Formation and retention of local melted films in AZ91 friction stir spot welds

The formation of local melted films during friction stir spot welding of as-cast AZ91D and thixomolded AZ91 material is investigated. The average temperatures close to the tip of the rotating pin vary from 438 to 454 °C during the dwell period in friction stir spot welding. These measured temperature values are higher than the melting temperature of α-Mg + Mg₁₇Al₁₂ eutectic (437 °C). It is suggested that the temperature in the stir zone during the dwell period is determined by the relative proportions of α-Mg and (α-Mg + Mg₁₇Al₁₂) eutectic material, which are incorporated during friction stir spot welding. Based on the stir zone temperature measurements and a detailed examination of material located at the root of the pin thread it is suggested that material is moved downwards via the pin thread and into the stir zone during the dwell period in friction stir spot welding. Evidence of local melted film formation is observed in the stir zone of AZ91 spot welds. It is suggested that melted films are retained since their dissolution rate is much slower in the high temperature stir zone than it is when melted films is formed in the stir zone during Al 7075-T6 friction stir spot welding. The spontaneous melting temperature, solute diffusion rate and the thermodynamic driving force for droplet dissolution are much higher during Al 7075-T6 friction stir spot welding.     

合成2,4-二叔丁基苯酚工业试验

以离子交换树脂为催化剂，苯酚和甲基叔丁基醚为原料合成2，4-二叔丁基苯酚(简称2，4酚)，合成产物经过滤再经间歇真空精馏精制提纯，得到高纯度的2，4酚成品。成品精馏后釜中残液在酸性白土催化剂的作用下通过歧化反应生成对叔丁基苯酚，再经精馏提纯得到成品对叔丁基苯酚。通过工艺优化，使2，4酚、对叔丁基苯酚形成联产生产工艺，降低了生产原料消耗和成本。     

二厘米微波衰减标准装置不确定度的验证

采用传递比较法对二厘米微波衰减标准装置不确定度进行了验证。测量标准装置的重复性以组内实验标准偏差sn(A)定量表征，测量标准装置的稳定性用组间实验标准偏差sm定量表征。     

An alternative method to compute the component fractions in the geometrical optical model: visual computing method

A method called visual computing was used to solve angular four-components' proportions and directional vegetation cover fraction for discrete canopies and continuous row-planted plants. It proved effective to predict the angular characteristics on pixel scale. The method could be an alternative way to a classical solution of geometrical optical models. A visual computing method would be effective especially when the canopies' spatial distribution and shapes were irregular and could not be described statistically.     

脉冲电镀最佳参数之探索和优化

本文利用正交实验法对脉冲电镀各控制参数进行试验,对影响分散能力、镀层可靠性及外观质量的各种因素进行探讨,寻找影响外观质量的显著因子并加以控制,同时进一步优化脉冲电镀的工艺参数。     

STUDY ON PHASE PERCEPTION IN SPEECH

The perceptual effect of the phase information in speech has been studied by auditory subjective tests. On the condition that the phase spectrum in speech is changed while amplitude spectrum is unchanged, the tests show that: (1) If the envelop of the reconstructed speech signal is unchanged, there is indistinctive auditory perception between the original speech and the reconstructed speech; (2) The auditory perception effect of the reconstructed speech mainly lies on the amplitude of the derivative of the additive phase; (3) td is the maximum relative time shift between different frequency components of the reconstructed speech signal. The speech quality is excellent while td <10ms; good while 10ms< td <20ms; common while 20ms< td <35ms, and poor while td >35ms.     

低发射率材料红外法向发射率谱测量方法的研究

采用热管技术研制了材料发射率谱的专用测量附件;利用双温测量技术,在P-E983型红外分光光度计及3600型数据站上进行了较低温度下低发射率材料红外法向发射率谱测量方法的研究.实测了几种材料的发射率谱;讨论了影响测量误差的诸因素.     

现代企业制度条件下企业管理的内涵

论述了在社会主义市场经济体制和现代企业制度条件下企业管理的主要内涵，提出了加强企业管理的途径和对策。     

氰化浸出体系中金的溶剂萃取

本文评述了金的碱性氰化溶液溶剂萃取研究与开发工作的最新进展。包括改性胺，季铵盐，磷氧化物及胍类萃取剂等。