磷铝杂原子固体酸催化剂催化合成乙酸异丙酯

以丙烯和乙酸为原料 ,自制的磷铝杂原子固体酸作催化剂催化合成了乙酸异丙酯 ,考察了反应温度、反应压力、反应空速 (LHSV)及催化剂用量对酯化反应的影响 ,同时考察了固体酸催化剂的重复使用性。确定了最佳合成条件 :反应压力 1 5MPa,反应温度 1 60℃ ,反应空速2 0h-1,催化剂用量 2 0g。在此条件下 ,酯化率可达 91 5 % ,乙酸异丙酯选择性达 99 0 % ,且催化剂的重复使用性良好。     

WSP特殊螺纹接头油井管的研制

介绍了WSP特殊螺纹接头的基本结构和设计思想,运用有限元方法,重点论述了密封设计和连接强度设计的方法和准则,并通过全尺寸试验进行了验证。计算和试验结果表明,该接头具有先进的螺纹形式、合理的扭矩台肩和金属/金属密封结构,有效地克服了API圆螺纹和偏梯形螺纹的不足,螺纹达到了与管体等强度,气密封能力达到了管体的内壁屈服压力。研究结果可以为开发更多适合油气田实际的特殊螺纹接头油井管提供参考。     

Why are Websites co-linked? The case of Canadian universities

This study examined why Websites were co-linked using Canadian university Websites as the test set. Pages that co-linked to these university Websites were located using Yahool. A random sample of 859 co-linking pages (the page that initiated the co-link) was retrieved and the contents of the page, as well as the context of the link, were manually examined to record the following variables: language, country, type of Website, and the reasons for co-linking. The study found that in over 94% of cases, the two co-linked universities were related academically; many of these cases (38%) showed a relationship specifically in teaching or research. This confirms results, from previous quantitative studies, that Web co-links can be a measure of the similarity or relatedness of sites being co-linked and that Web co-link analysis can thus be used to study relationships among linked Websites.     

M8011H16铝合金防盗盖板生产工艺研究

研究了元素含量变化对8011铝合金防盗盖板综合性能的影响，在8011合金中改变Cu、Mn元素含量后可提高防盗盖板的强度，同时研究了烘烤处理后的强度变化问题。本文研究出了8011铝合金防盗盖板新的生产工艺制度。     

硫氰酸铵光度法测定钒渣中钼量

研究了钒渣中钼与硫氰酸铵的显色反应，结果表明λmax=460nm，在0～50mg／50ml范围内吸光度与钼量的关系符合比尔定律，用于钒渣中钼的测定，结果令人满意。     

汽轮机数字电液控制系统及其应用

介绍了汽轮机数字电液控制系统（DEH）的硬件组成，着重论述了DEH的控制原理和控制过程。结合天津碱厂新建4^#机组,与前3台机组的液压控制调节方式进行比较，突出了DEH控制的优势。对DEH系统的软件作了介绍。同时对DEH的控制系统Foxboro I／A Series的系统软件和系统网络作了较详细的论述。最后，讨论了运行中可能出现的问题和解决方法。     

曲轴激光喷丸强化试验研究

采用实验的方法,研究了激光冲击强化对175A型柴油机曲轴疲劳寿命的影响,取得了激光冲击强化试验条件下曲轴过渡圆角处残余应力场的数据。并将激光冲击强化工艺效果和曲轴滚压强化效果做了对比性分析,结果表明：虽然激光冲击强化效果不如曲轴滚压强化,但考虑到激光工艺参数精确可控、加工质量好、成本低以及可避免滚压强化所造成的表面疲劳、撕痕等,激光冲击强化工艺可望代替滚压强化成为新型的曲轴强化手段。通过此类激光冲击强化强化实验可优化激光冲击的相关参数,使曲轴过渡圆角产生有利的残余应力场。     

基于CORBA和多Agent的模具敏捷制造的工作流管理

介绍了CORBA的工作原理，分析了模具敏捷制造的特点，提出了基于CORBA的模具敏捷制造工作流管理模型，并且将多Agent技术应用到该模型之中，使其具有清晰的结构，良好的开放性、集成性和自适应性。     

Fisher最优分割法在星星哨水库汛期分期划分中的应用

Fisher最优分割法是对有序样本进行最优化分段的一种数学方法。本文利用该方法对星星哨水库汛期进行相应的划分,结果表明该方法是可行的。因此,可利用该结果对分期实施不同的汛限水位,使水库的防洪和兴利效益达到最大。     

High‐Performance,Monolithic Polyaniline Electrochemical Actuators

New polyaniline (PANI) asymmetric membranes were fabricated using a phase‐inversion technique with hexane as the coagulation bath. These membranes exhibit a dense structure with macrovoids distributed asymmetrically throughout the cross‐section. A stress–strain study demonstrated that the Young's modulus (1.421 GPa) and strain at break (7.6 %) of the new PANI asymmetric membranes prepared from hexane are approximately 12 and 4 times higher, respectively, than the values reported previously for the PANI integrally skinned asymmetric membranes (ISAMs) (123 MPa Young's modulus and 1.8 % strain at break). Furthermore, monolithic electrochemical actuators based on a single PANI asymmetric membrane were constructed, and a bending movement of up to 20 Hz was experimentally recorded in a hydrochloric acid aqueous solution. A lifetime of over 329 500 cycles was determined for these actuators at a ± 2° angular displacement (5 Hz). The lifetime is limited by a bending fatigue that creates a transversal crack on the PANI membrane at the air–water interface. Control over the actuator movement is also manifested by the linear dependences of the bending angle on the charge and of the angular velocity on the current. These relationships are independent of both the kind of applied electric signal and the frequency used.