Die einzelnen Lebensmittel (Chemie, Technologie, Analytik)

Ohne Zusammenfassung     

Critical Issues on Kalman Filter with Colored and Correlated System Noises

The Kalman filtering (KF) is optimal under the assumption that both process and observation noises are independent white Gaussian noise. However, this assumption is not always satisfied in real‐world navigation campaigns. In this paper, two types of KF methods are investigated, i.e. augmented KF (AKF) and the second moment information based KF (SMIKF) with colored system noises, including process and observation noises. As a popular noise‐whitening method, the principle of AKF is briefly reviewed for dealing with the colored system noises. The SMIKF method is developed for the colored and correlated system noises, which directly compensates for the covariance through stochastic model in the sense of minimum mean square error. To accurately implement the SMIKF, a refined SMIKF is further derived regarding the continuous‐time dynamic model rather than the discrete one. The computational burdens of the proposed SMIKF along with representative methods are analyzed and compared. The simulation results demonstrate the performances of proposed methods.     

Simple and accurate analytical solution to the post-buckling response of an electrostatically actuated MEMS curled cantilever

In this work, we propose to investigate the micro-electromechanical post-buckling response of an electrostatically-actuated curled cantilever microbeam. The analytical/numerical model is based on a nonlinear differential governing equation, derived via assuming a continuous Euler–Bernoulli beam model, combined with a multi-modes Galerkin decomposition of the beam deflection. The pull-in voltages which govern the stability of the micro-curled beam actuator are also obtained analytically. These approximate solutions show excellent agreements compared to solutions obtained by other computationally expensive numerical methods as well some previously reported experimental data, for a wide range of the microbeam length. The derived expressions of these analytical approximate solutions are easy to implement, quick to solve, and could be conveniently used by MEMS designers for quick estimations of the effects of the various micro-actuator parameters on its structural stability.     

A resource allocation algorithm for throughput maximization with fairness increase based on virtual PRB in MIMO-OFDMA systems

This paper deals with a new resource allocation algorithm in downlink MIMO-OFDMA systems. The objective is to maximize the system throughput with respect to fairness criteria since some users may experience bad channel conditions for a long time. Known to be NP-hard, the original optimization problem is divided into two sub-problems where radio resource allocation and power allocation are performed separately. Firstly, a recursive PRB allocation algorithm is performed aiming at maximizing the system throughput. In LTE systems, 41% of sub-carriers are considered unused which introduces spectral efficiency loss. As solution, the eNodeB aggregates the unused sub-carriers by each user to construct a “virtual” PRB to be allocated to seldom served user for fairness and throughput increase. Secondly, power allocation is performed to select a more appropriate MCS.

     

Preparation of a novel zwitterionic graphene oxide-based adsorbent to remove of heavy metal ions from water: Modeling and comparative studies

A novel zwitterionic graphene oxide-based adsorbent was first synthesized in a multistep procedure including the successive grafting of bis(2-pyridylmethyl)amino groups (BPED) and 1,3-propanesultone (PS) onto graphene oxide (GO) sheets. Then, the as-prepared materials were used as adsorbent for the removal of metal ions from aqueous solutions. The influence of solution pH, contact time, metal ion concentration, and temperature onto the adsorption capacity of the zwitterionic GO-BPED-PS adsorbent was investigated and compared with the GO-BPED adsorbent. In particular, it was shown that the maximum adsorption capacities of the GO-BPED-PS adsorbent were as high as 4.174 ± 0.098 mmol.g^?1 for the Ni(II) ions and 3.902 ± 0.092 mmol.g^?1 for the Co(II) ions under optimal experimental conditions (metal ion concentration = 250 mg.L^?1, pH = 7 and T = 293 K). In addition, the adsorption behaviors of Ni(II) and Co(II) ions onto both the GO-BPED and GO-BPED-PS adsorbents fitted well with a pseudo-second-order kinetic model and a Jossens isotherm model. Moreover, adsorption thermodynamics of Ni(II) and Co(II) ions have been studied at various temperatures and confirmed the exothermic adsorption nature of the adsorption process onto the GO-BPED-PS adsorbent. Furthermore, the zwitterionic GO-BPED-PS adsorbent retained good adsorption properties after recycling 18 times which is much better than the conventional adsorbents.     

Development of a Novel High-Performance Thin Layer Chromatography–Based Method for the Simultaneous Quantification of Clinically Relevant Lipids from Cells and Tissue Extracts

Lipids such as cholesterol, triacylglycerols, and fatty acids play important roles in the regulation of cellular metabolism and cellular signaling pathways and, as a consequence, in the development of various diseases. It is therefore important to understand how their metabolism is regulated to better define the components involved in the development of various human diseases. In the present work, we describe the development and validation of a high-performance thin layer chromatography (HPTLC) method allowing the separation and quantification of free cholesterol, cholesteryl esters, nonesterified fatty acids, and triacylglycerols. This method will be of interest as the quantification of these lipids in one single assay is difficult to perform.