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21.
Shintaro Nakano Nobuyoshi Saito Kentaro Miura Tatsunori Sakano Tomomasa Ueda Keiji Sugi Hajime Yamaguchi Isao Amemiya Masato Hiramatsu Arichika Ishida 《Journal of the Society for Information Display》2012,20(9):493-498
We have successfully reduced threshold voltage shifts of amorphous In–Ga–Zn–O thin‐film transistors (a‐IGZO TFTs) on transparent polyimide films against bias‐temperature stress below 100 mV, which is equivalent to those on glass substrates. This high reliability was achieved by dense IGZO thin films and annealing temperature below 300 °C. We have reduced bulk defects of IGZO thin films and interface defects between gate insulator and IGZO thin film by optimizing deposition conditions of IGZO thin films and annealing conditions. Furthermore, a 3.0‐in. flexible active‐matrix organic light‐emitting diode was demonstrated with the highly reliable a‐IGZO TFT backplane on polyimide film. The polyimide film coating process is compatible with mass‐production lines. We believe that flexible organic light‐emitting diode displays can be mass produced using a‐IGZO TFT backplane on polyimide films. 相似文献
22.
Takeshi Kikuchi Yoshizo Kitami Masato Yokoyama Hiroshi Sakai 《Journal of Materials Science》1989,24(12):4275-4278
The phase equilibria in the pseudo-binary system Bi2O3-TeO2 at 600° 950° C in air were examined by solid-state reaction techniques and X-ray powder diffraction method. Four pseudo-binary compounds appeared, i.e., -Bi2O3 type solid solution having a compositional range of (1-x)Bi2O3·xTeO2 wherex=0 0.4 a new compound Bi6Te2O15 which has an orthorhombic cell of a=2.27(4) nm, b=1.06(1) nm and c = 0.539(8) nm, 2Bi2O3 · 3TeO2, and an unidentified phase Bi2O3·2TeO2. The formation of the phase Bi6Te2O15, in which all the Te ions are hexavalent, was confirmed by the thermogravimetry and by the Mössbauer spectra. The liquidus curves for whole system were determined by DTA method. 相似文献
23.
Taxonomy for protective ability of rust layer using its composition formed on weathering steel bridge 总被引:2,自引:0,他引:2
For a quantitative evaluation of the protectiveness of a rust layer formed on a weathering steel bridge, the relationship between the corrosion rate of the bridge and the composition of the rust layers formed on the girders was first investigated. These corrosion rates were clearly classified by the protective ability index (PAI) of α/γ∗ and (β + s)/γ∗, where α, γ∗, β and s are the mass ratio of crystalline α-FeOOH, the total of γ-FeOOH, β-FeOOH and the spinel-type iron oxide (mainly Fe3O4), β-FeOOH and spinel-type iron oxide, analyzed by XRD, respectively. The inequality of the former index α/γ∗ > 1 expressed the protectiveness criterion of the rust layer, while that of the latter index, (β + s)/γ∗< 0.5 or > 0.5, classified the corrosion rate of the non-protective rust layer. The PAI is useful for a quantitative evaluation of the protectiveness of a rust layer formed on a weathering steel bridge and is an important item for the corrosion assessment of the bridge. 相似文献
24.
In Situ Observation of Phase Separation of a Barium Borate Melt in a Stable Immiscibility Region under Microgravity 总被引:1,自引:0,他引:1
Satoru Inoue Akio Makishima Hiroyuki Inoue Kohei Soga Tomoya Konishi Tomoyoshi Asano Yuu Ishii Masato Koyama 《Journal of the American Ceramic Society》1997,80(9):2413-2417
The precipitation of droplets was directly observed on a BaO–B2 O3 melt in a drop shaft experiment. This is the first time that precipitation of droplets has been observed in a 4.5 s drop test. The melt film of 4BaOz96B2 O3 (mol%) held on a platinum wire loop was heated above the critical tem-perature to produce uniformity and was cooled down to the phase separation temperature range. Phase separation of the melt was observed directly with a video camera. The IR image of the melt was simultaneously detected with a CCD array and was converted into a two-dimensional thermograph. 相似文献
25.
