Monitoring the Synthesis and Composition Analysis of Microsilica Encapsulated Acetylacetonatocarbonyl TriphenylphosphinerhodiumCatalyst by Inductively Coupled Plasma (ICP) Techniques

A novel technique to monitor the synthesis process of encapsulated acetylacetonatocarbonyl triphenylphosphinerhodium within a microsilica nanoshell has been studied using inductively coupled plasma (ICP) techniques. Nanospheres sized around 50-100 nm were obtained and ICP was used to quantify the exact composition of rhodium, phosphorous, and silicon with differing digestion solvents. In addition, ICP was used to detect rhodium and phosphorous in the nano core-shell catalysts as a quality control procedure     

Particularities of condensation of atoms with increased kinetic energy

Novel universal method for measurement of the condensation coefficient α is developed. Using this method, noticeable difference between measured (α≈0.8) and expected (α≈1) values of the condensation coefficient for sputtered Cr atoms was revealed for the first time. The effect is assumed to be a result of considerable elevation of the surface temperature during atomic condensation induced by the energy delivered to the condensation surface by sputtered atoms and from the plasma.     

基于XC164CS微处理器的正弦脉宽调制信号的实现

把电压空间矢量的概念引入到正弦脉宽调制波形产生中,介绍了16位微处理器在正弦脉宽调制中的应用,并基于具体硬件结构利用双极性调制方法实现了正弦脉宽调制波形的生成。试验证明:本方案具有计算速度快、效率高的优点,在工程实践中切实可行。     

Sintering and Electronic Conducting Properties of Lao.7Ca0.3CrO3 Perovskite Synthesized by a Glycine-nitrate Process

La0.7 Ca0.3 CrO3 powder consisting of superfine and uniform particles （ 100-200 nm ） were synthesized using a glycine-nitrate process （ GNP ）. The sintering and electronic conducting properties of La0.7 Ca0.3 CrO3 were invetigated in the sintering temperature range of 1 200-1 450 ℃. The desired morphology of the powder significantly improved its sinterability. La0.7 Ca0.3 CrO3 ceramics sintered at 1 250-1 450 ℃ show high relative densities above 95 % . The ceramics sintered at 1 250-1 400 ℃ have very similar electronic conduct- ing properties, providing electronic conductivities around 55 Ω^-1 cm^-1 at a measuring temperature of 800 ℃ . Further increasing the sintering temperature to 1450 ℃ led to an apparent degradation of electronic conducting properties. This research demonstrates the advantage of the GNP in producing La0.7 Ca0.3 CrO3 with respect to the enhanced sintering properties and superior electronic conducting properties.     

High performance series-resonance energy-recovery circuit for plasma display panel

A new high performance series-resonance energy-recovery circuit (ERC) for a plasma display panel (PDP) is proposed. Two different ERCs are used for both sides of the PDP, and the slow falling and fast rising times are employed. Therefore, it features the zero voltage switching, low electromagnetic interference, low current stress, no severe voltage notch, and high energy-recovery capability.     

冷镦钢新型脱氧剂的试验研究

采用新型复合脱氧剂和脱氧工艺对冷镦钢进行工业性试验研究，研究结果表明：冷镦钢采用AlMg合金脱氧获得了良好的脱氧效果，可以避免形成大型夹杂物，提高钢水纯净度。     

中国(大陆)粉末冶金零件行业2004年进展

本文介绍了中国（大陆）粉末冶金零件行业2004年的生产概况与市场动向。阐述了粉末冶金汽车零件的市场动态。分析了中国（大陆）粉末冶金零件行业面临的挑战。介绍了美国APMI International的PMT认证。     

加工配送，钢铁企业营销新战略

加工配送是当前一种新型的钢材物流服务方式，在营销战略方面已经越来越受到钢铁企业的高度重视。对当前国内钢材加工配送的市场状况的成因进行了分析，对部分生产企业的基本特点进行了描述，并对钢材加工配送未来的发展方向进行了阐述。     

生物脱氮技术处理废水的应用实践

对废水生物脱氮工艺的开工调试进行了分析,通过对污泥的培养、驯化、使活性污泥达到最佳的污水处理状态。对在调试过程中出现的问题提出相应的改进措施,进一步降低了外排水生化指标。     

级数sum from n=1 to ∞(α(α-1)…(α-n+1)x~n/n!)在x=±1处的敛散性研究

用比较原则及莱布尼兹判别法对函数f(x)=(1+x)α的马克劳林级数在x=±1的敛散情形给予讨论.