–1200 °C range. Detailed SEM-TEM investigation and microanalysis proved that no diffusion phenomena occur at the pigment–glassy coating interface and that willemite pigments are chemically inert during firing at 1050 °C. 相似文献
23.
Black iron-chromium (Fe-Cr) bearing oxide pigments are generally utilised as effective colourants in a wide variety of applications. However, in the case of their use within ZnO-containing glazes, they yield an undesirable brown colour instead of expected black colour. In order to understand the colour change in this system, we report the use of focused ion beam (FIB) sample preparation technique followed by the use of analytical transmission electron microscopy (TEM) characterisation techniques. According to the results, the formation of a reaction layer between the pigment and glaze was identified with an average composition of Zn0.48Fe0.79Cr1.32O4. Additionally, the valance of Fe was determined as 3+ in the pigment grain, whereas 2+ in the reaction layer and the glaze, respectively. Therefore, it was concluded that the colour change is occurring as result of the valence variation of Fe, the formation of Zn0.48Fe0.79Cr1.32O4 compound and the outward diffusion of Fe into the glaze. 相似文献
24.
Fatih Alim Kursat Bekar Kostadin Ivanov Kenan Unlu Jack Brenizer Yousry Azmy 《Annals of Nuclear Energy》2006,33(17-18):1391-1395
Due to inherited design issues with the current arrangement of beam ports (BPs) and reactor core-moderator assembly in The Perm State Breazeale Reactor (PSBR), the development of innovative experimental facilities utilizing neutron beams is extremely limited. Therefore, a study has started to examine the existing BPs for neutron and gamma outputs and develop a new core-moderator location and BP geometry in PSBR. Although 7 BPs are placed in PSBR, 2 of them are using currently. In this study BP 4, one of the currently being used BP, is examined. With changing the location of the BP 4 and structure of the core assembly, some artificial models are developed and compared with the original model. 相似文献
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Kenan Xu Quanhong Wang Hossam Hassanein 《International Journal of Communication Systems》2005,18(7):619-637
This paper proposes a multi‐dimensional Markov model to analyse the performance of the IEEE 802.11e EDCF MAC protocol. Based on this model, we present extensive performance evaluation in terms of throughput, throughput ratios, and access delay of flows of distinct priorities under RTS/CTS mode. We also provide quantitative analysis of the impact of prioritized parameters, i.e. Arbitration InterFrame Space (AIFS), Contention Window (CW) on Quality of Service (QoS) differentiation. The accuracy of the proposed model is verified by means of comparing the numerical results obtained from both analytical model and simulations. Our research can be used as a guideline for the prediction of how flows belonging to a certain Traffic Category (TC) perform with their TC‐specific parameters, as well as designing EDCF‐based WLANs and tuning the parameters to achieve the desirable differentiated QoS objectives. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
27.
Ozone is a sufficiently strong oxidant to cause the oxidation of bromide ion and formation of bromate ion. In this study, bromate ion formation in a wide variety of drinking water sources was analyzed, with bromate ion formed in all sources under drinking water treatment conditions. Threshold levels for pH, bromide ion concentration, and ozone dose were found to be source-specific. Two non-linear empirical models were developed to predict bromate ion formation; these models are easy to use and require only several water quality and treatment variables. The models were tested against several literature data and a good simulation was found in other bench-scale tests, whereas the model tended to under-predict bromate ion formation in pilot-scale and full-scale programs. 相似文献
28.
An integrated optics (IO) device that is an implementation of an IO tapped delay line is discussed. It is capable of performing discrete convolution of an optical pulse sequence with a preset digital function. Several architectures for the device are presented. A systematic realization of the preset function samples that permits efficient utilization of all the input light power and maximization of the output signal-to-noise ratio (SNR) for the device is discussed. A detailed analysis of what determines the number of preset samples that can be realized and how to realize them on a LiNbO3 crystal is given. Two digital filter design examples are presented, and the quantization error effects on their performance are examined. The same architectures are shown to implement digital-to-analog (D/A) conversion and systolic multiplication of a Toeplitz matrix with a vector having the form of optical pulses 相似文献
29.
Yong‐Mei Xia Zhi‐Shan Hua Onnop Srivannavit Ayse Bilge Ozel Erdogan Gulari 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2007,82(1):33-38
Polydimethyl siloxane (PDMS)–glass microchip has a very strong surface effect on polymerase chain reaction (PCR), leading to a very poor PCR yield. In the work reported here, practical dynamic passivation of surfaces of PDMS–glass microchip using polyethylene glycol (PEG) or polyvinylpyrrolidone (PVP) was achieved using a conventional thermocycler. The passivation procedure was cost‐effective and easy to conduct. The effects of polymer molecular weight and polymer concentration on tube PCR efficiency were investigated primarily to prescreen out suitable polymers and polymer concentrations in the PCR mixture. The result from tube PCR indicated that both PEG and PVP could affect the performance of Taq polymerase. A final concentration of 0.025% (w/v) or 0.4% (w/v) polymer in the PCR mixture can enhance the tube PCR, while 1% (w/v) polymer was found to inhibit the reaction. PEG was more effective in tube PCR, although PVP performed better in chip PCR. Instead of employing the polymer directly in the PCR mixture, i.e. the conventional in situ passivation approach, another approach of dynamic passivation by pre‐injecting polymers into the microchip achieved better performance. The efficiency of pre‐passivation was found to follow the order: PVP10000>PVP55000, PEG8000> PEG10000>PEG400. After pre‐passivation with PVP10000, PVP55000 and PEG8000, the PCR efficiency can recover to 93%, 86% and 83%, respectively, of that obtained from tube PCR. Copyright © 2006 Society of Chemical Industry 相似文献
30.
<正>项目位于上海市青浦区,比邻汇金路和盈港东路,定位为其东侧的青浦宝龙城市广场临时售楼处。青浦宝龙城市广场作为青浦区首个地铁上盖(17号线汇金路站)城市综合体,拥有35万m2的建筑面积,建成后将成为西上海全业态都市生活中心。项目基地是临时的,事实上是10m宽的基地退界绿地。项目预算封顶,业主内部立项的时候包括室内和景观的总造价就已经确定,且不可以追加。在10m城市道路退界绿地内造临时售楼处,对业主一系列的项 相似文献