Summary The ring-opening polymerization of deoxophostone 5, a five-membered cyclic phosphinite, has been studied. Some cationic initiators gave polymer whereas anionic and radical initiators as well as metal chloride (Lewis acid) catalysts did not yield polymer. The polymer consisted of a phosphine oxide repeating unit 6. The polymerization proceeded via the Arbuzov-type reaction. The reduction of polymer 6 with a HSiCl3/Et3N system gave polyphosphine 7. 相似文献
26.
Jacques G. Noudem Sophie Meslin Daniel Horvath Christelle Harnois Daniel Chateigner Bachir Ouladdiaf Sophie Eve Mousta Gomina Xavier Chaud Masato Murakami 《Journal of the American Ceramic Society》2007,90(9):2784-2790
The recently reported hole-patterned YBa2 Cu3 O y (Y123) bulks with improved superconducting properties are highly interesting from material quality and application variety points of view. It is well known that the core of plain bulk superconductors needs to be fully oxygenated and some defects like cracks, pores, and voids must be suppressed in order that the material can trap a high magnetic field or carry a high current density. To minimize the above defects, we have used a combination of standard superconducting ceramic processing and an infiltration technique to prepare regularly perforated YBa2 Cu3 O y (Y123) bulk superconductors. This process leads to negligible shrinkage upon annealing and a uniform distribution of Y211 inclusions. Texture was evidenced by neutron pole figure measurements. Flux mapping was used to verify the superconducting homogeneity of the samples and to investigate the field-trapping ability. In addition, the textured drilled samples were reinforced using resin or metal impregnation and the influence of the different processing steps on the hardness of the materials has been investigated. 相似文献
27.
Summary A binary system of a palladium complex as catalyst and zinc alkoxide as initiator conducted a novel ring-opening polymerization of cyclic carbonate, i. e., 5,5-dimethyl-4-ethenyl-1,3-dioxan-2-one. The polymerization proceeded along with releasing carbon dioxide to produce the corresponding polyether. The -allylpalladium complex generated from the monomer with the catalyst is the key intermediate for this new polymerization. The propagating end is zinc alkoxide, which nucleophilically attacks the monomer activated as the -allylpalladium complex in the propagation. 相似文献
28.
Masato Sakaguchi Tetsuro Yokono Yuzo Sanada Junkichi Shoma Hisatsugu Kashiwabara 《Fuel》1981,60(2):136-138
The ball-milling of coal with methylmethacrylate monomer was carried out under vacuum at 77 K and at room temperature and in air. The e.s.r. and i.r. spectra of ball-milled material showed that a copolymer of coal and methylmethacrylate was formed on the surfaces of coal created by ball-mining. Oxygen is an inhibitor to this process. 相似文献
29.
Masatomo Yashima Katsuya Ohtake Masato Kakihana Masahiro Yoshimura 《Journal of the American Ceramic Society》1994,77(10):2773-2776
Homogeneous metastable tetragonal ( t ') solid solutions of ZrO2 — x mol% CeO2 ( x = 20 and 50) were successfully synthesized by the organic polymerized complex method. The citric acid-ethylene glycol solution containing Zr and Ce ions was polymerized at about 140°C and then heat-treated at about 350°C to obtain a precursor. The black precursor was heated at 450°C and then fired up to 1300° or 1590°C, resulting in the homogeneous solid solutions. 相似文献
30.
Somsak Vivatpanachart Hiroyasu Nomura Yutaka Miyahara Hisatsugu Kashiwabara Masato Sakaguchi 《Polymer》1981,22(7):896-901
E.s.r. spectra of chain-end spin labels on the surface of polyethylene powder were obtained for high and low density polyethylene samples at various stages of heat treatment process. The subsequent crystalline structures of the samples were examined with wide angle and small angle X-ray diffraction spectra. The effects of annealing on the motion of the labels were dependent on annealing temperature and the type of the samples. Higher temperature annealing decreased the rotational correlation times (τc) and their activation energy in high density polyethylene but did not affect those of low density polyethylene. Melting decreases the values of τc and ΔE for both high an low density polyethylene samples. The cause of these decreases were attributed to the changing of the sites of the chain-end labels. The motion of the labels appeared to be influenced by the local segmental motion of the polymer main chains. 相似文献