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41.
An efficient, convenient and quantitative method for characterising polyester end-groups is described. We have found that trichloroacetyl isocyanate (TAI) reacts rapidly and quantitatively with both carboxyl [C(O)OH] and hydroxyl (OH) chain ends to form derivatives that can be readily determined by 1H NMR spectroscopy. The TAI capped end-groups give rise to characteristic imidic NH resonances in a normally clear region of the 1H NMR spectrum [δ∼10-11.5 for C(O)-O-C(O)-NH-C(O)CCl3 from C(O)OH, δ∼8-9 for O-C(O)-NH-C(O)CCl3 from OH]. The method has been successfully applied to quantitative determination of the end-groups of a wide variety of oligomeric polyesters. It has also been applied to higher molecular weight polyesters including commercial, bottle grade, poly(ethylene terephthalate) (PET) and PET based copolyesters (e.g. PETG). 相似文献
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The results of study of the effects of yttria stabilization (0–6 mol.%) on the room-temperature fracture behavior and toughening mechanisms in zirconia-reinforced MoSi2 are presented in this paper. Transformation toughening is shown to occur only in composites reinforced with zirconia particles stabilized with 2 mol.% yttria. However, the fracture toughness levels are comparable in the other composites with yttria levels between 0 and 6 mol.%. Toughening in the other composites is attributed to the combined effects of residual stress, microcrack shielding/anti-shielding and/or crack deflection. A rigorous micromechanics-based model is presented for the estimation of residual stress levels in brittle materials reinforced with phases that can transform during cooling or under stress. The model is applied successfully to the rationalization of the observed fracture and toughening phenomena. 相似文献
44.
J. K. Richard Weber† Collin D. Anderson Dennis R. Merkley Paul C. Nordine† 《Journal of the American Ceramic Society》1995,78(3):577-582
Solidification of aluminum oxide from undercooled melts was investigated in containerless experiments. Specimens were levitated in a gas jet, stabilized with an acoustic positioning device, and melted with cw CO2 laser beams. Cooling curves were obtained by optical pyrometry when the laser intensity was reduced. The materials examined were high-purity Verneuil sapphire, 99.5% polycrystalline alumina, and oxide materials recovered from the effluent of an aluminum-fueled rocket motor. The degree of undercooling, the apparent temperature behavior during the thermal arrest on solidification, and the structure of the materials formed were different in argon and oxygen atmospheres. Undercooling of the sapphire and alumina materials was 360 ± 10 K in an oxygen atmosphere and approximately 450 K in argon. Melting and solidification of high-purity sapphire resulted in a dendritic and porous polycrystalline material in oxygen. Dense, larger crystals were obtained in argon. Products formed from 99.5% alumina were discolored and the cores were white, indicating impurity segregation effects. More reproducible behavior was observed for the sapphire and 99.5% alumina than for the tungstencontaminated rocket motor effluent materials. 相似文献
45.
Richard Quon 《电子产品世界》2002,(22):29-30,40
如今高性能通信系统有多种形式,在企业网络中,它也许是路由器,或是将以太局域网(LAN)的数据转发至OC-48 SONET光网络的多业务转换装置;在蜂窝网络中,它可能是第三代宽带无线网络控制器(RNC),将基站(BTS)的移动蜂窝电话呼叫发送至公共交换电话网(PSTN);在存储网络中,它可以是将服务器的数据备份至廉价磁盘冗余阵列(RAID)的光纤通道存储转换器。无论何种特殊类型的网络,这些系统的共同用途是接收来自信息源的数据,决定它需要发至何处,并有效地将它传送至目的地。为了支持这些关键功能,需要有一套通用通信元件或“基本构… 相似文献
46.
Rahul Sarpeshkar Richard F. Lyon Carver Mead 《Analog Integrated Circuits and Signal Processing》1998,16(3):245-274
Low-power wide-dynamic-range systems are extremely hard to build. The biological cochlea is one of the most awesome examples of such a system: It can sense sounds over 12 orders of magnitude in intensity, with an estimated power dissipation of only a few tens of microwatts. In this paper, we describe an analog electronic cochlea that processes sounds over 6 orders of magnitude in intensity, and that dissipates 0.5 mW. This 117-stage, 100 Hz to 10 KHz cochlea has the widest dynamic range of any artificial cochlea built to date. The wide dynamic range is attained through the use of a wide-linear-range transconductance amplifier, of a low-noise filter topology, of dynamic gain control (AGC) at each cochlear stage, and of an architecture that we refer to as overlapping cochlear cascades. The operation of the cochlea is made robust through the use of automatic offset-compensation circuitry. A BiCMOS circuit approach helps us to attain nearly scale-invariant behavior and good matching at all frequencies. The synthesis and analysis of our artificial cochlea yields insight into why the human cochlea uses an active traveling-wave mechanism to sense sounds, instead of using bandpass filters. The low power, wide dynamic range, and biological realism make our cochlea well suited as a front end for cochlear implants. 相似文献
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48.
Although lexical frequencies are familiar measures of stylistic and thematic analysis, only recently have some stylostatisticians been tempted to investigate the relationship between the frequency and topography of repeated lexical items. In the present paper the authors have turned to the study of the four focal types of discursive narratology, using Marguerite Duras'Moderato Cantabile. Their intent is to uncover aspects of narratological performance which further elucidate the communicative strategies in the story. Part 1 summarizes the problematic between frequency and topography. It describes how a topographical index can be computed for any repeated item and how a Global Topography Index (GTI) can summarize the major topographical characteristics of any text sequence. Part 2 presents a four-cell typology of narrational mode: a segmentation of the verbal chain into narrating and narrated speech acts, with each text sequence tagged according to its discursive function: overt sender intervention for story coherence or comment on the focal level of a narrating present; representation of discrete or unlocalized events on the focal level of a mimeticized past. In Part 3 the focal encodings are displayed in numerical and graphic form, first according to the eight surface chapter divisions and then according to twenty-six subsets of approximately equal length. The fluctuations of the topography indices are reviewed, with particular attention being paid to the manifestation of cluster effects. Although sender interventions predominate, the relativized behavior of each focal type contributes to a climactic unraveling of the intrigue in the final chapters. In conclusion, the authors stress the dichotomy between the calm surface of the chapters and the agitated tensions of the twenty-six subsets. 相似文献
49.
The abrasion characteristics of Tencel fabrics were evaluated by Martindale abrasion and laundering, and the breakdown mechanism of fibers was surveyed by scanning electron microscopy. The fabric was subjected to pad‐dry‐cure treatment with two different types of modified dimethyloldihydroxyethylene urea resins (Reaktant DH and Reaktant FC). Although the degree of dry abrasion varied with different resins, the damage exhibited by individual fibers differed little from untreated to resin‐treated; the major mechanism of abrasion was through friction, and the mechanism of fiber failure was multiple splitting and transverse cracking. In untreated Tencel, the characteristic feature of wet abrasion was massive fibrillation, and in crosslinked fabrics, the wet abrasion mechanism was through fiber slippage and slicing action, although in the Reaktant FC‐treated fabric, the wet abrasion mechanism was more through slicing than through fiber splitting. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1391–1398, 2006 相似文献
50.