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采用不同工艺参数对2 mm厚Ti40阻燃钛合金进行电子束焊接(EBW),通过金相分析、电子探针(EPMA)、室温拉伸以及显微硬度测试对Ti40阻燃钛合金电子束焊接接头的显微组织和力学性能进行分析.结果表明,焊缝中分布着晶粒内部有片层状组织析出的β柱状晶和少量等轴β晶粒,熔合线到焊缝中心晶粒逐渐细化,无明显热影响区.接头中易产生气孔、裂纹等缺陷,通过添加直线扫描波形能够有效地控制焊缝气孔缺陷,从而提高接头的强度.添加直线扫描波形电子束焊的Ti40阻燃钛合金的抗拉强度仍可达到917 MPa,断口呈现出脆性断裂与韧性断裂的混合特征,焊缝区的硬度高于母材,其最大值为376HV. 相似文献
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Li Y Zhou W Wang H Xie L Liang Y Wei F Idrobo JC Pennycook SJ Dai H 《Nature nanotechnology》2012,7(6):394-400
Oxygen reduction reaction catalysts based on precious metals such as platinum or its alloys are routinely used in fuel cells because of their high activity. Carbon-supported materials containing metals such as iron or cobalt as well as nitrogen impurities have been proposed to increase scalability and reduce costs, but these alternatives usually suffer from low activity and/or gradual deactivation during use. Here, we show that few-walled carbon nanotubes, following outer wall exfoliation via oxidation and high-temperature reaction with ammonia, can act as an oxygen reduction reaction electrocatalyst in both acidic and alkaline solutions. Under a unique oxidation condition, the outer walls of the few-walled carbon nanotubes are partially unzipped, creating nanoscale sheets of graphene attached to the inner tubes. The graphene sheets contain extremely small amounts of irons originated from nanotube growth seeds, and nitrogen impurities, which facilitate the formation of catalytic sites and boost the activity of the catalyst, as revealed by atomic-scale microscopy and electron energy loss spectroscopy. Whereas the graphene sheets formed from the unzipped part of the outer wall of the nanotubes are responsible for the catalytic activity, the inner walls remain intact and retain their electrical conductivity, which facilitates charge transport during electrocatalysis. 相似文献
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Hongyang Wang Baoqiang Feng Gang Song Liming Liu 《Materials and Manufacturing Processes》2018,33(7):735-742
The laser–tungsten inert gas hybrid welding method was adopted to realize the welding process between Q460 high-strength steel and 6061 aluminum alloy. The influence of the dual heat source on the mechanical properties and microstructure of the welded joints are discussed. In addition, the effects of including a copper–zinc interlayer on the microstructure, elemental distribution, and mechanical properties of welded joints are also studied. The results show that the mechanical properties of the welded joints are influenced by the relative heat inputs of the two heat sources and the Cu-Zn interlayer. The braze welded joint fabricated without a Cu-Zn interlayer fractured at an Al-Fe intermetallic compound (IMC) layer formed at the interface, whereas the braze welded joint fabricated with a Cu-Zn interlayer fractured at an Al-Cu IMC layer formed at the interface. Comparisons show that the maximum tensile shear load of the brazed welded joint with the Cu-Zn interlayer was increased by about 20% relative to that formed without the interlayer. The formation of Al-Fe IMC layer in the deep penetration joint was inhibited by the combined effect of the dual heating sources and the Cu-Zn interlayer. 相似文献
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Bioadhesive Polymersome for Localized and Sustained Drug Delivery at Pathological Sites with Harsh Enzymatic and Fluidic Environment via Supramolecular Host–Guest Complexation
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Meiling Zhu Kongchang Wei Sien Lin Xiaoyu Chen Chia‐Ching Wu Gang Li Liming Bian 《Small (Weinheim an der Bergstrasse, Germany)》2018,14(7)
Targeted and sustained delivery of drugs to diseased tissues/organs, where body fluid exchange and catabolic activity are substantial, is challenging due to the fast cleansing and degradation of the drugs by these harsh environmental factors. Herein, a multifunctional and bioadhesive polycaprolactone‐β‐cyclodextrin (PCL‐CD) polymersome is developed for localized and sustained co‐delivery of hydrophilic and hydrophobic drug molecules. This PCL‐CD polymersome affords multivalent crosslinking action via surface CD‐mediated host–guest interactions to generate a supramolecular hydrogel that exhibits evident shear thinning and efficient self‐healing behavior. The co‐delivery of small molecule and proteinaceous agents by the encapsulated PCL‐CD polymersomes enhances the differentiation of stem cells seeded in the hydrogel. Furthermore, the PCL‐CD polymersomes are capable of in situ grafting to biological tissues via host–guest complexation between surface CD and native guest groups in the tissue matrix both in vitro and in vivo, thereby effectively extending the retention of loaded cargo in the grafted tissue. It is further demonstrated that the co‐delivery of small molecule and proteinaceous drugs via PCL‐CD polymersomes averts cartilage degeneration in animal osteoarthritic (OA) knee joints, which are known for their biochemically harsh and fluidically dynamic environment. 相似文献
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分布式IP视频会议系统中声像同步技术的研究与实现 总被引:3,自引:2,他引:3
在分布式多媒体系统中,多媒体信息的同步传输是一项关键问题。该文探讨了在分布式IP视频会议系统中如何实现声像同步控制的问题,并给出了具体可行的解决方案。 相似文献